PEM 6U ATA H A\AT-1 P\(AAT

A65I RACT

The Put0o!Q a.id pipenmen[ arg to tearnihe pr0H.t\ 0rmaqtn{ P'ccl'

or ma(rn!j P'La(

ocid srom phenoL 1rlt!h !!Lronattoo (g4cbton b! L0llcSnlrated uf!0t lourilDo

ana nlb.ailon r€o('
troo by Lon(gnrta!p4 lrdo. !0Lu!lon crrrh hga!rng pro(e(! and to QtLr\.ane the vreLa oF the Fcrr(

4crd , tirlL. u€l{ht bot,ile anl Phenol ural oQr(Jhol ,lh€n t,oaE 4 at Pheaor ura( put lnto
r,he

EETAnCQ Ft-a(H. Th€n, '9 rnL ot oncpnrralo/ q'loq !o!0tlDn nJa/' o.l.le.l t,he rtorenQ rLal(.

rlg(L ths lot0ilDn lr)4( heaLQd uP ror r! mlnute( . API€( that ,lt ujas LooLed untlL ilrr
tlmp€rarure wA( t!'C , The . r! mL or HFlo. !OluLlo0 orot dolAe..1 Dit bq b,l !rlrrr0g i!
NoLL . lt uJar haA\pd ar roO.C UntrL ll torm€r{ br0un \\p4fi ?A\ a@\t 3u rrnu!p('
-[hQt,
,ro n,r. Dr r0(\rpn{(awl 11r(or !01!trur v:t\ aa.|a.\ aqafi ltt Uq l)lt qith
!!\(rlnq ,.,:l hgat prDLpr! r0r ,O d\rnUte! .'thqn, 9 mL 0t tDnLpntrqted tlH03
(otnrron o0! oa*ed b\t b\ blL qilth (trrlog a d nf4rrnq ProLQ!! ror I0 mnut€(. rlgrt lt ll)a(

!0ot0d untlt trr! !othP€f4rure w0( 19'c ,and thco !hg P(eLrPriate wa( I rtefea Erom lrr(
!ol0lroo .Ihe flQ(pltote ua( c(lttal!?€A bg elhan0t. Thq nnLqrcruc( rlllpd rha Preoprl,a!! u'(

P\rL r0 Lhp- o\rQn ror \E rnrnoi€(, aod pui lor0 the el,(!rta!o( . nnd lhg SleLd at $LttL a'tal
ir ql,3t ,1, all/ {r(td moL ot prcnc acra r! t6 ql '{o

(eguJora! r flrtra on, P(edfl14r€, tutronaLron

AgqlRAK
({rcobaan inr addtal rnrrK momperrJari ?ombuai4n asafi otq(at h'
{u}JOn
'larl
rl rc00L mgutut sltronoll do00a0 alam ruLr4l Pexa b d^ r0akcl niiracr 4eogan 't<Afi it-
$tga a{t ^taq Pt\.on.
psl(Ar AserL4r ?Q$a}atlvLn.lan mooghlt0tg Parra
trar 'fla
/dn t{\o\ ,d^o momaitl(ran 6,oo( €t r00oL adui \'ab\ tl4t$<e-
mQofmb4nl boLoL Pe0lmbanq
mewl)or
Lat, m€maslK(rn lE mL t4r0tan Hzso{ p€xat $e rlllad1 labu rLorenog' [dt! '
(ao krutan Seuma ls meNt, Spteuh ltu mendlngln(4n hogga culo \A(Uc4n ,lr.
L4to mQlhalukl(an rg mL HNo3 P0r4r s€dlhlt ,cmi (ellKtt \a(nbiL dtarluq, laiq at'
oengetuarka0 \aP ctKQVv Clta'ha ao fiantL. lalv,
?ataswLo Pd^ ruhu loo'c samp4
mgn4mDahxan k€mbaui 1o mL hd09 PeKa! Sodl(ll Ae i \pdtv'b SQttbtt ,L.rd04,

tldl Meli.'ano.st.an sc)arna 20 mo-llic . t/l, IYl]goalukkao , mL Hnor ?ekaL gd)t^tv

deml (er{ixrr dl*4ut\, Adr (^e dnLat^an $!rm' romenlb. (Pmu/14^, Mcnar'
'Il\biL
nqrnxan l.4rwan 94mpar suhu lr.rut4n tc'c, r4n mon$^rlnl at\*aPa\ ;af,t l^(u'
tAn lnaut^. K€mudr4n Mon4l{ tuuf,4ri endaPan detban Ol/.oo-. Stn tercr'l(r Vao{
botr{t enaapao /lm4l!t(K4n Aalatv o\eo /4n m0masuKl44n RO Aavd', 9t {ra|or.
\tgti ^!4tl' Pl[(aL U40g Wty./I$rk ^dalah ut 'rt'(o dan grM mDL cebera( ll''{1210
1,(4ra l.{ uocl I Endapct, Htrr4sr. SuEooasr
 so,H 0rth0s\, [ronot

OH
Hr\O\ PeKot, t0o"c
HrSOq
OH
f0(aL

P4rl!ut( 0 0at

(0r
tl
adaPun Prcduv Va00 tebth sl4bt\ daavh ?aaa su'
?ara- l$Lton.al , Ko(Qia
h') gah0 ringgi te.idai Ke\e\i(^banaan . SaddtYkao elecTi bebat at'\i vo'
sinua W.bih \t(\q{ Aa(i 0rt0sutr0nat ainooa ?adn suhu rpndah. rearri Pp!t.
bgntuKao tobth cepat .

( Sotomon , gltl ,20 n )

aAabh s\)at) relksi sUbltil'u(i eteKrroflti( OL€h sQ-
R€al{gi nitr4si
nu4N, vang meog4rdun0 {r{v( No, (dirrir). 9^d'a \en\aua s€pQr inl
b801en4, re4(ri subLirusi lrngsuo{ Pada pe(aaKsi an dQt1a\ aedm rfital
?g(N dan a\aM \rL|az ?e(,t, Ai\ef$l pgna.nason- As4m suLF4t P€{4t ttrgll-
Pel cQ?A+ fedKei f\|'ra\i tlSnga^ Ce(a mQAaiKAaCt
l(onsentr4ei gtentroFit , Uqltu
100 nttronium (Nor t ) . R€a(si reriqdi sebagai berixut r

H02
r HHOc t H:SOv ---------+ +HNosrtH2lOq-
5a. - r9"c
8e1,
6rl , 20 lr ) (sobmon,
AQarsi nrtrasr pada lpno, /engan merQ/(etKa.. AAnqan ata$ n.i,'/rat
enNr /€09a0 palo suhr Kamar menghosiLhan tpblh banuak 0r{0nttro Penol
da(i Pada tsra - NtropQn0[ . Adq?r(\ y{A)a ?(odb( AaPat la(tq\$ng dlPi'
s4ht{4n a0ftgrn c4(a Al\\itAti U4p, karen4 0rt0ni[roPOnot bprsilar tgblh
\.ro\ottL . \0tar\Lito! isomgr vadvol'lo davt a[lta\ dati lxatrn hldro{oo ma'
sin0- ma(inq lsomor. P(oduH otio0ltrDP€no[ Memti(i iK4tan hi/rog00 iot14 m0'
\gl(ul,a( , (044n{k40 para nitrop€[ot, memr\it(r tKatan hidrogen rnre(m0t0({uLar,
guonq(an p4(a nttroF€'no[ m€mrttxi i(atan hidfoqen totprmotS6uur.
OH oH
OH
H0r
:o'l, H H0r
t
29aC

nirrorQoor
orro pardilf;r0oor
30 - rro'/, t9'1.
XItr ' rort ) (soLomon,
Qtl((istal.rEdci 4a4uh Plo\Qs p€murnia0 sen\jaL!a !an3 umum ,li -
1un4l(an Untuk mgnd4poiK4n sg0Vaura / crud€ yanq diinninvan ,tyhan
/ari s€olawa y4n{ K0!or da^ i\qqi imPuritie! . prtnsipnga aaaLal nPU
{vna(an PQta(uv yac\q aqQAt mO[4rutK4n sDLid ?ada suhu tin99i . totapi
seai(it mOLarutt(4n PaAa suhu (gndah dilat w\ at' a4L4r, sol'uQnt bgrsuhu
tin{gi /i/iogin(ao da(t dis(irg Un1UK m0nghrl,on0xl0 lmpurlttas
,xomuarro
p(orQE tor(8Dut/ /ruL4nOl sarn
Uanq Kota0q At\t\ pada Urwan. Pa\ ald4paL
crudo mu(nt dan rmpurltlo! tortlngg4L Pado \.at utat inauK . l(0mulian
Lgu4r Pemanaran / Pooqerin94n la( b+an aayl liPer0tph c(vde !ang
m0fnr .
[mann,re,tgto)
Alam piKr4t ad^lah sa(Nawa lgr\)pa ?adara KnstaL Derwarna
klnlng /Olg4o ttti( Wteh r2r'c . Asam Pi(r4t Urut Aalom avaoaot dart
bgn?en4, sodtt{rt la.w dqtan afi, dan pada Pomana(4n dta$< Soooc Aa-
Pat meL€da(.
( 6orqg ,sto , zou )
As4m ptfir^ Aapat A\b\ar dAngan cau mer€al{sikan (Qnol Aqtgco a'
9m nitrat pAK/?- Aa^ 4sam q)Lfat Pe\,ar Alapft,ai ?efianagoft . RoaKsi ni-
trAsi 4Kan murt4 l( 4or]4di paaa ?a@ -
.ldn veAua o(fi' ?ado F8[0L, [YLO&-
b0rrt(an hastt bgtora agarn plk?t ,,u,6 - trlnitrofeool , ?gc<a$a,
^tou
mgrea(siKan tenot Aan asan svlt4t Pe(at /lsortal Pemaoasa0 d6on nQAq'
hoglt('ao 4lmp!ran o(o - Adn P4ra - fonoLsur,foniK.
0u oH
sos tr
H: SOq ----> + tl2 O

(03 H

kqti|(o Pendmbaha0 49am niLtat ?A$ou data$ PA$ara\qn, ro,l.{si nl Lr4tr,

aon {ugu( - S02tl /rlubiltusi Otoh - tto, ?oAa uqp asam lrnrtror€001 sl,rt-
tat , r'P09halrthan asam pl(far .

ofl o\1
s03tl+rHN0s-J S0. H r rHiO

eH
H0r

HO, S03R NO, |-ro,

t H *or ------> t uzsOy

(Hann , 170, !q6o )

Ina(\ot a\a\ e t zLxohoL adalat\ 9ral\ Prolu( Komor\iaL lJan€
mongan/ung C2NsOA dat mgmpunu4i 14p4+40 o,8t 4r/cn! ELaioL
l{\\)dan \el fuRar aat, iart)\ disrmpa0 AdaM pgli aLal LQfio(t \ngam
( svento , b2r,l9lg )
Asam t\ttt4L PSML lanq komqtsl4r. mQrupa,{an LarUtan tQP0rti air
l|lngan capatat r,U.l €rlCm3 tarut n inr y\Onqqn[uoq Gg,5"l" HNo3 ata!
0,gg /mL , (on(e0tmstnu o *t(a-KJa t),6 mot4r. uap 0itro(o membr,4r
HFIO3

reaqs0slo q0n5 se4tKt Lefufat rtu borNarn0 coKeto( t.(0mofah4r. ?4r tnt ha-
rus 4rpQrta(uron detqao ],BJam,li haH-hatl ,dlngao fiaftaiat sarung m-
n04n,{4n poundunq matq.
(tvenLa, 6r: , lgrg )
Asom suLr4r gg(at adalah reage0qo Komorstal
Uaog met0paKan
catfao \^K borwarnd gopofri minuaK ,agng4n rapatao
va00 ttnggi (l.8rt
qr/cmr) . 0.e4gensla haros a{ip€rta(0Kan denqao hau-hatt aAAqAn
, mef(ra-
Mi sarullg @nla.l don KafeL dan pgun/unq m4r4. t(erlKa mgngQncarK4n,
aqam suLtaf PgKat hafus lltu4ntKan ge .ahai - l'han daw$ atr L.lon
^e
ta( boteh ee(4ri -kA!,i qobatirnua) sambl! /t4du( ,Aan J\Ka ?att$ didtogtn.
|(40. Lrrutan re0o€nsl0 hafur sa€pra /th,unol(an /4 KU[rt a.a\) ,4a p^.
karAn don{a0 mgnc0dnua Aennar att ga00 b,lnVAK Sghati
(Cretta , b39 ,14rS )
UNut.( momPeroiph OMap4o hdbtur Ka\a(, ada suat! Ut{ura0 U4n{
l4ne0t oenrilrq drpQth4tiKao aava $o\a\ ?enqatld?pn . gal{nl K0Lorr4r-
lsnuhan nigbi IR). KeteuatJpooh 4r\ cp] /tr0must(a0 de(\Tan pe.Iianaao
leba3ar beflkur :

a.
s

Dtqlnr R. (pL€urarJ
anuhan rli!bi
0' xeclpatan moLar ururan ser€t4h /lcampur, t4pl borl)m llmbul
O(\dapqn
I' (€urutao mour eodapan
)lva Lldapa momp00gai hastl kaLi Kotarutan Uanq rgn a4h [!
lu90 re0aah) Aa^ At,dqpat ir,u terbonilx daci tdrlttal \lanq dl^v pgt\at
t0 rrnqgr) moK4 kotoujauonoh4n fttsbinga at<on ur,gqi
( Bil4r, 29t , ts95
)

t s oriqqig (orJa AL4r, U14ma

I 1 I Wq ter I et PumP

e
Pt

@(\bac Izr Nate( lst fump

 Nate( ltt adalah alar !4nq dtgrna'4ao u^tuk mempp(c0pab
PD'f,P
penvayinq40 aengan o\emdnfaarK4n prinsip 6grnovli , Var+u ,

% , p 0 tv , p \,, = p. r pg h, + pv,,
; )
riK sat! ,{an dro sQ.PQft^ Q*da 14 b Aatas . P aaavh \e(aoao t ? adalah
mas\o je0\s E\uda, aAaldb KQringglon Aor, \ ada\ah tlQepatan 0^t\
^ ^t(.
armb4r tQrl,iha{, bahura '.

sehrngg4 Komponen Qnef€i POtposrat aa?at dthtll$qvao darr 9Qr\amaan

Pqr!Pv,' = P,r t,7tt'
"

?ada gi51q61 inr ju94 berLaKu Pc.r\a$aart Konlinlt14( cQba4at bQftvut .

Ar!{:A,V,
!r : A, \J

Armaoa A ddatah l\)os panan.atq ,lar \r ddatath ,rlt( \Qht(\g7a da'

^ALQPtah
P4t dr\Ubt\tuSiKan paAa ?at \arfaact s€9eLumn!4 gA[\l ]
pr r !^ p/e,.v,\= Q, t -\ pr,,
- \--;; )
r^s\a ar,,.c\ra At da^ A, saag^ltah +inggi sQhinsga a?obib art,\odqt(afi , w.
(a, nit4i /4rr l, P (A, \t, /\r )2 saozlnttah KecrL (€hrngg4 AapL Atatzt-
K4n ,ian /r4!umslK4n s4ma d'elgao 0 toot) t\4(4 Pa( sa$aal Aiata. dapq\ Al

t$tis (embatt loDqg4i berlKut

pr , p, * )pv.,
04n eerl4mqan tgrtQbvr l4Pat dtltn^L bqhwa Q')?" ggnlnqqa rtvda a\4ar
Wrqetu' dL(i pr m(0ujv p,. ?etgetuKan r[uida inr mgng4Kibarkan tgr4nan
Ai A^lafi\ \tJaLg( Ja.r Pump rend4h tLo lgbth fgndah Aa(i?dda LQ\aooo tlt \ra(
uJaier le1 ?ump . qohlnqga \,et\010n \,7a(a dt atffi}\te( men/oron{ tlutda pado
srntQrcf0ts vniuK iuru() /4n maluK t\Q dalafi \lalQr i0t P'rmP a40 mpmpQraepar
ProSQ.! a4l4m ppogefl ng4n Qndapdn,

Iposen- 0orpn trlrxa i 156 , 2011 )

I j 2 OK\*\arO(

6a$b6( l3 2 eKsiKaror

EK!i(aur aaauh SQbuah ujadah (ac, bonuu,p \anq ditanca^q

Untu( men!imp40 Ob]Qk dat4m sllatu 4tm0(ter |(ering. Ei4EanT4 g(siK4t0r ,{i-
isi leng4n suAru bahan pen4ertnq.SgPorti Kalsium N\or ida anfll.drutt qel,
\\tiKo, 4tomlO4 ,don t(A[qium Karbon4r. sebudh gK(iKator jugA serlrg 4i-
gt(a(afl u0tlll( menqorin4K4o ben4r -bQnar 1ai' ?4d* unt\,l{ anaLltlK z(on un(uK
ma[\!d t4(n. Dporasrnga Sang e+rsien tgr$nruno pada baaat Pengerlng ,l<a-
rena iw b4hanini di?e(bAarui dd\a(f ggtanq \riaKtu Vcnq rerln3,
^atu\air terl,at! Un33t .
totutaMa liKa Kandvn{an
IQ.(Aq pq A\!a mQKrnrsme $e(Ja !4n{ \qiadi da@nt OxstKator. P0r'
t^tt\a ojAldh mQ(anism€ fisiKa. ProsQ! Fist(a tni lQri4di \eca( a adgo(b sl
a^abati\ \aoq Dera.u PcnqQfa0an HrO yng \td^t< AtsVLd Aetga(l pefPtnola'
hao K4trr h^l( /arr (isrgm Ke LIngKung4n MauPUn Sobal"ll1o$4 , Qada mQKani\.
me tni lorladi \\!ott) diman4 KonsQntraci va) Fda bagt qn ara\ lQ'
^eadddo
brh berar dart {paa batlt^^ Vwdt\ . \enryXa lla) a\aa^ Lrt)(\ d,an ata\ N,Q

baurah . Pefl srlr^r4 ini /rsobut Jug4 /n!rng t{oo. lQr4njurnVd

ForcQ Concenrra
$(laai mer4nisYne Ximi4 /rman4 fe4t19r tl:O Aeigan bhao pgngorlng/ Se-
Suai a.Qngoo rea(ti beriKUt -.

tl:O(t) I faco3 $) -------+ OO(s) t \t CO ztaq)

tl, CO 3 (a1) ------------+ H,O 1q.l t CO, 19 )
CaO $t r .z HrO({) ---J C, (0H ), (}) t H: ar)
Ktnrudrao Ca(0H)) /(an bQr€al(si t(ombrLt denqa\ ca) seluai lmg4A re'
a(si bQr lt(ut .
Ca [okl ), cs) I CO, t9t Cz COr .s, r Hiotq)

lUo,i"a, , tor ,1993 )

u ME1ooo L0 6 I

I 1. Aut lj z b aaaa
A\4t -at4t Uang At4 unal{an Whe^ - baMn \qnq A!)na^ao
/arrm Pr4[tiKUm \ , adovh I ,laLrm praL(l''t t{Uan iot aalo\a h '
t. g,oE[ I FQn0t
Penlmbqrq ro mL lbuah ro,oo9 gr4M

r [rbu ttourooce I I lh/ah , L4t!t4n HrSoq Q€l{ot \5 m!

3 Piget u$u( ,9 mr I buah 5 La(ut4n YNO 3 PQt,(At 30 mL
'{ 0au.( barh 1 DUrh q At[DhoL t 2 5 fi&.
L Sroterrru(! I budh 5 E9 ba.t\t sQ(lrr lpnga

6. \lalx( let Pump I buah

1 goro[ Peocu[i t U]dh
g Pipot mar, r budh
o. Uare[ pen0hisop r buah
to Hot ptate 1 buah
. E(stx^ror r btuh
r: 0ven I h bu4

13. Hetoo Anal.rt{K I budh

v Pel,elddt( 6aca
19 goaKQr 6La(r
\b larmomeLQr

! a. Pro\ertu r
prolerlur pra(u|(lJm lnr Ada\ah :

1 t4snlatoPt(ao !in!Stcruls a'n men9e'eK (rol.qrcru<(

r Mgt\rmbaoq tQnoL sebanlax 6,ao, {a \ /pogan boLoL ponrmbang Qaolo

^Qraca

3 Mem4!$(K4n rcnoL |1od4Lam Labu pLof4nce Aal' $ef,ahba64aa H:soq sebangax

ri tatttan datot, l.!at,er bath V4og tersuhu loo'c (gL4ma l5 mpnrc

Meo40a(v(ao
9 Mgndrn.J'qr^4n taruran sarhpai !!hu l9oL
6 HQtnana((an L4cui4n ,l4n mgo4mbahKan l9 m! laautao HFlos pQKdr loal(ig
AQmr e^!(rt daq t!0ggu ta(rtpat muncul Kgmbau hiLan{ lomPa'
^.d? Yang
50 menit

I Menguung\ Lang(ah 6 z{Qngao riNo3 lebanlaK lo mL sdMPa' ,om€0iL

3 tlacg$langr LaogK4h 6 /eng40 hFlo3 lebangaL< 5 mL !ampar Lo fi€n(E
g. trendtn4h(ao Larutrn mengguM(an ur4ter bsrh tqfltr es hrnqq4 luhu 19'c
ro !4enuao0q Qndo?vo Aeiqan !rorcrc(u(! aQnqan banwa0 uJaLer ler P'rmP
ll menrucr andapan de09an t te\!! etao0L ancgf
t, m€md\lKKao !rnLgrcau(( be(t(l endapao (e dabn\ o\te\
B Hemo!u(Kan linbercr!!! tprt!r pnd.apao gang teLah dtoaid\<art te daLar.

lq Me0)mbaoq berar asaM pt(rat yong ,lrha(iLl^4n

! q ll(Qma A[at

Eambar ii _ t{ 1 lr(omo Atar ppmbuaron Alam Pii{r4!

:tl I,I As IL OAH PEMgAH(AH
|ll t tl4siL 9ra!(ril(um
S€rlf,ut ini aAalah aabel harit Pf4(tlKUm
T4be[ ltl I I Pe(tbah.an Wdha
NO Lan0Kah 0Q( cobaa^
uQnqur(lr mas!4 Fenot 6€nrnq , I(€ 6$ah m\r/aao
, I't0ncampurKan 6 gtam FQnot ,{engqn 6erN4r n4 ke(oHta ran
I5 m[ tl2 Soq 9e(al
3 MemanosK4n lAruun !,e (ama 19
g€t lr)ar na !QtOI<tatan

mQnit
q M€nArngin('4n lactta^ sdfipqt lLetwatr|.d KoLa6ta0t ?aK^L
luh\t 19"c

, }{enambahKrn HNo! tq mt /40 gerlr)ar[4 mgrah $etol(taian Pgt^aL, ttmDuL a-

AlPa$asy'ar| Sotam4 Eo m enir

MQn4mh|4hl^an HNo! l0 rYt\ aan
Ai pdnL\r'/.,if. sotama 20 menit
'I
{eMmbah{an HHO3 I mL /an
di@naty.^i Sot4ma t0 Menit
I UQfldingin l,(an VtUVn k.t{\qgd
s!h\r 19.c

5 U0ngarrng enaapan
lo Hencuci O04aPan del'qao AqvadQab !t0r4h oar4
It. MQncuci 0ndaPan r tetel et4n0L
t1 Pemandsan dqo AtAiamNan dalai\ l(u nr nS

e(!iK0t0t
Tdbet rlr r 2 Aq\\a lqrlg Aida?^r
Nl) t{omp0nen M4!Sa C {ram )
no!s0 sin t€rc(u(s K0!0n{ te, tl qo

Mas!4 sin [6crutr , vndapal 20, t5 hx

3 Ma!s, 6oror Pgnr mbanq l(osong ,2, 30Xg
Balsa Soiot P€ni baog t Fenol 28, 3t\8

HAsrL 9e(hiiunq4n
AgrtKUr lni Aratah t4bel hasi! Qerh\{ung4n
Tabet \-r 21 Haltt Pgthr!vng0n
HO U gteranOan lla!r\
I M0!!4 t€nol G,ooe q(a$
Ma!so Alanr Qiwar, (Ee,dapan ) 2, L\8)g atafi
1 YieLd (t'ro.t")
q Yreu I r'1ol ) 16 , !.2 ,b
 ru - 3 0embohasan
0Qr(obadn pembua!4n asam pi(rar rni adauh untuK nenpLlaiari pgmbuat4n
4s.r pr(r4r do(i tenoL dengan rg^(!i lrrr.fonari otlh urur4o H2!oe pQuat aan w(si
nitrasr oLQh t4(w4n HNo. pe|(at drlortai cufiar.atao (Qfta ,ugnohilun{ ltetd dafi asan
pi(rar !4tr0 terbtntt(.
ditdrrra1 gattu metirflbang boLoL penrmbang Koloru.
LAoqrah PQft.dno \laoq
Saat, Elenrmbong botoL penr bang /rs&t4i m€masuK(an siftgrc(us! long \Qt4h diLoba
(0 d4taF olQrl, at iqi bQrtllu4n uftuK merglrpKao tat- 1a+, ya(\g mdlih mgnempet 4tru
+pJAqeab Pqda llnietatuts miSaL UrO. Seleuh rlu (r0fr(rus( ArmasvKKan \g datant e^-

sir,(4t0r /en9a0 rullr0 r(dodlng4o 1.at -aat pQwa(t\q$ leperu H2o b€na(- benar hilang.
(eMlljdrao Sln{g((!S! Kolong b4ru dt ffbang pddo letoca o^aitlK. glqrndr,an (QG@ ata.
Litlr (4ren4 arsLltil{, (arana Aorqco af|dugv m*ooa$ao iotlfumen u4o{ a(urar lcng
nQfa@

nemiuKi (gmampuao mQodetgKri boboh poaa (lsara., too qrarn sd?nPai dlngao , o,ooot
4rarn t! 0,r mg)
( Unaeroooa , Gos , too-\
r\Qt\\ldtdn lidapaL .hasto st0tgr[rula $o\ong adalan 18,17qo n(ar,,dd\ m4r(a boroL

Penimbang (oconq aaaluh 22,a098 {a?o.

[€mua|ao mQngdmbL Fenot Vang ingin z{tgUnaL(an. t14.!(Kan ve dd\an bDrot

000lMb4n4 tatu dlbit bins.oldrpatk4n M4s!a Dorot ponimbaoo r taloL adatah 13.lttt3
4ram .
l€hlngga A4apatqan rrw(a f€noL sebanVaK 6.oo5a.am. 0tjuna(rn^ga bobo!
pen\n\&tv dddlah t<dr€M tubano botoL penlmbang Lgbih bolar ztanpada .I<nolrrenu t
\ehlngoa Lebrh muaah memafut^tl{an ponoL dan boto! ponimbang mQmlLt(i lur.op SQhrng-
46 fenoL u/aK m\,rlah igfl,(ontamllaci /(arena FeooL mudah !e((ont4minost /a^ rp.flhah
uqrna gan€ 4agaL\la petcobaan.
mengebabr<ao

souojurng4 memalvK(ao FE.,ol 6e aavY\ Eabu0q rt0r00.g adn rnaoa$bahKao

r5 mr La(!t4n $jEo{ ro aaLam @bu FLo,oncQ . oel'a$oahal u'\oq geua+ adalrh ltnwK
metindungi FenoL dati oKstdasr oLgh 9d4(d s*ot bArQat..i AQnMn Hdos ndnunlr4,Kaae-
na oKqdasr 9/o4 rQfuLo nebat. aQolan fitlo. daPAb Mengebabrun Kgrusa(d0 genva-
t!4. tarltan Haloq /llambah(an torL€bih ,vhuio KArQna Ar\o4 n oP^v\an $edla ?Q-
n$rasi l(4re04 bglot)oa serp,n,tt t€(lonl(asrog4 HHo6 mgNadi Flor'.lon Nori ini haror ar-

b€n!u( terLobh Arhul0 aeogqr\ menalrlr)ah(an H2l0q.

LangK4h SOtanjlrnga memanalK4n V(\aat\ dtd\ai' labu rtorenae seli?m4 rE me-
nit,, [-auu 69191164 at€un4r<rn (a(en, b€ntu(0gd g4n0 buLat t4ipa $raut mavk pennqd!^an
fo|b|h MU/ah /tu(u|(an rarena pe0qartu(an uanq mrar4 Lgbth cep4r la.\ad aon Nana,Ia -

54n lgbih mgrara .

(loLomon , n1u. tot)
oemanasan inl aiu(ur4o /r(orrai Pgnqad0(0n /eoqao 1n6i roo.c. saat pQm4noran rJ(omP0Elll
4!om -Q F€floL lutFona{ ldlga\' tlnggi Uoltu {0"1' ,pngan agam-o luLton& h0nga t0%. sghrq'
qo tanqK4h {,gl4nJUthU.r 94ri! mgndinoin(an t rutan hingga suhu l9'C $dng bertuJoan
u0t\rK m€mpercepat Pembgnt'l(4n atd$ o(to aSat mQmiLl[r k0mpoli(i (nelderlali ataq
P^ra ,9ang aKon meng4(ibarkan reo[li [aniutao unr\rK memboour( J,q FenDtlrJLrona{.
^Ua
0lma oa (ompoli(r laat suh! \5'c alam -o FgooLlulFooqt tt4,h aan a\an p, Feno! llLForvrr

Fellgnde0, qrt , tss6 )

9Qr@baan /iLa^lut\,(an agnqa^ nrrra(t uatru ponafibahan HHo3 pe(ar sgdll^ib d0
m \odi(it arau bpruhAp, H Os diumbah(dn Se^ao beftqt.gp l(ar€M r€a(ri Aatt pembtll
tu(on pl(r4l *Ml(i ado 4 iat'aP adn iri/.La ditd$b,.h1,\an ranqsJf.q Atuu terl4Lu banuEx
diraKv.[an 4,(ro meoghasiu(o0 +,etll/.! ha^$t< €4s No, U4og bgrbahava jiKa tgrhrrvp
adn dit4KvtKqn ubu f Lorenae a^on peah. Tujuoo .0nambahan Larutao HH0. p€rau
4aordh unrur mo0(ubs u[i irrgu( Ht a4t4m o-FemL suLEontl{ d€ngdn No,. pen4mba-
hao PQrtama gaitu m€nambahr(an HH03 tgbanga( lgmr lQdl{tE demi ledtl(lL sdmbrt ai-
aa\)^ Ai ddvfi1 Ua$rbaLh rSoog dtLoKu(ao setoma 60 menit. QQ0xsi uonq *( !a^ a&ttah
qlqus N0, mQntubtiLusi Hr . 0lm000 pada req(si lebeklm0go goitu re4((i ltrLFon4lt aengan
0emonas06 dan pendtrlgindn tgl4h mgmbuat FenoL menJ4di r,4 tuLronr|( . Aea((i nrEfo-
sr (ooud(an lorJaai. Setet4h itlj tQrjodi iea(li nitra(i,pert4na d€ngan men$rblltrJ sI xan
Hr refuhh dahuLu d€ogan No,r. H4Lini tgrjadi K4rpt4 l(aian c-H tqhh $rda}, dt.
EQIdoq dan rers'Jbulusi pdtla at^tr da.ipda iv.ata^ C-9,
(Fldno . llo , lq6o )
$a$L gong.lidapar adatah \e(bQnv.!t/( uape(eur! Uop loi tBrbencoK datt ( pzuigi
cota@ Nort acnqan Hfsoq . Terb€nr0Kng4 uap co(eLa! ini mQnuNu(kan bahurq Hdo. tpr_
\trar dlan Lersubtrrusl Ke Ofro- dao paaa- fenot(ULfoniK ,(eMvdt4o mombgnuJk 4Ar NOr
$anq be{uPa uaP beruiafn4 (o(0t4t htmQrah4o ara! tiQ,tatge-AO.
(luchr,a, .56, r9?3 )
$tantltnga dltatr$(ao \aqi 9eoombahan tdrutan HNo3 Wdc acbz.ngav ro fiL
ddn metaku,(an pem4Msan \e(ta Ntgodu^ai seldma 20 meoit. ?oda pQ^ambahah !(e-
d|d inl gugur Ho,r m€n!uu,r,rrusit^an P-ru!"fontr menJadi P-nrrrot€noL,(Q(uqi /ongan
tahap4A niiaasr b4h[ra e'nltroFeoD! a^di tgrbenLuk ter[ghh 44h0Lu dqtiqdo o-nro
(€noL ,dro
tugu! NOrt 4(a0 bert4mbah dLo b}(qQ\e( .
( Mann , tro , tlloD )
tlqlrl ara4Fr 4dal-ah terbentU( UqP mrur4rno .0l{0[ab Sanq menot\JUh
Yqog
Kao rQaKli 4niar4 NOrt dengan H:SOk A4mun LQbin Sedtt(rt,(Ar€na HrSOq dan NOrr
laog bar€4((i SQmat{ro sedir(it.
seufu\,inga ,tl4rlan Pgnombqhan La(ut4n Hdo. seE ollar( I m[ sedtKrt,la-
ml leai(it aao mg,l(ut(do pomAoamn rplt4 Peog4du(,n let4ma romgoiE. Podo ?a^onba-
hoo (0tlg.t , 9uqlrt Ho,r m{n(obtlurll 0 -(l)!gonik .npnla4i o -orrfoEeno! sehrnqga 4lha(iL.
Kao ,,q.b- ErtnlrtDFQno! Ara\, oram e(rat. ?r0Q( ioi mengha((Kan sedt^it u4p ber(Uar-
n0 oKeutt ddn t4rut4n bgruMrno me[ah l{QioKLaian.
(M4nn, rl3. tg6o )
L4nl$ah (etAnJUt^!a adAL-rh mgndtngrn(ott lAat!l,a$ hin{ga l5oC. fvil.ronnga
arl.tah loruv monutunl{an l(e0ru@n sehr0gga diAapawao oodapan g4KmaK(llna!
4aN Lebrh ban$au(. P4d4 Ptosor \ni b4rr, [ef lihar o0/apan gang befurd.n4 mofah
baEa !(qm!(tr'.tan Podut t^fllln beruJorll4 mof4h t g(o|(taLao , f,ndrpao $r!€bus
meruP4lun e0dap4n Pi[rar zrrfluno lni /tbont,u( ufitoK 'nen dopdlKan led.
earlatten
A\4sa0 m00g4pa penambah4n !0rLama lang FUng bqnuar \laiur sebangaK rs
mL t^are(\d

lgteuh vrutao berluhu rg.c endaoaa dtsa(inl mengq\rna(ao linleacruq( aan

baniuan Lu4ter let PUmp. wAte( lat f,JMp dlXuiakao UntuK mem pprr(/gpaE
0r0ler Pen!4rin9an . selanit]tl\ga endapa^ At(rtltali!ari ooh euanoL !gb4,
ngA!( 6 tore( . TuJvan Aari QLnaa bah^n gtanaL gncer Vnt\)K ( L\.a -
^daLab
NtKan Pen90t0r bgruPa l+,(,0q /an HFlo. lefta menqKrlltaLi\asi e(\dapan
dtNw a pdaa |(flrraulaai tnt Lorjaa celbedoao f,Lta(trao \ ?i.tdt
^nt^ta ^ra
aenq4r pencamPutan n{a ,4(am (rat toi [ebth rrriav la(uE do\atn etanol,, EranoL
lnl mgmumr(4n eOdAean dlao momi!4hKan 14V Fdah ole\gan taE patub Lanrlla.
Eihaool i{4a $Qmo olahv(an dalarn pqzngo\lgnan 9(a(On, qK dldlhtrva 1g.3.c !g,
hrrlqg4 tidaE rngmbJiohKAo NaK\U tlrt4t! [ama Untuh menguapr^ao Wtat* datarn
olen .

Lfelenapn , eor , t$a )

SeQUh Ondap4n lQr(uhp\rL adLad svabu !tnLer-Cau!. , llnlercrlJ!! gdng berr
t g\dapao dtma$r(L(an Kq aaLam o\,en lOlama It mon[. -t!lo4nngz, a.t^Lah t^-
b\it( menqer(ng(an Qodaean da^ fi\on€!4pxan t& 7at ?e^qgan gs! . lereuh /,Maruk
v'or daLafi oven ,!to(pr!ru(! qn AaLam eK\Va$( , Yoog wlvannrja a4arrrh
^teta6
uo\uK mpnghlLangK4n peuauL Y4ng ma(rh \Qrada dt
'.r4p
dal\i1 lirtllrar!s( ,atman4
uaP rnr AlrkaL Aleh (aA Aalam et\<t\afi( ,
ttlqrtadr , lot. 1933
soteLah Defaaa aa[am eK$6aror d^taff, $aen-r r hAri
,stnLQrcr!!5 dlr(g
tlarkan d4n dlumbanO maslanY4 o gar, d\t Aap!2iwai lnals4 ltn r€fcrv!( \ qrdapdn
ad.^\ah )o, Brhn .a(afi .
oari Petcobaan ,{an Frhru.lngan {4^g tpuh dilaq\)(a(, , AapaL Airt (\p)t.
XaO bahwa 4!am Pivir4r d.ap^ Aibrtrt, dArl ronoL apngan rerK luLtoAa(r OtBh t,
rut4n H:\0q ?eKdr aoo r€aKsl nitrasr O\gh Uru€an HNo3 peKAt /r!orra' pemdna.
ran, drmana U\QLd m4(94 !4nO drpprotph datt a\on pi((4! 9aoq to(bentu( alaL4h
\t , ar'l" Aal \\eld $ot a^a\ah \Qusat \to ,qt 'b

ber da\att\Ai ha![ Poraobaan dtqeroLgh ha(lt, (eh4gar bgrit(ur ,.

I 0l(r4r d.apan Atb\)at Aari FeooL dQt\\a^ utq loLfonacr ,la^ oirra{i
Asam

, Alam pr(rat Uano /tpS(oteh lebesar ,,qdrg n(arn d enqa\^ lrekl lv\ar(a
\sbes4r r'1r,35'lo dao ltetd moL !Qb€!a( 11,,02 '/"

ON FlA R OU\IAKA
ooran - dOS€$ Ei tt(a FtttPA lI5. eou . "Ftslra ! l(r n€matlx4 - or nami( - 6eraran
_panac n . Surabaga . Yatlartr<4 l'I !
oos.cA /an A-! \JnaotNood foor. rr Anallq! (tmra (u4n uLtF Eaict KeeoaM,,.
l4xarta E(v^gga
Ee!(gnden , Fe!(endQn . 1582 . 'r kiml, Organt{ liLt/ 1 !. lat{afta ' €ttan. g..
6e0rgg, ur 6o(eL , ,ooq . 'r 0e4n,s llaolDoox or org4nr. ChSmllrrg ! . NerJ Yo.( :

Mc6rauJ - tllll
Ha(tAdr ,{,1985. 'rlLm0 Krlhra AnaLi(a oasar !. lararta 6ra $ed1a
r\aon, tederrL( 6€0rge , lgfo . " ?eoc,loat A(o,antL Chemitr(y " . Lond.on I lo^gm.ro
\nC

lvlarriloo , R0b€r1 {hom(00 . )ao2. t'0f44nta Chemr(tr$ " . rleD oeLhi Pr00uce
0f \nrl(a
HaLl
Pivar , Hdm!\tt. 1389. ' Ata! Ppme Klaan Ktmta { laKdrta : Ul pRE((
Sofomon ,'I u) |tahafi ,20[ ,,org4nrc afteml(!r! " . USA I J0h0 tr]rL€U { !00!
lnc
Svehu 6 . lgl5. '' Anrtil! Anorganrx K!4qralrr ". Jono."o r Qt xaLman
He4l a pu!t4K4
 AP?EIIDI14!

!\atsd : 22, aog8

b0t0L peotmb4ng
Masta boro! Pentmbang + ter1oL =
28 ,31t18 NQfi
l-) i4alsa EenoL . 2E , A\qB - a2 .50€t =

i^a$a srnLg(cfu(s a $, a1L1o lra.n

marra glnlerc(!!! t endapan : )o,ar6q $ram
L+ a!!a Vndapao LArafi p'\ra.) . )o,g56n - 16.Zitab , 2,4t)9.Xr4h

m0l asam pr(rar moslo A !arY! 9r(rZ o

6M
)9
2,118

a2q, \
: 6,010?
m0 L Fen0l ma !s4 FenoL
6r.1

5q
. a,ob 38
t--+ yieLa moL asam p,krar moL 4(am pt{raL a,o t1g x roo./.
m0L Fen 0L o,0io 48

Y'eU mosra aram pl(rat : mossa asam plfirar

ai1 ' Po"r"

LAMOIBAI..I
 LABORATORIUM KIMIA ANALISA DAN KIMIA ORGANIK
DEPARTEMEN TEKNIK KIMIA
FAKULTAS TEKI.IOLOGI INDUSTRI
INSTITUT TEKNOLOGI SEPULUH NOPEMBER

I,APO EMENTARA
PRAKTIKLIM KIMIA ORG 20r8

Modul PraLlikum PqrnrruZrt,'.' ecam fiL[.t

Hari/ Tanggal !€nrn is Po\,€-rnbLr )o\t
Kelompok xlv
Nama I tqsM\ CqlrriY,qa\ p N
. NRP o )) trl
r]c{rcul6t

2 Rgryldg Solnci_r5 te\1ca NRP 0unlqcsrlco

NO Yang diukur Massa (gam) I Botol Sm ref,,,

1 Ir{cngutur massa fenol
te . )cn 6
2 Monoampurka n 6 gam lenol a),'l 'OO
) ), a0q8 qtLtn

dengan l5 ml H:SOr pekat

2,t ,3c.96

Fenol b, aot I hc\, 1. rlnhrrnq I le nct

3 Sintercruss \( r+4, :i ilLl6
4 I Sintercruss + endapan asam Ji :', rtl! t8,3|t18 ai^ff
I 2a,3rL1 .l,i I Lr)
i pikrat
Endapan asarr pikrat 2, Ll9 )g , \r\t€(i(!!\ \ l'nLitl?at\

)a.3i11
)a,8t6\ )at8 rbrl 9taa
No IvlW mol I
)o ,8 910
l Fenol 1 q4 O,c.o)$
2 Asam Pikat ra5 0, 0l 0{,

Ygtd uarsa
----
),A82q \rcI.1, Asisten
gietd m(l!s4 ,
6,00b ALL

qt, 6s'1,

Yeta t',t0,"

0r0l0b,,06"1,
UieLa moL .
0,0638
 LABORATORIUM KllvllA ANALISA DAN Klt\illA ORGANIK
DEPARTEMEN TEKNIK KIMIA
FAKULTAS TEKNOLOGI INDUSTRI
INSTITUT TEKNOLOGI SEPULUH NOPEMBER

LAPOR{N SEIIIENTARA
PRAKTIKTIM KIMIA ORGANIK 2018

Modul Praktikum 0gmruatan Asom 0tnrat

Ha / Tanggal &n / s {o,lurioer &lg
Kelompok x \,'l

Nama I l-gr:ml ahYTllgllt

p?n9td!a:
l' NRP
oa,,'Jlqaoooa LE .

2...19l1\a9
s
NRP
Orruiq00OolOO

NO Langkah Percobaan Hasil Pengamatan

I Mengukur massa fenol D tn\nq , (Q m((dh m,iddan

2 Mencampurkan 6 gam fenol dengan 15 DQTQATnO 1^QcDX\4!4 n

ml HrSO4 pekat
3 Memanaskan dan mengadul larutan UrN\[^n beldari0 (Q(0! tal4o pP(,rl
I

pada suhu 100"C selama l5 menit pada

labu Flqrence dan mendinginkan sampat

suhu 15"C

1 llenambahkan HNO. sejurnlalt 15 ml hc((x6c(\o mQravl t^€(al',1\(rtdn p(Kal

trm[.u\ nlaf tl(fL{Ofrc' !/un,rq vo'
sedikit demi sedikit sambrl dipanaskan
0(4ngQ4O
selama 30 menit pada suhu 100.C

5 Menambahkan HNOr sejumlah l0 ml 6OroJarfno me(dh l^Qcol( 14lan PQl(4[, l

sedikrt demi sedikil sambil dipanaskan r\$1bu! asaP bQluJ4ln4 (\)rroq $€

selama 20 menit pada suhu 100'C

o{d0qern lQAl(lL

6 Menambahkan HNO, sejumlah 5 ml I bet$arno motah lQlol^Lat.an Perqt.

sedrkit demi sedikil samhil drpanaskan .umb!! alqp beruJarno lr!fl\og ll(e-
selama l0 menll pada suhu l0{)'C 0range a0

7 Mendinginkan larutan dengan lap basah l^Q(chIatao

Mgfoh bal4
kemudran dengan arr es hrngga suhu
 l5'c
8 Menyaring endapan dengan sintetcruss AQtot, bTra l(Q(ol,(t4rao
dibantu dengan waterjet pump

9 Mencuci endapan dengan aquadest . ] tnzlapan be(wdrn0 mprah bota ke(okt4t4[

IO Mencuci endapan 15 ml etanol 50% di fo d4?an bQluJafnu mofAh bau
sintercruss

Asisten
 MSDS
llari/Kelompok : Senin / xrv
Modul Praktikum: /embuatan Alom Pit'(rar

Physical and Chemical Toxicological

No Name Oormula) First Aid Measures
Properties lnformation
! -r0 [id - Karsrno{gntK - unulK mata 440 [r]_
Fertol,
- Nar0anVA beni{19 - pin( - m€mbuab lribosi /4n Lir bal0hi dongan
arr lJong banYa(
- bo! Khar K0rO\if
-iiKa torh'ruP Pin'
Aah $e ud^to s8'
4a(
- tit{o t€(gan ,l4nro
/rmunt4ht(4
Ur\0r p€Kat - tiquid [D'tU tiquid thlc() - K4(slno{€$rl( - unttx mata zla o

- {tuu ada batJ +aqi (o- - mQ$hjai irimsi dao (utit baqhi 1€n94n
t/u ?4MS men€KiK t(0r0si€ ai( v4n4 banua|(
- UdaK b€ru)arn4 - j$(a tarhirup. (0S-
$ I\i(rp rdatu seqt
- iixa tPrtt !an, zli
\JlAha}(ao ria4t mu0-
tah
1 HH03 Pet<Ai - u4vid - membuat lri t4li - li$a terken4 m4M
- b4lnga KUAL /an t{oro(ir /4n KUtit , U!^ghl
- uarn4 beltoS - t(unin3 AaWn
^l( lonq
hrnuax
-J\(a r0(hr(uP. 1e9Q
fa hlruP vd4ra le'
qa(
- jiM t €r toun. ri
\SoM$o( tlAa\
munt4h

q Atr(oho ! encer - \iquid

^ grsa m€mbuai -.!ll(a terKQna rY'At(
- berbau Seporti gronoL trit/sl dan kutlt, b4r4hi
aan , ser0n .,t0094n ai r \ang
- Pahit, b4 n
Ual^
- trda( bQru]arA4 -Ji(a iorhrftP, re'
{€ra hirup udq-a
!egar
- iiKa l,ofteLa0 r

di\\atfi(an isdar
m lJnt/h
 fusk Assesment
Hari/Kelompok: S s nrn ,/ xrl1
Modul Praktikum: Asdm ?iKf4r

No Problem Possible Consequences

Causes Action Requred
I Torjadr K€rPtdK4n pa- KeLemb4b4n hanl# lat\bao lang sedonq sol.rt'r ee.rhat lK4n
Aa $aAqh S44t mefiu. \Adt6iL lal di ?q^4,1,^ao A awrtt iin{K4t f.€tPm bdban
n4sKan urut4n .di igr$ena ?arus daiah boco. dan Paa uedah -\a n

Pure Ebih 4da KPm un{Ki n4n Panas Yahg arK€lu'

vraolah peu.t1 )a(r ttot.?t ue
^(wr
I L4(Ut4n H2Soy pQ(aL arutan uz!o!
?faKtlKan IUr/rg L po_
NetratKao a 0n9rn
tumPah laat i0q ln hatl -h atl KAt /4pri m€rus0l{
ber \A{uLa} \Ada /
r'lrroaKslKan mgngamblL Lanrai t\4reno slFat0 K,PUr , (€bQUm Al'
adn rqr buro -bufu sangai t(0rollf ttrdm 4lr

b Kaot pon$hrs0f t(daH adaitlo Ai. tuKar rarot

^tt \l4au tQI\adotnud tgqera
Wff \t{t{sl goal 6p;a - {or,qTa
^o(e\ 1,^t ?dAa 9,a\ ?e- P00g hi
sqP mgtalu'
Nl^ao poog4Mbitan hlsaPkar0r tor -
,
ngamDiuo bav!4 n A\iStom Ubo(at0(rum
?A KonMmin4 !r ?at
o.n{g UnaKan Fp0r seigLah metol^ul(on
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 TIME SCT{EDULE
Hari/Kelompok : Spnrn /xlrt
Modul Praktikum: Pembuatan Asam prl{(at

No Waktu Kegiatan Nama Pralrtikan

MoluK tllb. Abspo , Persiopao Prat,l. rixan

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