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Abstract: The rapid development of urban areas and the increase in construction activities have resulted in a scarcity of land with favorable
soil conditions, necessitating the use of locally available weak soils for construction activities through stabilization techniques. This study
introduces a new material, areca fiber, and its suitability as soil reinforcement. Although areca is available abundantly in many parts of the
world, its application in geotechnical engineering has not been explored. In the present study, bottom ash (BA) is used as a stabilizing agent,
and the suitability of natural areca fiber as reinforcement is demonstrated through detailed experimental investigations and reliability analysis.
The test method includes compaction tests, unconfined compression strength (UCS) tests, California bearing ratio (CBR) tests, and split
tensile strength tests. The BA content was varied from 0 to 40%, the fiber content was varied from 0 to 1.5%, and the corresponding per-
formance assessment was done. A small amount of cement (3%) was also added to improve the pozzolanic reaction. The UCS and split tensile
strength tests were conducted on samples at different curing periods with a maximum curing for 90 days, whereas CBR tests were conducted
after 7 days of curing for both soaked and unsoaked conditions. There was considerable increase in UCS, CBR, and split tensile strength of
the soil with addition of BA, and the strength values increased tremendously in the presence of areca fiber. Mineralogical and microstructural
studies were conducted on the stabilized soil sample using X-ray diffraction (XRD) and scanning electron microscopy (SEM) analysis. These
results confirmed the formation of cementitious compounds in the XRD patterns and showed development of dense matrix in the SEM
images. The performance of the modified subgrade soil was validated using a reliability approach, which found that the soil subgrade with
BA and areca fiber can certainly be used as pavement material for low-volume applications. DOI: 10.1061/(ASCE)MT.1943-5533.0002326.
© 2018 American Society of Civil Engineers.
Author keywords: Soil stabilization; Soil subgrade; Areca fiber; Bottom ash; Reliability analysis.
Introduction stabilized samples. GGBS and FA are significantly used in the ce-
ment and concrete industries in addition to soil stabilization. FA
The rapid growth of population, fast development of urban areas, and BA are the major combustion products in the thermal power
and increase in construction activities have resulted in the scarcity plants after the burning process of coal. FA has got much applica-
of land suitable for construction. Structures frequently have to be tion as compared to BA. It has been successfully utilized along with
built upon problematic (weak or expansive) soils. The stabilization many other materials in cement and concrete as well as in subgrade
of soil with chemical additives helps to improve the engineering and many other civil engineering uses owing to its better reactivity
properties of the soil. The common admixtures used to stabilize and pozzalonic reaction (Kolias et al. 2005; Parsa et al. 1996; Sahu
soil are lime, cement, ground granulated blast furnace slag et al. 2017). Utilization of BA has been quite limited because of its
(GGBS), fly ash (FA), and bottom ash (BA). However, using lime slow pozzolanic activity and sandlike property (Cheriaf et al.
and cement raise environmental concerns and are not preferred 1999). However, the use of BA has huge potential in soil stabiliza-
nowadays. In the recent past, sustainable binders have also been tion application, which has not been widely explored. BA gener-
developed for the application in soil stabilization (Latifi et al. ation varies between 0.6 and 2.10 t/MW from the thermal power
2017b; Latifi and Meehan 2017; Rashid et al. 2017). Latifi et al. plants, and India’s energy production is more than 307.28 GW
(2017a) examined the effectiveness of a new calcium-based addi- (Kumar et al. 2010). Its exposure results in many environmental
tive developed from biomass silica for stabilizing a residual laterite hazards. In the present scenario, less than 30% of coal ash produced
soil. They found that the new stabilizer had significant effect on the is reused; hence, measures to improve its usage have to be
strength properties, which was also evident from scanning electron considered.
microscopy (SEM) and X-ray diffraction (XRD) analysis on the Fibers can be used as a reinforcing material in soil to impart
tensile strength. Previous studies reported the suitability of using
1
M.Tech Student, Dept. of Civil Engineering, Amrita Univ., Coimbatore, synthetic fibers, such as polypropylene (PP), polyvinyl alcohol
Tamil Nadu 641112, India. Email: soorajsudakaran@gmail.com (PVA), and natural fibers such as coir, jute, and sisal, among others,
2
Assistant Professor, Dept. of Civil Engineering, Amrita Univ., in soft ground applications. The reliability studies conducted by
Coimbatore, Tamil Nadu 641112, India. Email: ak_sharma@cb.amrita.edu Moghal et al. (2018) reported the effect of synthetic fiber reinforce-
3
Assistant Professor, Dept. of Civil Engineering, Amrita Univ., ment on CBR behavior of lime-blended expansive soils. The study
Coimbatore, Tamil Nadu 641112, India (corresponding author). Email: showed that the concentration and length of the fiber have signifi-
k_sreevalsa@cb.amrita.edu
cant influence on the CBR value. Chauhan et al. (2008) studied the
Note. This manuscript was submitted on July 4, 2017; approved on
January 9, 2018; published online on May 28, 2018. Discussion period effectiveness of fiber reinforcement in subgrade soil along with fly
open until October 28, 2018; separate discussions must be submitted for ash. They reported that the coir fiber shows better resilient response
individual papers. This paper is part of the Journal of Materials in Civil with respect to cyclic loading against synthetic fiber owing to a
Engineering, © ASCE, ISSN 0899-1561. higher coefficient of friction. Cai et al. (2006) studied the effect
Experimental Program
Compaction Tests
Optimum moisture content (OMC) and maximum dry density
(MDD) for different proportions of soil and BA were determined
using a series of minicompaction tests. The minicompaction appa-
Fig. 2. Areca fibers. ratus consists of a mold of 3.81 cm internal diameter and height of
10 cm, with a falling hammer weight 1.0 kg with 36 blows=layer in
three layers for the Proctor compaction curve. The minicompaction
apparatus requires only about one-tenth the volume of soil needed
Table 3. Physical properties of areca fiber when compared with the standard and modified Proctor test. More-
Physical property Value over, the time and effort involved in carrying out the minicompac-
tion test is much less (Sridharan and Sivapullaiah 2005).
Young’s modulus (MPa) 2,770
Maximum tensile force (N) 3.21
Diameter (mm) 0.25–0.35 Unconfined Compression Strength Tests
Length (mm) 50 to 80
Elongation at the maximum tensile force (%) 2.4
Three specimens were prepared for each test according to the MDD
and OMC of the mix obtained from the minicompaction tests. The
soil-BA mixture was prepared by adding the required amount of
water and mixing properly in a wet state. The mixing was done
study, areca fibers were collected from Kannur district in the state by hand and good care was provided to prepare a uniform mix.
of Kerala, India. The dry areca nut shells, which are brown in color, The specimens (38-mm inner diameter and 76 mm long) were pre-
were collected for the present work, and the fiber from the shell was pared and tested per IS 2720, Part 10 (BIS 1991). The prepared
extracted manually in the laboratory. Fig. 2 shows the physical mixes were then placed inside the mold and compacted. The spec-
appearance of areca nut fiber, and the physical properties of areca imens were then extracted from the mold. Some of the prepared
nut fiber are tabulated in Table 3. A dried fiber of length 5 cm was samples are shown in Fig. 4. The specimens were preserved by
used for estimating the tensile strength of the areca fiber using ten- wrapping them up in polyethylene bags and then placing them
sile testing equipment available at PSG College of Technology, inside gunny bags with a regular sprinkling of water to maintain
Coimbatore, India. humidity. The UCS tests were conducted on soil-BA mix samples
(with varying percentage of BA) to arrive at the optimum content
of BA.
Treatment of Areca Fibers
BA is a pozzolanic material and may require external activators
The areca fiber used in the study was chemically treated so that to improve the pozzolanic action. Hence, in the present study,
its flexural strength and durability properties are improved 3% of cement was added to increase the pozzolanic reactivity of
(Venkateshappa et al. 2010). The step-by-step process of the areca the mixture. Once the BA and cement contents were fixed, further
Fig. 3. Process of areca fiber treatment: (a) areca fiber soaked in water for 15 days; (b) drying for 15 days and keeping in KOH for 15 days; and
(c) treated fiber after drying.
UCS tests were conducted at different percentages of areca fibers condition. Later the specimens were soaked in water for 4 days and
(0, 0.5, 1, and 1.5%) on the soil-BA-cement mixtures after curing tested for soaked CBR value.
for 7, 14, 28, 48, and 90 days. The details of the different mix
proportions of the samples tested for UCS are shown in Table 4. Microstructural and Mineralogical Studies
For every combination of mixes, three samples each were tested,
and mean values were reported. An XRD technique was used to determine the mineralogical
changes in the stabilized soil, using Rigaku Ultima (Tokyo, Japan)
at a scan speed of 0.5°=min from 2θ ¼ 5 to 85° with a wavelength
Split Tensile Strength Tests of about 1.54 × 10−10 Å. Scanning electron microscopic analysis
Tensile strength is an important parameter in predicting the suitabil- was done to observe the microstructural alterations happened dur-
ity of a subgrade material in pavement construction. The simple and ing the stabilization process using a Carl Zeiss Evo 18 scanning
easy procedure to determine tensile strength is the split tensile electron microscope.
strength test (Das et al. 1995). The specimens were prepared in
a similar way as mentioned for UCS test samples and cured for Results and Discussions
the same period of time. For testing, the specimen was laid diamet-
rically on the Universal Testing Machine (New Delhi, India) and
the load was applied until its failure. The split tensile strength is Compaction Test
calculated according to IS 5816 (BIS 1999), as below: Figs. 5 and 6 present the variation of MDD and OMC, respectively,
against the varying percentage of the BA from 0 to 40%. From
2Pmax
T¼ ð1Þ
πdL
Fig. 6. OMC versus percentage of BA. Fig. 7. UCS versus percentage of BA.
Fig. 5, it is clear that as the BA content increases, the MDD of the a great effect on the strength, and this is attributed to the hydration
mixtures also increases; beyond 30% BA, a decrease in MDD was process of the cement with soil and BA. In previous studies, similar
observed. It is possible that the soil-BA mixture becomes well- strength improvement was reported (Cai et al. 2006; Chauhan et al.
graded with the addition of BA up to 30% and enhances the 2008; Kumar and Gupta 2016; Lekha et al. 2015; Moghal et al.
MDD, whereas a higher amount of BA disturbs the intergranular 2018; Parsa et al. 1996; Sahu et al. 2017).
packing leading to the reduction in MDD. OMC was found to re- There was increase of 191% in UCS value with the addition of
duce with an increase in BA up to 30% and increased beyond 30% 1.5% fiber to the soil-BA mix for the 90-day curing period, whereas
of BA (Fig. 6). Similar trends in OMC and MDD were reported by the percentage increase in UCS value owing to the addition 1.5%
several previous studies (Ibraim and Fourmont 2007; Osinubi fiber was 210% for the 48-day curing period.
2000). Additionally, the replacement of soil with excess bottom
ash may lead to a reduction in MDD because bottom ash has lower
specific gravity in comparison to the soil. The decrease in optimum Split Tensile Strength
water content gives an indication that the soil can be stabilized even The performance of the soil mix under tensile load was studied
at lower water content. On the other hand, the increase in MDD through the split tensile strength test. The split tensile strength for
demonstrates the suitability of soil-BA mixtures for use as subgrade the soil-BA-cement mix with and without fiber was determined
and embankment material. In IRC (2007), the density of material for specimens cured up to 7, 14, 28, 48, and 90 days. Fig. 9 shows
used for subgrade construction should not be less than 1.64 g=cm3 , the variation of split tensile strength with curing period for
and the present mix satisfies the criteria. the soil-BA-cement mix with and without fiber. The results ob-
tained in the present study were similar to previous findings
UCS Test
Fig. 7 shows the variation of UCS at different percentages of BA
without any curing. From the UCS tests, it is clear that the strength
of the soil improves nominally as the percentage of BA increases up
to 30%, whereas there is a drastic reduction in UCS at 40% of BA.
The reduction in UCS after 30% may be attributed to the reduction
in MDD that was observed in minicompaction test results. The
reduction in density reduces the particle packing; as result, the un-
drained shear strength reduces with 40% BA content. Based on the
results of compaction and UCS tests, 30% BA can be considered as
optimum content for further detailed investigations.
Fig. 8 shows the UCS variation of the soil-BA-cement mix with
a varying percentage of fiber for curing periods of 7, 14, 28, 48, and
90 days. The test results show that as the percentage of areca fiber
was increased, the UCS value greatly improved. Notably, the
increase in UCS up to 1% of fiber content is nominal, whereas
the UCS increases tremendously with 1.5% fiber content. This
is attributed to the improvement in the cohesion, better gradation,
and interlocking or packing of soil and BA. A similar observation
was reported by Lekha et al. (2015) when laterite soil was mixed
Fig. 8. UCS versus percentage of fiber content.
with areca fiber and cement. Fig. 8 shows that the proper curing has
(Kumar and Gupta 2016; Sahu et al. 2017). Generally, the fiber fibers. In the present investigation, CBR behavior of both soaked
inclusion improves the tensile behavior property because of the and unsoaked conditions fulfills the criteria of a minimum CBR of
interlinking property. Different quantities of fiber can cause dif- 15% for subgrade applications (IRC 2007). However, CBR showed
ferent effects on the strength behavior of the soil sample. An in- a 24% decrease under soaked condition, as obvious because the
sufficient quantity of fiber may lead to less stabilization of the sample becomes loose and soft in the presence of water.
soil, whereas an excess quantity may result in ineffective stabi-
lization and decrease the strength of the soil. The study by Kumar
Mineralogical and Microstructural Studies
and Gupta (2016) using polypropylene fibers showed that the
maximum strength obtained was in the range of 60–65 kPa. Li Fig. 12 shows the XRD diffraction patterns for the optimum sta-
et al. (2014) also found that the tensile strength of the Nanjing bilized mix (soil mixed with 30% BA, 3% cement, and 1.5% fiber)
soil mixed with polypropylene fiber increased significantly with sample cured for 28 and 90 days along with the untreated soil sam-
the addition of only 0.2% of fiber. In the present study, the tensile ple. XRD studies showed that with 28 days of curing, cementitious
strength of the mix with the addition of fiber is improved up to compounds like tobermorite are formed as a result of pozzolanic
905 kPa after 90 days of curing. This is well above the minimum reaction. Tobermorite is a form of calcium silicate hydrate that
tensile strength of 469 kPa required for subgrade pavement gives strength to the stabilized mix (Solanki and Zaman 2012).
applications (Osinubi 2000). The peak intensities are increased with the 90 days of curing.
Emergences of new peaks are also observed in the 90-day cured
CBR Test samples. Additionally, calcite peaks, which are formed along with
the cementitious compounds, are also identified (Solanki and
CBR for the optimum mix composite for unsoaked and soaked con- Zaman 2012). The calcium hydroxide peak is found at 2θ − 47°,
ditions after 7 days of curing is provided in Table 5. The load pen- which is the result of the hydration of cement. Calcium hydroxide
etration curves for unsoaked and soaked conditions are shown in
Figs. 10 and 11, respectively. With the proposed modifications
regarding the addition of BA, cement, and fiber, the CBR was ob-
served to increase from 2.25 to 39.45% for the unsoaked condition,
whereas the increase was from 1.20 to 29.98% under the soaked
condition. The similar kind of decrease was also noticed in previous
studies (Sahu et al. 2017). Ravishankar and Raghavan (2004) found
that the CBR of the coir-stabilized soil increased up to 10% of the
coir content, but it further reduced beyond this amount. The thick-
ness of the base course can be reduced considerably by using ran-
domly distributed fibers as reinforcement (Gosavi and Patil 2004).
Sarbaz et al. (2014) did thorough experimental studies on CBR
behavior on soil stabilized with date palm fibers and found that
the longer fibers had a greater impact on CBR behavior than shorter
1X n
μ¼ ðx Þ ð2Þ
n i¼1 i
Fig. 12. X-ray diffraction pattern of (a) untreated soil; (b) stabilized
mix cured for 28 days; and (c) stabilized mix cured for 90 days.
The sample variance is
1 X n
helps in increasing the pH of the system, which further enhances σ2 ¼ ðx − μÞ2 ð3Þ
the pozzolanic reaction. Some of the high intensity quartz peaks ðn − 1Þ i¼1 i
that were observed in the untreated soil diffraction patterns
(2θ − 63°) is now found to reduce with stabilization and curing From the variables, the μ (sample mean) and σ (standard
periods. It is quite possible that the quartz is being consumed as deviation) are determined. Coefficient of variation (expressed as
a result of pozzolanic reaction, thereby forming new compounds a percentage), which is defined as the ratios of standard deviation
such as tobermorite and CH, among others (Sharma and (σ) to the sample mean (μ), is also determined. The coefficient of
Sivapullaiah 2016). variation can be defined as the spread that describes the amount
Fig. 13(a) shows the micrograph of the untreated soil. The gen- of variability relative to the mean commonly used to quantify
eral fabric of the untreated sample resembles a clay matrix con- the uncertainty related to a problem (Ayyub and McCuen 2011).
nected with visible pore spaces (Al-Rawas 2002). However, no Information on mean and variance is used for calculating the reli-
aggregation of clay particles is observed in the absence of additives. ability of the system expressed in terms of reliability index (β).
SEM micrographs of the soil stabilized with 30% BA, 3% cement, First-order reliability method (FORM) is used to determine
and 1.5% of fiber at 28 days is shown in Fig. 13(b). The hydration the reliability index of the problem. If C and D are the capacity
process of BA is enhanced by adding up the cement, which results and demand of a system and performance function is defined as
in the formation of hydration products such as tobermorite, CH, gðxÞ ¼ C=D; for log-normally distributed C and D, the reliability
and other hydrates (Mohamed 2002). However, few pores are also index (β) is obtained as follows:
observed along with the dense matrix for the samples cured for h qffiffiffiffiffiffiffi2ffi i
28 days. Fig. 13(c) displays the interaction between areca fiber- ln μμdc 1þδ c
1þδ 2d
stabilized soil for a 28-day curing period. The bond between the β ¼ pffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi ð4Þ
soil and the fiber is clearly visible. It is observed clearly that ln½ð1 þ δ 2c Þð1 þ δ 2d Þ
the areca fibers have rough texture, which induces resistance be-
tween the soil grains owing to an interfacial interaction. This en- where μc , μd are the mean; and δ c , δ d are coefficient of variation
hances strength in the BA-stabilized soil in the presence of fiber. in capacity c (N f and N r ) and demand d (design traffic load),
Further, the formation of cementitious compounds with curing respectively. The coefficient of variation in demand is taken as
makes the microstructure denser with increased resistance between 40% in the present study. According to USACE (1999) guidelines,
the fiber and hydration products (Tang et al. 2014). It is interesting a reliability index (β) of 3 is acceptable for above average perfor-
to note that the areca fibers are intact even after the failure occurred mance and 5 for excellent performance. Based on the obtained val-
in the specimen. After 90 days [Fig. 13(d)], the amount of hydra- ues of reliability index, the performance of the pavement can be
tion products continued to increase, resulting in a higher strength of analyzed.
the mix, which was reflected in UCS test results. Moreover, a much In the present study, numerical analysis of a three-layered flex-
denser matrix is observed with fewer pores, showing continuous ible pavement was performed through ANSYS 3D, and maximum
mass of the stabilized soil, which further increased the strength tensile strain at the bottom of the surface course (εt ) and maximum
of the sample. compressive strain (εc ) at the top of the subgrade layer was deter-
mined. The values of the number of load repetitions for fatigue and
rutting failure (N f and N r ) were estimated through Eqs. (5) and (6),
Reliability Analysis respectively, per IRC 37-2001 (IRC 2013) guidelines. The pave-
ment under consideration is of unit length and 3.5-m width, con-
Reliability-based methods are used to account for the uncertainties sisting of three-layered systems. The subgrade depth was taken as
in the design process. Flexible pavements are analyzed according 500 mm, whereas the base layer and surface course depth were
Fig. 13. SEM micrographs of (a) untreated soil; (b) stabilized mix cured for 28 days; (c) fiber-stabilized mix interface cured for 28 days; and
(d) stabilized mix cured for 90 days.
assumed as 150 and 75 mm, respectively. The analysis was focused Elastic modulus of the bituminous layer (E) was considered
on low-volume traffic roads; hence, IRC (2007) was followed for as a constant value of 5,000 MPa. The vehicle loading was approxi-
the guidelines. mated as circular loading of 550 kPa with the radius of contact
The number of load repetitions for fatigue failure (N f ) is area as 110 mm for the standard axial load of 80 kN. For the differ-
3.89 0.854 ent set of E and μ values, the maximum strain values at critical
−4 1 1
N f ¼ 2.21 × 10 × ð5Þ locations were obtained through the analysis using ANSYS 3D
ϵt E (Fig. 14).
The number of load repetitions for rutting failure (N r ) is The corresponding N f and N r were then estimated using Eqs. (4)
4.5337 and (5), respectively. The number (N) of N f and N r values were
−8 1 obtained through this method. The coefficient of variation in capac-
N r ¼ 4.1656 × 10 ð6Þ
ϵc ity was obtained for the fatigue and rutting. By knowing the mean
and coefficient of variation of capacity and demand, the reliability
Randomly distributed variables (N), i.e., elastic modulus of index values with respect to fatigue (β f ) and rutting (β r ) can be
subgrade (Es ) and elastic modulus of base materials (EB ) were determined. The pavement performance based on the reliability
estimated by Eqs. (6)–(8) as given in IRC (2013), using MATLAB index are tabulated in Table 6.
programing; the modulus of elasticity of subgrade is From Table 6, it is observed that the performance of the pave-
Es ¼ 10 × ðCBRÞ For CBR ≤ 5 ð7Þ ment will be excellent (β f and β r > 5) for 0.6 million standard
axles (MSA) of design traffic load. Up to the 1 MSA performance
(β f and β r > 3) of the subgrade is acceptable and can take a maxi-
Es ¼ 17.6ðCBRÞ0.64 For CBR ≥ 5 ð8Þ
mum load up to 1 MSA. IRC-SP: 72-2007 clearly states that the
The modulus of elasticity of the base layer is traffic volume of a low-volume road varies from 10,000 to 1 MSA,
and particularly, it is at a range of 50,000 repetitions throughout the
EB ¼ ES × 0.2 × h.45 ð9Þ design life.