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20
C H A P T E R

Aerospace Applications of
Radiographic Testing1

Lisa Brasche, Iowa State University, Ames, Iowa


Donald J. Hagemaier, Huntington Beach, California
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PART 1. Film Radiography of Aviation


Components

Radiography inspection plays a critical missiles and the beginning of the space
role in the life cycle management of shuttle program. These advances placed
aviation components with applications new demands on radiographic testing.
during production and service. Initial
applications of radiography to aerospace
inspections occurred over 50 years ago.
During the years from 1955 to 1965, the Automated Inspection5,6
aircraft industry produced the first Computers are used in all aspects of
commercial jet transports with expansion inspection, for data gathering, processing,
in the aerospace field to ballistic missiles, transmission and storage. Automation of
research rocket aircraft and the beginning radiographic testing can take any of
of manned space flight. The rapid growth several forms.6
in engineered systems placed new
demands on nondestructive testing.2,3
Initial routine applications used
radiographic testing to check castings and FIGURE 2. Radiograph showing corrosion in bonded
weldments for discontinuities as part of honeycomb.
fabrication quality control.4,5 Many small,
lightweight aluminum castings were
inspected semiautomatically by
fluoroscopy. Nationally, commercial
aircraft and military aircraft were Water filled honeycomb cells
periodically X-rayed to detect fatigue Corrosion in honeycomb
cracks (Fig. 1) and corrosion (Fig. 2).
Lightweight portable X-ray machines were
not available at this time, which required
specialized designs like the boom
mounted, mobile X-ray unit (Fig. 3) that
allowed placement of the X-ray source in
the proper position for each exposure. It
was especially useful for radiography of
wings and empennage structures. In the
1970s, the aerospace industry was
engaged in the moon projects, wide body
commercial transports, research and
military satellites, advanced ballistic FIGURE 3. Mobile X-ray system.

FIGURE 1. Radiograph showing cracks at door corner.

Skin crack

End of titanium crack

Frame crack

Jamb crack

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1. Radioscopic inspection may take place 203 mm (8.0 in.) wide, at a 1.22 m
in assembly lines for mass production (48 in.) source-to-film distance. Table 1
of components, such as printed compares the techniques used.
circuits, that are later integrated into In-motion radiography has also been
aircraft. used for liquid hydrogen tanks in solid
2. Robotic inspection calls for rocket motors (Fig. 5).
programmed control of test object
position, including loading into,
orientation with and offloading from
test system. Flight Test Aircraft
3. Automatic inspection involves Inspection7
programmed manipulation and
indexing of source or sensor system Applications also include a nondestructive
components relative to a test object testing unit to perform inspections of
in situ. flight test passenger jet aircraft. To address
issues that arise with performing
nondestructive testing in the field, such as
In-Motion Radiography5 the transportation of equipment to the
job, a mobile laboratory was designed
Applications of radiography have involved specifically to house portable equipment
inspection in support of the manufacture and to serve as an X-ray film processing
of intermediate range ballistic missiles. A darkroom. The system was used for
major problem is to provide techniques inspection of jetliners and military
for the X-ray inspection of large tank aircraft. An elaborate, accelerated test
weldments — imperative to meet schedule program was undertaken during the flight
requirements for reliability, to make test phase of the passenger jet in 1957.
timely delivery of missile components and
to keep costs commensurate with those of
an average product development.
In-motion radiography of weldments FIGURE 4. In-motion radiography of welded steel tanks:
in one case has required that an X-ray (a) schematic; (b) photograph.
facility be built and special equipment
(a)
designed or purchased. In the absence of travel
riage
packaged strip film, engineers have tion of car
Direc
designed and built a machine to cassette
70 mm roll film. The technique consists Weld
of placing two rod anode X-ray tubes on a Aft X-ray tube with
boom and porting the X-rays through an restricted aperture
aperture that projects a narrow beam to
the longitudinal welds of the tank. The
welded tank was placed on a carriage that
rode a track anchored on the floor of the Forward X-ray tube
exposure room (Fig. 4). An electrical with restricted
variable speed drive propelled the carriage aperture
Weld
and tank along the track at a speed of
0.15 m·min–1 (0.5 ft·min–1). 70 mm (2.8 in.) strip
Simultaneously, the three longitudinal film outside shell
weldments were exposed to the X-ray
beams.
Two 150 kV X-ray units were used to 70 mm (2.8 in.) film
reduce the exposure time by half. One outside three welds
tube was located at the end of the boom
(b)
and a second was located half the tank
length behind it. With this arrangement,
it was necessary to propel the tank only
half its length to obtain complete
exposure of the three longitudinal welds.
The aft X-ray tube was positioned inside
the boom to compensate for the two
different tank lengths. The carriage drive
mechanism and X-ray machines were
synchronized to operate simultaneously
when the start button was pushed in the
control room. Three lead ports were used
to restrict the X-ray beams to the three
longitudinal welds. The slits in the port
ends were 3.2 mm (0.13 in.) long and
25.4 mm (1.00 in.) wide, producing a
beam 25.4 mm (1.00 in.) long and

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TABLE 1. Comparison of techniques used for in-motion radiography of longitudinal welds.


Distance from Focal
Thickness
______________ Length
____________ Point to Sensor
Voltage Amperage ___________________ Travel
__________________
Material mm (in.) m (ft) (kV) (mA) m (in.) mm·s–1 (in.·min–1)

2014 aluminum 9.53 (0.375) 6.1 (20.0) 90 15.0 1.22 (48) 2.5 (6.0)
2014 aluminum 9.53 (0.375) 4.6 (15.1) 90 15.0 1.22 (48) 2.5 (6.0)
4340 steel 2.29 (0.090) 3.7 (12.1) 150 3.5 0.46 (18) 1.7 (4.0)
4340 steel 1.65 (0.065) 2.0 (6.6) 140 3.5 0.46 (18) 1.9 (4.5)
4340 steel 3.81 (0.150) 4.3 (14.1) 160 4.0 0.51 (20) 1.5 (3.5)

The equivalent of 40 to 120 years of


endurance (depending on the type of FIGURE 5. In-motion radiography of liquid
operation) under simulated service loads hydrogen tanks: (a) X-ray tube, collimating
was imposed on the test specimens. In slit and drive mechanism; (b) film transport
this way, damage propagation rates and mechanism for stop frame radiographic
failsafe characteristics of the structure system used on forward dome.
were studied under deliberately prolonged
exposures to fatigue beyond that (a)
permissible in actual service. From this
information, the company decided what
areas to survey with nondestructive
testing.
The passenger jet was X-rayed to
ascertain that all extraneous material
(debris) had been removed from all
control surfaces — ailerons, flaps,
elevators, rudder and vertical or
horizontal stabilizers. It required 480 films
of 360 by 430 mm (15 × 17 in.) each to
cover the necessary areas. The airplanes
were then turned over to a testing
division for evaluation and certification.
In flight tests aircraft were subjected to
stress levels above those normally (b)
encountered in regular service. Hence, all
critical areas were periodically surveyed
100 percent. The technician placed the
film on one side of the vertical stabilizer
and then moved the bucket to the
opposite side to make the exposure
(Fig. 6).
The closed areas and control surfaces of
jet aircraft are also radiographed for debris
or discontinuities as part of final assembly
inspection. Figure 7a shows the placement
of 360 by 430 mm film over the structure
to be inspected. The X-ray source is
positioned to expose a large area of the
assembly, as shown in Fig. 8. The film is
read and discrepancies are reported. The
area is opened up and the debris is
removed and compared with the object
indicated by the film images. Typical
debris includes tools, springs, wire clips, and workmanship errors consisting of
flashlights, nuts, bolts and paint brushes. inadequate rivet shank-to-hole fit and
Routine inspection for fabrication short hole-to-edge distances. Radiographs
errors or discontinuities in closed areas is of aircraft structure contain a wide range
accomplished simultaneously with the of densities and complicated geometrical
debris survey. Defective areas are reported images.
and corrective action is implemented. Aircraft X-ray inspection can readily
Film evaluation and corrective action are locate the following discrepancies: cracks,
performed in the shortest possible time. corrosion, double drilled holes, oversized
The radiographs may show both debris holes, short hole-to-edge distances, loose

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rivets and loose hardware. It is also used adjustable aperture for controlling the
to check for missing assemblies and used radiation pattern and hence the
for general inspection of closed areas. unsharpness gradient necessary for
blurring of all preselected details nearest
to the radiation source without causing
unsharpness of the image surface adjacent
Composites to the film. The focal-to-film distance was
Radiographic testing has found various established at 910 mm (36 in.). The
applications in the inspection of optima in definition, area coverage,
engineered materials such as composite radiation potential and speed of travel
laminates.4,8-10 were considered in determining the
focal-to-film distance for brazed
honeycomb. The X-ray exposure was
Brazed Honeycomb Structures accomplished by controlled linear
In the 1960s in-motion radiographic movement of the brazed assembly across
inspection of brazed honeycomb the area of radiation emitted by the
structures was developed for military stationary collimated X-ray source (see
aircraft. A radiation collimator was Fig. 9).
designed and fabricated with an

FIGURE 8. Position of X-ray source to expose maximum area


FIGURE 6. Radiographic inspection of aircraft of structure being radiographed.
stabilizer.

FIGURE 9. In-motion radiography facility for brazed


honeycomb structure.
FIGURE 7. X-ray film placement on vertical stabilizer for debris
and structural inspection.

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The fine grained, high contrast film radiograph showing only the brazed fillets
was cut in widths of 300 mm (1 ft) and on the film side (single surface) of the
varied in length. Cassettes to panel. It is much easier to detect lack of
accommodate the various lengths of X-ray braze and to measure the fillet width on
film were designed and fabricated from a the latter radiograph.
special plastic material suitable for
radiographic work. The plastic cassettes Helicopter Composite
were secured in intimate contact with the
honeycomb panel by precut lengths of Rotor/Propeller Blades11
magnetic rubber strips placed on the Significant performance improvements in
cassette and magnetically attached to the rotor/propeller blades were realized by
honeycomb panel. proper use of composite materials. From
In all phases of the operation, 1954 to 1962, intensive research into
in-motion radiography was less time materials and fabrication techniques were
consuming than conventional performed and backed up by component
X-radiography. The ease of operation and sample fatigue testing. The successful
was particularly noted in the use of fiber reinforced composite materials
interpretation of the radiographs. in helicopter rotor blades leads naturally
Figure 10a is a conventional (still) to an improved capability for a successful
radiograph showing brazed fillets on the V/STOL propeller design.
source and film side (double surface) of To fully appreciate the enormity and
the panel. Figure 10b is an in-motion importance of the nondestructive
inspection to be done, one must be aware
of the types of loads that rotor blades bear
and the general construction of the blade.
FIGURE 10. Brazed honeycomb structure: Rotor blades in service are subjected to a
(a) conventional (not moving) radiograph of variety of static and cyclic loads. These
two surfaces; (b) in-motion radiograph of loads include beam, centrifugal, torsional
one surface. and flatwise and cordwise bending.
(a) One of the most important tasks in the
use of composites is the development of
the nondestructive testing capability to
ensure that the hardware to be tested is of
known quality. Some of the most
challenging efforts come not in the
selection of nondestructive test technique
to use but in the mechanism necessary for
practical application of that technique to
the complex structure of a rotor/propeller
blade. Figure 11 shows a concept of the
automated penetrating radiation
inspection equipment provided for an
X-ray sensitive vidicon and image
intensifier presentation. The system was
basically a mobile X-ray unit in which the
blade is fixed within two tracks and the

(b)
FIGURE 11. X-ray structure sensitive vidicon
and image intensifier system concept.

Blade
Camera

Handling equipment Television


monitor

Control console

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enclosed generator-and-detector system


traverses the length of the rotor blade.
The X-ray vidicon image was presented
on a remote 430 mm (17 in.) video screen
at about 30×. The image amplification
system also presented a view on the same
screen at 1:1. The viewing area using the
vidicon tube was about 13 by 13 mm
(0.5 × 0.5 in.) with 1 to 2 percent image
quality indicator sensitivity whereas the
viewing area of the image amplifier is
about 200 × 200 mm (8 × 8 in.) with 3 to
4 percent image quality indicator
sensitivity.
Both the X-ray generator and pickup
tubes had free 90 degree movement to
allow for selection of the viewing angle
that proved to be most desirable. Viewing
speed was variable, the maximum speed
being limited by interpreter perception.
All controls and viewing apparatus were
remote. Figure 12 shows some
photographs taken of the video screen
showing various conditions and
discontinuities.

FIGURE 12. Typical vidicon monitor presentations: (a) image


of honeycomb structure; (b) cell wall fracture and separation;
(c) cell structure deformation; (d) cell wall separation.
(a) (c)

(b) (d)

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PART 2. Radiographic Testing of Space Flight


Components

times to cover the full length of each


Solid Propellant Rocket weld. The cylindrical section welds, or
tank welds, were similarly radiographed.
Motors
Large Rocket Motors
Saturn Fuel and Oxidizer Tank During a time of international tension in
Weldments the 1950s and 1960s, solid propellant
During the early 1960s, many engineering rockets became an important part of the
talents were applied to the National United States arsenal. These missile
Aeronautics and Space Administration’s systems consisted of ground, air and
efforts for manned space flight. This submarine launched vehicles. They were
included fabrication of 6.7 m (22 ft) used in intercontinental and intermediate
diameter tanks for the Saturn moon range missiles, where high performance
rocket (Fig. 13). The weld joint and immediate readiness were required.
configuration for the SIV-B is illustrated in Discontinuities in the propellant and
Fig. 14. Initially, the in-motion technique propellant-to-liner joint affect the
using the welding fixture was used on the performance, reliability and safety of
dome welds but was discontinued because these motors.
smooth movement of the fixture was not Radiography of large, 0.75 to 1.5 m
achieved. The conventional techniques (2.5 to 5 ft) diameter, solid propellant
located a 100 kV beryllium window X-ray motors can be accomplished in several
tube on a fixture inside the dome.12 About ways. If the central perforation is of a
1.2 m (4 ft) of extra fine grain film was design that permits the insertion of a
covered in each exposure. Circular dome cassette, radiography can be accomplished
movement was used between exposures to with a 2000 kV X-ray source or a
align each of nine segment welds with the cobalt-60 gamma ray source located on
X-ray beam. In Fig. 15, the operator is the exterior and the film placed inside the
placing 70 mm (2.8 in.) strip film over motor (Fig. 16a). If the motor design does
each weld. After the nine films are not permit the insertion of a cassette,
exposed, the operation was repeated three then radiography can only be
accomplished by radiation penetrating the
entire unit (Fig. 16b). For thicknesses
greater than 760 mm (30 in.), X-ray
FIGURE 13. Liquid propellant rocket engines energies above 2 MeV are required.
used to launch Apollo Saturn moon rocket. Therefore, most of the earlier work was
done with 10, 22 and 31 MeV betatrons.13
In the 0.5 to 6 MeV range, the van de
Third stage
graff and resonant transformer types of
X-ray equipment were capable of
providing the intensity and penetrating
power necessary for high quality
radiography in propellant thickness range
up to 760 mm (30 in.). Above about
Second
stage
5 MeV, however, and for heavier
propellant sections, these two direct
acceleration techniques became
impractical. In their stead, the betatron
and microwave linear electron accelerator
(linac) were required. The radiation
output from betatrons is in the 25 to
Booster
stage
50 mC·kg–1 (100 to 200 R) per minute
range, whereas the linear accelerator
radiation output ranges from 130 mC·kg–1
to 2.5 C·kg–1 (0.5 to 10.0 kR) per minute
and can thus rapidly radiograph thick
propellant sections as illustrated in
Fig. 17. High energy equipment was
developed in the 1950s.14

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FIGURE 14. Weld joint configuration for Saturn SIV-B rocket.

Fittings Flange and center plates

Meridian seams on forward


and aft dome and common
bulkhead face assembly

Tank assembly and Cylindrical tank


forward cylindrical longitudinal seams
tank rings

Seal weld

Tank assembly and


aft cylindrical tank rings
Common bulkhead and
liquid oxygen tank
assembly

MOVIE. FIGURE 15. X-ray technician placing film on FIGURE 17. Exposure thickness data for
Automated dome segment welds before radiographic propellant at various X-ray energies.
inspection of inspection.
rocket motor. 1000

B
100
Exposure time (min)

C
10

1.0

FIGURE 16. Radiography of solid propellant 0.1


rocket motors: (a) single-wall radiography; 0 0.5 1.0 1.5 2.0
(20) (40) (60) (80)
(b) double-wall radiography.
(a) Film Propellant thickness, m (in.)
Liner
Legend
A. 2000 kV peak at 1.5 mA
Film Source B. 10 MeV betatron at 7.0 Sv·min–1 (700 R·min–1)
Propellant C. 22 MeV betatron at 1.4 Sv·min–1 (140 R·min–1)
D. 10 MeV linear accelerator at 10 Sv·min–1
(1000 R·min–1)
Film
(b) Film

Film

Source

Film

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at over 160 km (100 mi) above sea level. It


Jet Engine Inspection14,15 is apparent that the quality reliability of
these small engines must be ensured for
On-aircraft, periodic gamma ray the intended mission of the spacecraft. An
inspection of jet engines is used for illustration of the type and number of
detection of compressor and turbine blade motors in the Gemini vehicle is shown in
damage, including hot gas damage of Fig. 20.
burner cans. Possibly one of the greatest The radiographic testing of ablative
assets of the inspection is the ability to materials has revealed various
judge turbine blade alignment. The discontinuities, such as delaminations,
flexible isotope guide is inside a rigid porosity, cracks and resin rich or resin
aluminum tube and inserted through the starved bands. Detail parts inspection
axial engine drive shaft to a revealed discontinuities similar to those
predetermined distance. The iridium-192 found in the billets. These discontinuities
source is stopped at the selected were undetected because the original
longitudinal locations along the engine billets were not radiographed or were
axis, as illustrated in Fig. 18. The film is improperly radiographed. Tangential
placed on the outside of the area to be radiographs also revealed case-to-ablative
inspected. The film (as shown in Fig. 19a) adhesive voids and porosity.
is evaluated for evidence of excessive Tangential radiographic inspection of
wear, misalignment or other the case-to-ablative bondline is illustrated
unsatisfactory conditions. Figure 19b, in Fig. 21. Measurement of the film
photographed after engine disassembly, density at an interface is not possible
shows that a stator blade had worn its slot unless a separation of 0.75 mm (0.030 in.)
excessively and the resulting vibration or greater exists, because the minimum
had caused a crack in the retainer ring. If aperture on a standard densitometer is
not detected, the resulting internal 0.75 mm (0.030 in.). Measurements of
damage to the engine can cause complete gaps less than this require an automatic
failure. scanning microdensitometer.
It was found generally that the X-ray
absorption of most adhesives was very
low, causing interpretation problems of
Small Ablative Thrust case-to-ablative and other bond joint
Chambers16 interfaces. Thick or thin bond joints
Silica phenolic materials have been used yielded different radiographic results that
extensively in the manufacture of exhaust were difficult to interpret. To compensate
nozzles for solid propellant rocket motors. for the problem, a small percentage of
In this particular application, the material antimony trioxide was added to the
must withstand high intensity, short time adhesives. This material did not affect the
ablation and erosion. In spacecraft cohesive bond strength but made the
engines for Gemini or Apollo, however, joint more opaque to X-ray and bondline
the motor is pulse fired at intervals discontinuities became more apparent by
throughout the mission to a total revealing the presence of adhesives as
accumulated time of 10 to 20 min. The illustrated in Fig. 22.
hypergolic engines are designed to The verification of delaminations and
produce from 111 to 445 kN (25 to location of leakage paths was proved by
100 lbm) of thrust in environments found radiographing various specimens and

FIGURE 18. Iridium-192 gamma ray inspection of jet engine.

Sixteenth stage exit guide vanes Film around engine circumference


Spherical gamma ray emission

Isotope iridium-192

Film around engine circumference Sixteenth stage exit guide vanes

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FIGURE 19. Gamma radiography of vane FIGURE 21. Tangential radiographic technique for case bond
segments in jet engine: (a) gamma using a microphotometer: (a) setup; (b) recording.
radiographs; (b) visual crack indication
previously revealed by gamma ray (a) (b)
inspection of vane guide.
X-ray focal point Brush pen recorder
(a)

X-ray
Microphotometer
response from
Light tangent radiograph
Motor meter
Film tangent Film motion
Light
image
source

(b)
FIGURE 22. Case-to-ablative bond
discontinuities are revealed by radiopaque
additive in adhesive: (a) first image;
(b) closer image.
(a)

FIGURE 20. Gemini vehicle space engines.


Sixteen 11 kg (25 lbm) engines
Four 45 kg (100 lbm) engines
Two 39 kg (85 lbm) engines (b)

Two 45 kg
(100 lbm)
engines

Eight 11 kg (25 lbm) engines

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motors before and after soaking in X-ray testing. After inspection, the chamber is
opaque solutions. Different solutions were returned to the cell for further testing.
tried but the one yielding the best results The prime factor of discovering
was a concentrated water solution of lead discontinuities when they occur and
acetate and lead nitrate. All delaminations before they can lead to failure is missed
and leakage paths were detected after a by this technique of using X-ray image
1 h soak period and rinse (Fig. 23). Motors equipment in conjunction with motion
showing delaminations and leakage paths picture film. Sequencing of the thrust
were rinsed thoroughly with deionized chamber image during hot firing will
water to remove most of the lead solution ensure that complete failure analysis data
and were then dried and pressure are obtained.
impregnated with resin. Reradiographing Cinefluorography has been used
after resin impregnation usually indicated successfully to establish the mode of
that the void was filled, thereby making failure in small solid propellant rocket
the part acceptable for use. Motors engines during hot firing.18 A similar
repaired in this way were hot fired study on solid propellant rocket engines
successfully, indicating the adequacy of was reported.13 Cinefluorography of solid
the repair procedure. propellant engines reveals the flame front
pattern and burning rate as a function of
Video Radioscopy and X-Ray contrast differential in the test object. The
failure analysis of liquid hypergolic
Image Intensifier Tests17 ablative engines by cinefluorography is
The normal technique of inspecting small more concerned with the detail resolution
ablative thrust chambers requires that of discontinuities as they develop in the
each chamber be radiographed before hot test object.
firing and also at subsequent intervals The equipment consisted of a
during the test program. This plan entails fractional focus X-ray tube, full wave
disassembly of the chamber and shipping rectified voltage transformer, X-ray
it to the X-ray laboratory for radiographic control panel, high gain, image intensifier
tube and an optical system for viewing.
Additional accessory equipment can be
used for special purpose applications.
FIGURE 23. Soaking in saturated solution of Such equipment consists of a 16, 35 or
lead acetate and lead nitrate: (a) before 70 mm motion picture camera capable of
soaking; (b) after soaking. 7.5, 16, 30 or 60 frames per second
(a) (Fig. 24a). In this way, cinefluorographic
time lapse studies may be made of
systems while functioning. Such studies
may include the analysis of small solid or
liquid propellant engines during hot
firing. Other techniques include the use of
a television camera (kinefluorography) in
place of the positive print and

FIGURE 24. Comparison of cinefluorography


and kinefluorography: (a) cinefluorography,
direct photography of output phosphor of
image intensifier tube; (b) kinefluorography,
photography of picture tube image of
output phosphor.
(b)
(a)
Image intensifier tube
Film
Optics

(b)
Image intensifier tube Display tube
Film
Optics

Television
camera
tube

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transmitting the image to a television per minute. The turntable can be elevated
monitor (Fig. 24b). and depressed over a 250 mm (10 in.)
An X-ray image intensifier system has travel. It can be positioned within about
proved successful in determining the 100 mm (4 in.) of the input phosphor for
mode and sequence of failure of ablative best detail resolution of as far as 760 mm
thrust chamber during actual firing. (30 in.) away for direct geometric
Delaminations, bond joint separations magnification. A horizontal travel of
and cracks were readily detected in test 250 mm (10 in.) transverse to the X-ray
materials and assemblies. A high gain beam also is provided. The X-ray tube
X-ray image system was installed at the head itself can be traveled horizontally to
Rocketdyne test facility for hot fire provide a range of 150 to 760 mm (6 to
studies. Excellent results were obtained 30 in.) from the input phosphor. This
using a 150 kV, 4 mA, 0.3 mm (0.012 in.) range permits the use of very high
fractional focus X-ray tube in conjunction radiation intensities at short focal lengths
with a 230 mm (9.1 in.) diameter, high or improved image sharpness at greater
gain image intensifier. focal length, as different test problems
Radiographic results of a chamber fired dictate.
to failure are shown in Fig. 25. Test results In selecting parameters for a specific
of the failure mode were recorded on test, the technician first positions the item
16 mm motion picture film at 32 frames on the turntable and adjusts the
per second. electrically driven lead shutters to confine
Used as a process and quality control radiation to the area of interest. Then,
device during manufacturing operations, while observing the image tube, the
the X-ray image intensifier has many technician selects the geometric
applications involving direct viewing of relationship best suited for the test
the image tube. Thus, the cost of film and objectives. Next, the energy level (kV) is
the time involved for film processing are adjusted for the desired contrast and the
avoided. Unusual phenomena might be tube current (mA) is adjusted for
photographed with a positive print or brightness. The component then is
regular camera when required. Cylindrical scanned on either axis or is rotated, or
objects can be rotated through combinations might be used. When a
360 degrees during viewing; in film significant anomaly is observed, it can be
radiography, they would likely have to be recorded in a variety of ways for later
X-rayed in two exposures at 90 degrees. observation.
Confidence in the detection of A functional multienvironmental
discontinuities is greatly improved by the fluoroscopic facility has been used for the
360 degree scan. evaluation of valves, switches, actuators
Parts to be inspected are placed on a and other components. The system can
130 mm (5 in.) turntable capable of reveal the operation of internal
supporting and rotating a 23 kg (50 lbm) components under various dynamic and
assembly in either direction at 1 rotation environmental conditions expected to be
encountered during flight. The
temperature and pressure of the
inspection chamber can be varied to meet
FIGURE 25. Ablative thrust chamber: (a) before firing; environmental requirements. A general
(b) after firing. view of the test room and inspection
(a) (b) cabinet is shown in Fig. 26a and the
control console and X-ray image monitor
are shown in Fig. 26b. Radioscopic results
can be seen on the monitor and images
are recorded on video media that provide
Case separation playback capability for the system
engineers responsible for analysis of each
Delamination component tested.
separations
Bond joint separation

Large Liquid Propellant


Rocket Engines19-21
Throughout the modern era of rocketry,
liquid propellant rocket engines have
demonstrated their ability to provide high
performance, high reliability and
operational flexibility. It is mandatory to
have highly reliable launch vehicles.
The engine reliability program begins
with design and manufacture to ensure

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accurate, high strength, failure free procedures have been developed for
hardware. Extensive inspection procedures unique problems as indicated in the
further assist this phase. Engine following paragraphs.
component testing follows inspection and
finally the liquid propellant rocket engine
can be subjected to extensive testing in
the development phase to uncover any Neutron Radiography of
potential weakness. This extensive test Special Aerospace
effort provides a high degree of
confidence in the engine reliability. Components
Liquid propellant rocket engines also Typical aerospace items that have been
provide the capability of testing the article neutron radiographed include jet engine
that will be used during the actual launch.
Also, each engine is tested before it is
delivered to the customer and later each FIGURE 27. Apollo space vehicle booster engine, 6.67 MN
stage and engine is tested as a unit and (1.5 × 106 lbf).
completely checked out before the
launch. Fig. 27 shows a completed engine.
Five of these 6.67 MN (1 500 000 lbf)
thrust engines were used on the manned
Saturn moon rocket booster stage.19
Radiography is used to detect internal
discontinuities in weldments and high
strength castings, to determine braze alloy
distribution in brazed thrust chambers
(Fig. 28) or components and to internally
inspect electrical assemblies for missing or
broken components. Special radiographic

FIGURE 26. Functional multienvironmental fluoroscopic


system: (a) installation; (b) control console.
(a)

FIGURE 28. Radiographic testing of thrust


chamber tube-to-tube braze joints:
(a) technique setup; (b) positive prints of
radiographs, arrows marking indications.
(a)

Braze joints

(b)

(b)

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turbine blades, adhesively bonded have a high neutron scatter rate, a


honeycomb and laminates, ordnance or neutron radiograph will image gaps,
pyrotechnic devices, flight controls and cracks, low density areas or other
metal assemblies containing nonmetal discontinuities that could prevent normal
O rings or seals.22-24 Inspection of such operation.
parts is possible because neutron A neutron radiograph will image
radiographic testing can detect certain low certain materials of low atomic number
density materials through heavy metal whereas the X-radiograph does not. The
sections. powder train inside an explosive device is
Attenuation of X-radiation is well defined in the neutron radiograph,
determined largely by the electron density for example, but is not shown in the
of the material being examined, so that X-radiograph. Hence, neutron
thicker and/or denser materials appear radiography has played a major role in
more opaque. Neutrons undergo two yielding a no failure reliability for
main types of reactions with atomic ordnance devices in aerospace programs.
nuclei: absorption (capture) and
scattering. The mass attenuation Adhesive Bonded Composite
coefficient for thermal neutrons is thus a
function of both the scattering and Structures27
capture probabilities for each element; the Thermal neutrons are highly attenuated
density of a particular material or by boron and hydrogen atoms. Therefore,
component is a poor predictor whether it when an adhesive bonded laminate or
will be relatively transparent or opaque to honeycomb specimen is neutron
the passage of neutrons.25 radiographed, the hydrocarbon adhesive
High attenuation coefficients for becomes very apparent because of its high
thermal neutrons are exhibited by neutron scatter. This condition is reversed
hydrogen and boron. Hydrogen has the for X-radiography where metal
highest scattering coefficient whereas components are high attenuators. A high
boron, cadmium, samarium and density boron fiber composite would be
gadolinium have unusually high neutron completely opaque to a thermal neutron
capture probabilities. For this reason, beam, as shown in Fig. 29.
hydrogenous or boron containing In Fig. 29, specimens have aluminum
materials being inspected by neutron honeycomb cores with adhesive bonded
radiography can be seen or delineated skins of graphite epoxy, boron epoxy and
from other elements in many cases where fiberglass.
X-radiography is inadequate. It is thus
possible to expose a specimen (for
example, a hydrogenous or borated
explosive or a fuel sealed in a metallic FIGURE 29. Attenuation in adhesive bonded, aluminum
container) to a beam of thermal neutrons honeycomb core, fiber matrix facing sheet, composite
and to project an image having excellent specimens: (a) low kilovoltage X-rays; (b) thermal neutrons.
resolution and contrast, thereby
distinguishing between the charge
material and its container while revealing (a) (b)
any imperfections in the specimen.
Similarly, neutron radiography permits
detection of hydrides,26 which can cause
hydrogen embrittlement in welds and can 1 1
be used for nondestructive testing of
ordnance (explosive) devices to determine
the relative density of the charge material
and/or the presence of voids or cracks.
2 2
Explosive and Pyrotechnic Devices
One of the important applications of
neutron radiography is the quality control
of certain critical explosive devices, such
75 mm 3 3
as pilot seat ejection cartridges, (3.0 in.)
detonating cords and pressure cartridges
for aerospace applications. These devices
normally contain explosives or
propellants of low atomic numbers. In 125 mm (5.0 in.)
most instances, they also have metal
housings. Therefore, it is nearly Legend
impossible to inspect them effectively 1. graphite
with postassembly X-ray examination. 2. boron
However, because hydrogenous materials 3. fiber glass

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reactivity of molten titanium. Ceramic


Investment Castings materials used to produce face coats for
the investment casting of titanium must
Investment casting, also known as the lost be stable and have low reactivity with
wax process, is a manufacturing method molten titanium. If the ceramic face coat
used to produce near net shape metal materials are reduced by the molten and
articles. A wax pattern is produced by solidifying titanium a type of brittle,
injection molding into a die cavity oxygen enriched titanium called alpha
typically machined into aluminum. The case is generated. The amount of alpha
die cavity replicates the desired casting case produced on a casting must be
shape. After molding, the wax pattern is limited as mechanical properties are
dipped into a series of slurries that negatively affected. This in turn restricts
contain ceramic particles. Multiple the candidate ceramic face coat materials
coatings of ceramic slurries are applied to that can be used.
build a sufficiently thick mold layer. The
dip layers are allowed to dry and harden
between applications.
The first layer of the mold is referred to
as the face coat, important because it is in
contact with the molten metal and
determines the quality of the casting.
Subsequent layers are referred to as backup
layers. After sufficient layers have been
applied, the wax is melted from the shell,
leaving a cavity whose shape is an exact
replica of the desired metal article.
The ceramic mold is sintered to make it
denser and stronger. Metal is then melted
and poured into the mold. After
solidification and cooling, the ceramic
shell is removed leaving a metallic casting
of the same geometry as the wax pattern.
After shell removal, the casting is
nondestructively tested to reveal
inclusions of mold material. These
discontinuities are removed by grinding
and subsequently repaired by welding.
Investment casting has been used to
produce precise, high quality aerospace
engine components that range from 0.1
to 1.2 m (a few inches to several feet) and
are cast in a variety of alloys including
steel, nickel, cobalt and titanium.

Titanium Castings for Aerospace


Structures
Airframe manufacturers have been
exploring the use of titanium investment
castings to replace components
traditionally produced from forgings.
Titanium investment castings in these
applications reduce weight, costs and lead
time. The fatigue driven, fracture critical
environment of these aerospace structures
requires a quality level higher than
necessary for titanium castings in
aerospace engines. The design of these
fracture critical titanium castings is driven
by the ability to detect mold face coat
inclusions in the components. The
required thicknesses have challenged the
limits of radiographic testing.

Investment Casting of Titanium


The investment casting of titanium poses
several challenges due to the high

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PART 3. Techniques for Advanced Materials

In the decade from 1975 to 1985, the processed in automatic film processing
aerospace industry was busy launching equipment and special film reading boxes
the space shuttle,28 producing high have been fabricated, some of which
performance jet fighters, attack provide for viewing up to 1.5 m (5 ft) of
helicopters, missiles and satellites. film at one time. The assemblies are
Considerable work was accomplished in oriented with the honeycomb cells
developing fiber reinforced plastic parallel with the X-ray beam and the
composite aircraft structures. In the 1980s direction of motion is parallel to the
and 1990s, radiography, particularly X-ray ribbon direction.
based imaging techniques and
applications, saw tremendous growth.29 Composites
As with many technologies, advances in
speed of data acquisition/analysis were Figure 30 shows in-motion radiography
enabled by the improvements made in being performed on carbon to epoxy
computers and semiconductors. Advances composite upper wing skin. The
in digital radiography continue to affect composite skin is about 8 m (26 ft) tip to
the aerospace industry, with many tip and 1.8 m (71 in.) forward to aft at the
benefits leveraged from medical centerline. The stainless steel tool is
applications. The Air Force Research designed to manipulate the assembly in
Laboratory has served as a major funding five axes to permit orientation of the
source30-32 driving the development of all contoured surface perpendicular to the
three of the main components of a X-ray beam. The X-ray tube head has a
penetrating radiation system: a source of lead shielded cone attached to the port to
radiation, a manipulation system for the limit radiation onto a narrow line about
test object and a detector system. Air 13 mm (0.5 in.) wide in the direction of
Force Research Laboratory investments tube motion. The tube support is
have focused on improvements in mounted on the ceiling and has an
sensitivity with emphasis on cost effective extension up to 12 m (40 ft).
applications. Simulation tools have been a A more detailed view of the gooseneck
focus of work at several research tube support and in-motion cone is
laboratories.33,34 Recent aerospace shown in Fig. 31a. This figure shows a
applications are provided in the bonded honeycomb assembly with boron
remaining section. epoxy skins on 360 mm wide roll film
that is on 3 mm (0.12 in.) vinyl lead
backup material. The pendant control

Advanced Materials
FIGURE 30. In-motion radiography of composite wing skin.
Adhesively Bonded Honeycomb
Structures
In-motion fluoroscopic inspection of
metallic bonded honeycomb structures
has been done for years by several
prominent manufacturers.35,36 In-motion
radiographic techniques have been used
to inspect a variety of bonded honeycomb
structures. These structures are composed
of aluminum core bonded to either
aluminum, boron epoxy or carbon epoxy
skins. The inspections are performed to
detect crushed core, core node separation,
foreign objects, core splice discontinuities
and core tie-ins at closures.
A collimator is used to limit the X-ray
beam in the direction of motion. Roll
films of required lengths and 70, 120, 254
and 355 mm wide are used. The films are

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permits movement of the tube support in an electron focal spot smaller than
three directions. 0.1 mm (0.004 in.). In practice, focal spots
The control console for a representative from 0.002 to 0.25 mm (8 × 10–5 in. to
in-motion radiography system has the 0.01 in.) have proven to be useful for
standard X-ray control panel modified to radioscopic systems37 and spots from
provide kilovoltage slope control during 0.025 to 0.075 mm (0.001 to 0.003 in.)
the in-motion exposure (see Fig. 31b). As have proven satisfactory for film
many aircraft structures taper in thickness techniques using magnification.
from inboard to outboard, it is impossible A typical system might contain a
to maintain constant film density without 160 kV constant potential microfocus
adjusting X-ray parameters during the X-ray tube capable of continuous
in-motion exposure. Kilovoltage was operation at 0.5 mA with a focal spot size
chosen as the variable because it can be of 12 µm (5 × 10–4 in.). Using a 12 µm
changed to match energy level with the (5 × 10–4 in.) focal spot size, the system
thickness of the part. Another can resolve details as small as 25 µm
improvement in the in-motion control is (0.001 in.) without magnification. The
constant speed control, which system may also contain a 230 mm
automatically compensates for varying (9.0 in.) X-ray image intensifier optically
loads and maintains a constant speed coupled to a 15 MHz closed circuit
readout on a digital tachometer. The television fitted with a 25 mm (1.0 in.)
television monitor (Fig. 31b) displays the vidicon image tube. With low absorbing
area of the assembly being subjected to materials, projection magnification of 50×
radiation. It does not provide an X-ray or more may be obtained.
image but is used to aid in alignment of A useful technique that can be
the assembly. achieved with radioscopic projection
microfocus radiography is that of
zooming or dynamically positioning the
object with a manipulation between the
Microfocus Radiography X-ray tube and image receptor.38 In this
Normal radiography is accomplished technique, magnification is achieved
using 1 to 3 mm (0.04 to 0.12 in.) focal when the object is moved away from
spots. Projection radiography can be image receptor and toward the X-ray tube.
accomplished with a true microfocus Figure 32 illustrates a single integrated
X-ray source; that is, an X-ray tube with circuit that was initially situated for low

FIGURE 31. In-motion radiography: (a) gooseneck tube support and cone assembly; (b) control
panel.
(a) (b)

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projection magnification of 2×. The inspected, including cases, propellants,


integrated circuit was then zoomed liners and igniters (Fig. 34).
toward the X-ray tube through 10×, 50× The inspection system features a
and 250× magnification. It is evident that 420 kV X-ray source to inspect objects up
the higher the magnification, the more to 1 m (40 in.) diameter (Fig. 35). The
detail one can see on the video monitor. range of measurable signal levels
A similar test, done on a metal jet produced is about 106 to 1, superior to
engine turbine blade is shown in Fig. 33a that offered by alternative techniques at
and at 10× magnification in Fig. 33b. Jet the time of testing. The information is
engine turbine blade inspection using more complete, detailed and accurate and
radioscopic microfocus radiography has the computer sorted images can be
been performed for jet engine manipulated and analyzed by design,
manufacturers. The blades are inspected manufacturing and quality engineers or
for cracks, voids, inclusions and plugged stored for future reference.
cooling passages. Work has been completed for the
United States Air Force to develop and
implement an automated device to X-ray
inspect turbine blades and vanes.40 This
Computed Tomography radiographic inspection module uses a gas
Computed tomography (CT) combines ionization X-ray detector as the image
the capabilities of the computer with an medium. A computer processes the
X-ray source for the inspection and detector output signal to generate digital
analysis of the internal structure of X-ray images. Advanced image processing
objects. Very minor changes in density
can be accurately detected by a computed
tomography system. Ordinary film
radiography inspection systems have FIGURE 33. Microfocus radioscopic images:
some major weaknesses. One is that they (a) jet engine blade; (b) enlargement.
create only superimposed images of (a)
artifacts. The superpositioning of images
— lying one on top of another — distorts
the inspection results. Computed
tomography eliminates superposition by
examining an object in a series of cross
sectional slices from different views along
the length of the object.
A computer calculates an image based
on the information in all the slices and
reconstructs a two-dimensional picture of
a slice through the object. This precise,
highly accurate, two-directional data
package can be viewed on a cathode ray
tube screen, printed out in hard copy and
stored on optical or magnetic media.39
In the 1980s computed tomography
was developed for industrial applications.
Solid rocket motor components were
(b)

FIGURE 32. Microfocus radioscopic images of


integrated circuit.

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software, operates on these digital images detection of hydrogenous substances,


to make automated accept/reject such as moisture and corrosion in aircraft
decisions. The handling of the part during components. The advantage of neutrons
X-ray exposure is carried out robotically is that low atomic number nuclei, in
under computer control. particular hydrogen, have higher
To detect internal material and interaction cross sections than the
manufacturing discontinuities and to surrounding material. Figure 37 shows a
make inspection decisions, the computer neutron radiograph of an aerospace valve,
operates on two data representations, in which the O rings are clearly visible as
depending on the application. The first is light horizontal bands.
digital fluoroscopy, or digital radiography, A neutron tomography system
and results in a filmlike image (Fig. 36a). generally consists of an intense neutron
Digital fluoroscopy allows quick source, object turntable, a scintillator
identification of internal anomalies and screen, a mirror, a cooled charge coupled
other features of interest. The second is device camera, and computer imaging and
computed tomography (CT) and results in processing support. With such an
a cross sectional image (Fig. 36b). This arrangement, the actual distribution of
latter data format, although requiring materials across a given path can be
more time to generate, yields significantly determined.
higher material discontinuity sensitivity
and a better ability to resolve internal
anomalies such as thin wall
discontinuities. Computed tomography FIGURE 35. Computed tomography system.
provides additional geometric detail not
available with conventional film
radiography. Computer based X-ray
inspection is expected to yield significant
improvements in productivity, reliability
and sensitivity for airfoils. In addition, the
new industrial computed tomography
capability provides new inspection
capability and offers new freedom to
design engineers, allowing them to be
more innovative. Advanced
nondestructive testing techniques, like
computed X-ray tomography, will be a
key to the practical realization of
optimum designs.

Neutron Tomography
Neutron radiography has already proven
itself as a reliable method for the

FIGURE 34. Simplified illustration of computed tomography


for aerospace structures.

Data
Reconstruction
FIGURE 36. Digital images of turbine blade: (a) fluoroscopic;
Solid acquisition (b) tomographic.
propellant and
and
motor imaging
processing (a) (b)
Density for
each matrix Scarfs
element in
Detector
pixel
array
X-ray
energy
source

M pixels N pixels
Scarfs

Tomograph
image

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As aerospace and nondestructive test radiographic testing.43 The technique uses


engineers have become more familiar an electronically scanning X-ray source
with the capabilities of neutron and a discrete detector for radioscopic
radiography and tomography, the imaging of a structure.
techniques have been used more. Neutron The scanning source system has several
tomography systems have been used to advantages. Miniaturization of the
determine the hydrogen content in discrete X-ray detector enables easy
aircraft compressor blades41 and the exact positioning inside a complex structure
placement and shape of O rings in critical (such as an aircraft wing) allowing images
components of spacecraft (Fig. 38). of each surface of the structure to be
An Air Force Research Laboratory obtained separately. Additional
program42 was initiated to develop and advantages include multiple detectors that
evaluate advanced radiographic and enable the simultaneous acquisition of
radioscopic systems. To ensure broad data from several different perspectives
applicability to many aerospace without moving the structure or the
inspection needs, a diverse team was measurement system. This provides a
assembled consisting of commercial means for locating the position of
companies and government contractors. discontinuities and enhances separation
The program evaluates detectors that are of features at the surface from features
proven in other industries and that are inside the structure. Finally, the amount
fast and easy to use. To reduce reliance on of secondary scattered radiation
more costly film techniques and enhance contributing to the noise in the image is
inspection productivity, these detectors reduced compared to conventional
include large area, flat panel, X-ray radiography. Noise reduction facilitates
detectors modified from medical the acquisition and analysis of
applications, recently available dental quantitative data about the integrated
sensors and photographic industry digital material density along the ray path
charge coupled devices modified for between the source and the detector.
radiography. Details of the techniques and
application to crack detection in aircraft
structures have been published.43,44
Results are shown for different crack sizes
Reversed Geometry, in a range of thicknesses. Application to
Scanning Beam Technique honeycomb structures is also being
presented. A honeycomb specimen with a
The National Aeronautics and Space
fatigue crack in one of the face sheets was
Administration has explored a technique,
imaged with the scanned X-ray system. It
reversed geometry scanning beam
was shown that the variation in contrast
as a function of incident angle can be
used to remove some of the image clutter
FIGURE 37. Neutron radiograph of aerospace due to the effects from the underlying
valve. O rings are visible as light bands. honeycomb structure, thereby improving
the detectability of the crack. A

FIGURE 38. Neutron tomographic image of


aerospace valve, showing bend in O ring.

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differential laminography image produced


from examining the difference in
laminographic images at different depths
Closing
gave the best image of the crack. Initially, radiographic testing was used for
The reversed geometry, scanning beam the quality control of weldments and
technique is discussed at greater length castings — it is still used for this purpose.
elsewhere in this book. Various publications cover the history of
nondestructive testing in the aerospace
industry,1,48 including radiographic testing
of aircraft during World War II.49 Every
Simulation Tools decade since then has seen major
advances in technology. Applications of
Advances in computational power has
the method have been expanded to
enabled not only new capabilities in the
include the inspection of components and
inspection systems but in the physics
materials for experimental rocket and jet
calculations used to design and optimize
aircraft, missiles, solid propellant and
X-ray techniques.45 Validated inspection
liquid propellant rocket engines, space
models offer an opportunity to design
vehicles (Fig. 39) and satellites.
inspection techniques for a given
component.
Advances include the development of
an X-ray computer simulation program FIGURE 39. Space shuttle: (a) Atlantis touches
capable of accurately simulating the down, 1992; (b) Discovery is launched,
output of an X-ray imaging system and 1995.
involves a number of components, (a)
including X-ray beam models for isotope
sources and bremsstrahlung sources, the
interaction of that beam with the part
including material effects, complex
geometry issues and finally the
conversion of the beam into a visible
form, in the case of radiography, film or
image intensifiers. Tools developed
include the ability to insert a
discontinuity of any size into the part at
any location, which provides a powerful
tool to evaluate the capabilities of a
particular inspection. The use of a
computer assisted design representation (b)
for the discontinuities allows realistic
cracks, shrink cavities and inclusions to be
evaluated. The limit of detectability for a
discontinuity at a particular location can
be calculated simply by varying the size of
the discontinuity and calculating the
resulting image. The location can be
changed at will and a detectability map
can be computed for the entire part at
particular kilovoltage, setup, orientation,
sensor type and all other parameters
currently modeled in the simulation
program.
Techniques to consider the probability
of detection as a function of position have
been developed. The application of a
quantitative X-ray simulation code has
applications at the earliest stage of design
where inspectability issues can be
evaluated. The simulation code can be
used to optimize an inspection to ensure
adequate coverage with the best
sensitivity at a minimum cost and can be
used as a training tool. Applications to
aerospace castings46,47 and other
components are being explored.

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The high reliability of these vehicles


and systems can be directly attributed to
proper application of nondestructive
testing as a whole and industrial
radiography in particular. This reliability
has been made possible through the
dedication of scientists, engineers and
technicians of the aerospace
nondestructive testing community.
Radiographic testing continues to be
important for aerospace quality and safety
in the twenty-first century.

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