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CHEMISTRY LABORATORY
REPORT
EXPERIMENT 1: CHEMICAL REACTIONS
Group members:
Total = 15 points
The report must be typed and handed in together with the signed data sheet by the deadline
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I. Introduction (1pt)
When one or more chemicals, known as reactants, are transformed into one or more
new substances, known as products, a chemical reaction has taken place.
Substances can include things that are chemical elements or compounds. In a natural
process, the atoms that make up the reactants are rearranged, creating a variety of
compounds as products. During this lab session, we will learn by doing, observe many
chemical reactions, and learn how to categorize them. By making observations, we
can determine that a change or chemical reaction has taken place. Different chemical
reactions will result in different phenomena. There are five general types of reactions:
synthesis, decomposition, combustion, single displacement, and double displacement.
.
Step 5: Mix tubes lightly and wait at least 2 minutes.
Step 6: Observe and record the result and clean up according to instructions
b. Section2: reaction of potassium bromide
Step 1: Prepare 2 test tubes, 0.5M KBr, 0.1M AgNO 3, 2M NH4OH.
Step 2: Drop 10 drops 0.5M KBr into each test tube.
Step 3: Then add 0.1M AgNO3 into both test tubes.
Step 4: After that, we continue to put 10 drops of 2M NH 4OH into tubes no.2.
Step 5: Mix tubes lightly and wait at least 2 minutes.
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Step 6: View and mention the result and clean up according to instructions
3. Reaction of H2O2
Step 1: Prepare 3 test tubes, 0.1M KMnO4, 2M H2SO4, 0.1M KI, 3% H2O2, MnO2.
Step 2: Add 1 drop 0.1M KMnO4 into tube no.1, 5 drops 0.1M KI into tube no.2 and 10 drop
3% H2O2 into tube no.3.
Step 3: Then drop 5 drops 2M H2SO4 to 2 tubes no.1 and no.2. In tube no3, we put a dash
of MnO2.
Step 4: After that, we continue to add 3% H2O2.
Step 5: Wait at least 2 minutes after lightly mixing the tubes.
Step 6: Observe and record the changes, then clean up as directed
4. Reactions of Nitrate
Step 1: prepare 3 test tubes, concentrated CH3COOH, 1M NaNO3, FeSO4, concentrated
H2SO4, 1M NaNO2
Step 2: add 10 drops NaNO3 into 2 tubes and 10 drops NaNO2 into the other test tube
Step 3: then, put into all test tubes 10 drops FeSO4
Step 4: Add concentrated H2SO4 into tubes containing NaNO3 and NaNO2 , and add
concentrated CH3COOH into the remaining tubes
Step 5: Mix tubes well and wait at least 2 minutes.
Step 6: Observe the changes and make a note of them, then tidy up as advised
5. Reaction of KMnO4
Step 1: Prepare 3 test tubes, 0.5M Na2SO3, 2M H2SO4, 6M NaOH, distilled water, 0.1M
KMnO4.
Step 2: To begin, fill each tube with 10 drops of 0.5M Na 2SO3.
Step 3: Then drop turn 5 drops 2M H2SO4, 6M NaOH no.2, and 5 drops distilled water into
tube no.1, no.2 and no.3.
Step 4: Put into all test tubes 0.1M of KMnO4.
Step 5: Mix tubes well and wait at least 2 minutes.
Step 6: Observe the changes and make a note of them, then tidy up as advised
6. Reaction of Potassium Dichromate (K2Cr2O7)
Step 1: Prepare a test tube, 0.5M K2Cr2O7, 6M H2SO4, C2H5OH
Step 2: To begin, fill each tube with 10 drops of 0.5M K2Cr2O7
Step 3: Then drop turn 10 drops 6M H2SO4
Step 4: after that, put into 5 drops C2H5OH
Step 5: Mix tubes well and wait at least 2 minutes.
Step 6: Observe and record the changes, then clean up as directed
7. Reaction of Fe2+ and Fe3+
a. Section1: ferric ion (Fe3+)
Step 1: Prepare 2 test tubes, 0.5M FeCl3, 2M KOH, and 2M NH4OH.
Step 2: Add 10 drops 0.5M FeCl3 per tube.
Step 3: Put 5 drops KOH into tube no.1 and 5 drops 2M NH 4OH into tube no.2.
Step 4: Put into all test tubes 0.1M of KMnO4.
Step 5: Gently mix them.
Step 6: Observe the changes and make a note of them, then clean as conduct
b. Section2: ferrous ion (Fe2+)
Step 1: Prepare 2 test tubes, 0.5M FeSO4, 2M KOH, and 2M NH4OH.
Step 2: Add 10 drops 0.5M FeSO4 into both 2 tubes.
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Step 3: Put 5 drops KOH into tube no.1 and 5 drops 2M NH 4OH into tube no.2.
Step 4: Put into all test tubes 0.1M of KMnO4.
Step 5: Gently mix them.
Step 6: Observe and note the results, then clean according to instructions
8. Reactions of Al3+
Step 1: Prepare 2 test tubes, 0.5M Al2(SO4)3, 2M NaOH, and 2M HCl.
Step 2: Both tubes are dropped 10 drops 0,5M Al 2(SO4)3.
Step 3: Continue to add 5 drops of 2M NaOH into two tubes.
Step 4: Mix the pair test tubes gently and observe the reactions.
Step 5: Put 20 drops of 2M HCl into tubes no.1 and 20 drops 2M NaOH into the other tube.
Step 6: Observe the changes after mildly mixing tubes and make a note of them, then up
following the instructions
9. Flame test
Step 1: First, we light the Busen burner.
Step 2: Then using distilled water, clean the loop.
Step 3: Hold the loop in the flame after dousing it in the tested solution.
Step 4: After that, we recognize the main color changes of the flame and note them.
Step 5: We can calculate the frequency and energy of photons released during flame testing
using the wavelengths table
III. Results and discussion
1. Reactions of Cu2+ (1 pt)
blue precipitate
becomes lighter in
color.
generates blue
precipitate, and
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when pouring
color changes to
precipitate
dissolves. The
blue precipitate
dissolves
completely, the
Figure 2: the reaction between 0.5M CuSO4+ 2M NH4OH
solution changes
Comments:
- Cu2+ reacts with OH- to generate blue precipitate.
- The Cu(OH)2 solution interacts with NH4OH to generate a complex molecule, making
reaction number two dark blue
2. Reactions of silver halides (2 pts)
is opalescent
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precipitate
white
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precipitate
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yellow precipitate
yellow
0.1 AgNO3)
+ 2M NH4OH precipitate
Comments:
Halogens group reacts with silver, creates precipitate and makes “exchange reactions”.
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+ H2O2 effervescent
changes to dark
heat
Comments:
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+ concentrated H2SO4
+ concentrated H2SO4
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+ concentrated
CH3COOH
Comments:
- The chemical reaction between NaNO3 and FeSO4 and H2SO4 with the solution turns
light yellow.
- The reaction of NaNO2 after reacting with FeSO4 and H2SO4 respectively will give a
dark yellow solution.
- The chemical reaction between NaNO3 and FeSO4 and CH3COOH with the solution
turns transparent.
5. Reactions of KMnO4 (1 pt)
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color
+ 0.1M KMnO4
Comments:
In the first experiment, it occurs H2SO3, so that it would make KMnO4 lost its color in the
acidity environment
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C2H5OH
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Comments: Our experiments record that they are exchange reaction, especially, the ion of
each atoms is unchanged
Comments: All of the ferrous salts reacts with base solution cause precipitation
+ 2M NaOH appeared
precipitate gradually
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interaction between
the precipitate
gradually dissolves
between Al(OH)3
and NaOH .
Al3+ is amphoteric because it can react with H+ and OH- in solution. furthermore, the
formation of a white precipitate is due to the reaction between Al3 + and OH-
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The color change when burning these solutions over a flame is due to electronic excitation to
a higher energy level
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REPORT
EXPERIMENT 2: pH AND BUFFERS
Group members:
Total = 15 points
The report must be typed and handed in together with the signed data sheet by the deadline
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I. Introduction (1 pt)
(Introduce what experiments you do in this report)
Observed pH
Time
1st 2nd Explanation
(second)
(Group___) (Group___)
0 (2 pts)
20
40
60
80
100
120
140
160
Measured pH
Theoretical
Solution Comments/ Explanation
pH 1st 2nd
(Group___) (Group____)
(1 pt)
10 mL of 0.1M HCl
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Add 90 mL of distilled
water
Add 10 mL of
0.1M NaOH
Add 90 mL of
0.01M NaOH
Comments: (0.5 pts)
Measured pH
Solution 1st 2nd Ka Comments/ Explanation
(Group___) (Group____)
(1 pt)
0.1M acetic acid
Measured pH Explanation
Predicted
Solution 1 st
2nd
pH
(Group____) (Group____)
(1 pt)
0.1M NaCl
0.1M CH3COONa
0.1M NH4Cl
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5. pH OF BUFFERS (3 pts)
A 10.0 40.0
B 40.0 10.0
C 25.0 25.0
Calculation pH: (0.5 pts)
Comments: (0.5 pts)
A (0.5 pts)
C
Comments: (0.5 pts)
`
Part II: Addition of 10 drops 0.1 M NaOH
A (0.5 pts)
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C
Comments: (0.5 pts)
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REPORT
EXPERIMENT 3: REDOX TITRATION
Group members:
Total score:________/15__
Total = 15 points
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I. Introduction (1 pt)
(Introduce what experiments you do in this report)
Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)
1 -
2 -
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Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)
1 -
2 -
1 -
2 -
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REPORT
EXPERIMENT 4: CHEMICAL EQUILIBRIUM
Group members:
Total = 15 points
I. Introduction (1 pt)
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(0.5 pts)
Initial solution
(0.5 pts)
+ Conc. HCl
(0.5 pts)
+ 6 N NaOH
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(0.375 pts)
None (control)
(0.375 pts)
6 M HCl
(0.375 pts)
6 M NaOH
(0.375 pts)
6 M HCl
None
(0.25 pts)
(control)
(0.25 pts)
0.01M FeCl3
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(0.25 pts)
0.1M AgNO3
Predicted
Addition Observation Explanation
outcome
0.1 M Na2C2O4
+ 0.1 M H2C2O4
+ 6 M HCl
+ 6 M NH4OH
Description of Predicted
Observation Explanation
conditions outcome
(control)
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(0.5 pts)
(0.5 pts)
Ice-water bath
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REPORT
EXPERIMENT 5: FACTORS AFFECTING
REACTION RATE
Group members:
Total = 15 points
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I. Introduction (1 pt)
(Introduce what experiments you do in this report)
Reaction 1:
__________________________________________________
Reaction 2:
__________________________________________________
Mixture # 5:
(1 pt)
[I-] =
[S2O82-] =
1 0.08 0.04
2 0.068 0.04
3 0.056 0.04
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4 0.044 0.04
5 0.032 0.04
6 0.02 0.04
7 0.08 0.034
8 0.08 0.028
9 0.08 0.022
10 0.08 0.016
11 0.08 0.01
Plotting the concentration of iodide ion versus time: [Note: X – axis: time; Y – axis:
concentrations].
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Reaction System:
(0.5 pts)
500C
Comment: (1pt)
Reaction System:
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5 + Zn (0.25 pts)
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