INSPECTION & TESTING REQUIREMENTS REVISION: 07/14/2012 CODE NUMBER: PAGE:

SAUDI ARAMCO FORM-175 REPLACES: 10/26/2011 IR010200 1 of 2

SCOPE: HIC Testing: Pressure Vessel Steels and storage tanks.

TEST AND INSPECTION PER: 01-SAMSS-016 & NACE TM0284-2003.

(1) VISUAL INSPECTION WITNESSING BY INSPECTOR (Note 1)

(2) CERTIFICATES / RECORDS TO BE CHECKED BY INSPECTOR
(3) CERTIFICATES / DATA TO BE PROVIDED BY VENDOR / SUPPLIER / MANUFACTURER
0010
0010
***
X
Pre-Fabrication/Production Requirements
Documentation Required for Bid Evaluation
Specification Details / Notes:
01-SAMSS-016, Appendix "A".

0020 X The steel mill HIC test certificate 01-SAMSS-016, Para.1.2.2, 1.2.3 & 1.2.4

0040 X X HIC Laboratory Approval The Chairman of the Materials and Corrosion Control
Standards Committee shall approve HIC Test Laboratories
(01-SAMSS-016, Section 6).

0020
0010
***
X X
In process inspection & test requirement
Test Specimen selection
Specification Details / Notes:
01-SAMSS-016, Para. 7.1 & Appendix "B", Section 5.

0020 X X Test Specimen preparation NACE Para. 5.2, 4.3 & 01-SAMSS-016 Figure 3: Inspector to
verify sample and mark for trace ability.

0030 X Cleaning of Samples NACE Para. 4.4: Degreasing and rinsing.

0040 X X Test Solution and Reagents NACE Section 2; 01-SAMSS-016 Paragraphs 5, 6.3 and 6.4,
Appendix "B", Section 2, Figure 3.

0050 X X Testing Apparatus NACE Section 3 & Figure 1 and 01-SAMSS-016, Para. 6.3,
Figure 3, Appendix "B"; Para. B.2.3. (see the note 3)

0060 X X X Control Sample Control Sample shall be used to validate the test.
01-SAMMS-016, Para 6.2 & Appendix "B"; (see note 4)

0070 X Specimen Orientation in Test Bath NACE Section 6 & Figure 10: Placed in test vessel with wide
effaces vertical and separated from the other samples by 6 mm
on all sides.

0080 X X Ratio of volume of Solution to Surface Area of Specimen NACE Para. 6.1: Shall be a minimum of 3 ml per cm2.

0090 X Nitrogen purge and flow rate NACE Para. 6.2.1 & 6.2.2: Purged for one hour, at a rate of at
least 100 ml per minute, per liter of test solution.

0100 X H2S Purge and flow rate NACE Para. 6.2.1 & 6.2.3: Bubbled through the test solution
entered from the bottom of the bath. (see note 5)

0110 X X Temperature and PH NACE Para. 6.3 & 6.4: temperature of the test solution shall be
25#3#C. pH as per the requirements associated with solution A.

IR010200 Continued...
INSPECTION & TESTING REQUIREMENTS REVISION: 07/14/2012 CODE NUMBER: PAGE:
SAUDI ARAMCO FORM-175 REPLACES: 10/26/2011 IR010200 2 of 2
(1) VISUAL INSPECTION WITNESSING BY INSPECTOR (Note 1)
(2) CERTIFICATES / RECORDS TO BE CHECKED BY INSPECTOR
(3) CERTIFICATES / DATA TO BE PROVIDED BY VENDOR / SUPPLIER / MANUFACTURER
0120 X X H2S concentration (Iodometric Titration Method) NACE Para. 6.2.3 Appendix C; 01-SAMSS-016, Para. . 6.4: As
a minimum shall be 2,300 ppm.

0130 X X Test Duration NACE Para. 6.4: Test duration shall be 96 hours. The test time
shall begin immediately upon completion of the initial 60-minite
H2S introduction period.

0030
0010
***
X X
Final inspection & test requirements
Evaluation and Acceptance Criteria of Test Specifications
Specification Details / Notes:
01-SAMSS-016, Para. 7, & Appendix "B" Section 7, figure 2.

0020 X X Reporting Test Results 01-SAMSS016, Appendix "B", Section 8.

0040
0010
***
X
Additional/Supplemental Requirements
Safety Requirements
Specification Details / Notes:
NACE TM0284 Appendix "A".

0020 X X Safety Procedure and Work Instructions see note 6

Notes:
(1) May only be waived by the responsible Saudi Aramco, ASC, and AOC Inspection Offices.
(2) See form IR000003 for instructions on using this form.
(3) H2S in gas Cylinders is the only acceptable practice for generating H2S (Purity shall be 99.5% minimum). The used nitrogen shall be minimum
industrial grade, 99.5% pure.
(4) The control samples shall be provided by the manufacturer / vendor and demonstrate a CLR of at least 20% in solution "A" for the test parameters
to be considered acceptable, only after this shall the actual specimens be evaluated.
(5) The rate of bubbling shall be at least 200 ml per minute, per liter of test solution for at least 60 minutes; thereafter a positive pressure maintained
for the reminder of the test of H2S gas.
(6)Adequate ventilation, permanent H2S monitors located by the entry door and inside near the test setup (near ground level), alarm system with
flashing light and horn, gas masks with either oxygen or proper cartridges, and safe disposal of spent solutions and chemicals.

End of IR010200