Angarsk Petrochemical Company Joint-Stock Company

Legal address:
665800, Irkutsk region, Angarsk, First industrial massif, block 63, building 2. Production Site:
Irkutsk region, Angarsk
e-mail: delo@anhk.rosneft.ru, t. 577-002

ISO 9001:2015 Quality Management System Certificate No. 19.2132.026

Certificate is valid until: 14.11.2022
ISO/TS 29001:2010 NO. 19.2140.026
Certificate is valid until: 14.11.2022

Testing Center - Quality Control Division

Angarsk Petrochemical Company Joint-Stock Company
665830, Irkutsk region, Angarsk, the territory of JSC ANHK
e-mail: of61@anhk.rosneft.ru tel. (39551 575-423

CERTIFICATE No. 273

Technical methanol grade A
Certificate of Conformity No.RPSS RU.AG91.НХ10
Valid till 07.02.2020
Designation of documents establishing requirements for products:
GOST 2222-95 "Technical methanol. Technical Specifications"
OKPD2 code 20.14.22.111
Batch No.: 273
Date of production: 11.12.2019
Size (weight) of the batch: 72.805 t
Place of sampling (under GOST 2517): Tank No. Е-6
Sampling date: 11.12.2019
Date of testing: 11.12.2019
The certificate is issued on the basis of: the test report of 11.12.2019, No.3352-250101/PK

No. Indicator Name Test method Standard under GOST 2222-95 Actual value

1 Appearance сl. 6.3 GOST 2222 Colorless transparent liquid Colorless transparent liquid
without insoluble impurities without insoluble impurities
2 Density at 20°C, g/cm{0>3<0} сl. 6.4 GOST 2222 0,791-0,792 0.791
3 Water miscibility сl. 6.5 GOST 2222 Mixes up with water without Mixes up with water without
traces of haze and opalescence traces of haze and
opalescence
4 Temperature limits: GOST 25742.1
boiling limit, ° С 64.0-65.5 64.1–64.8
99% of the product is distilled within, ° С 0,8 max 0.7
5 Mass fraction of water, % сl. 6.6 GOST 2222 0,05 max 0.010
Mass fraction of free acids in terms of formic acid,% GOST 25742.2 0,0015 max 0.0008

7 Mass fraction of aldehydes and ketones in terms of acetone,% сl. 6.7 GOST 2222 0.003 max 0.0017

8 Mass fraction of volatile iron compounds in terms of ferrum,% GOST 25742.8 0,00001 max Note Cl.2
9 Test with potassium permanganate, min GOST 25742.5 60 min 68
10 Mass fraction of ammonia and amino compounds in terms of ammonia,% GOST 25742.7 0,00001 max Note Cl.2
11 Chlorine mass fraction,% GOST 25742.6 0,0001 max Note Cl.2
12 Mass fraction of sulfur, % GOST 25742.3 0,0001 max Note Cl.2
13 Mass fraction of non-volatile residue after evaporation, %, сl. 6.8 GOST 2222 0.001 (max) Note Cl.2
14 Specific electrical conductivity, Cm / m сl. 6.9 GOST 2222 3 х 10-5 Note Cl.1
15 Mass fraction of ethyl alcohol,% GOST 25742.4 0,01 max Note Cl.2
16 Color on a platinum-cobalt scale, Hazen units сl. 6.10 GOST 2222 5 max 5

Conclusion: Technical methanol Grade A meets the requirements:

- GOST 2222-95 "Technical methanol. Technical Specifications"
Additional information:
1) Indicator 14 is determined in a product intended for the electro-vacuum and electronic industries.
2) Indicators 1-3, 6, 8, 10-15 are determined at the request of consumers.
Classification code 3222 (under GOST 19433-88).
Extremely hazardous flammable liquid. MAC (maximum allowable concentration) for work area 5 mg/m Hazard class 3
Warranty shelf life - 3 months from the date of manufacturing.
- Safety Data Sheets No. 05742746.24.42242.
- “Poison”, “Flammable”!
 Joint Stock Company "Angarsk Petrochemical Company" Legal address:
665800, Irkutsk region, Angarsk, First industrial massif, block 63, building 2
Production site:
Irkutsk region, Angarsk
e-mail: delo@anhk.rosneft.ru, t. (3955) 578-404: 577-002

Attachment to the certificate No. 273 dated 11.12.2019

Technical methanol grade A
GOST 2222-95 "Technical methanol. Technical Specifications"
No. Designation of a legislative act, a regulatory document or a set Information required for product description
No. of rules
Indicator Name Test method Actual value

1 Decision of the Council of the Eurasian Economic Commission Aggregate state at a temperature of 20 ° C and a — Liquid
of July 16, 2012 No. 54 "On approval of the Unified pressure of 760 mm Hg
Commodity Nomenclature for Foreign Economic Activity of the
Eurasian Economic Union and the Unified Customs Tariff of
the Eurasian Economic Union".

Refinery Process Name