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A transparent and flexible metasurface with both low


infrared emission and broadband microwave
absorption
Yao Ma1, Lihua Shi1, Jianbao Wang1,* , Liyan Zhu1, Yuzhou Ran1, Yicheng Liu1, and
Jie Li1

1
National Key Laboratory on Electromagnetic Environment Effects and Electro-Optical Engineering, Army Engineering University of
PLA, Nanjing 210007, China

Received: 1 September 2020 ABSTRACT


Accepted: 24 November 2020 Researches on radar and infrared stealth compatibility have drawn much
attention in recent years. In this work, a flexible metasurface with low infrared
Ó Springer Science+Business emission, broadband microwave absorption as well as high optical transmission
Media, LLC, part of Springer is simultaneously achieved. The whole structure is composed of an infrared
Nature 2021 shielding layer (IRSL), a radar absorption layer (RAL), a substrate and a back-
plane, and the total thickness is only 3.5 mm. Based on the impedance matching
theory, the microwave absorption higher than 90% can be achieved in the radar
waveband ranging from 7.3 to 18.8 GHz, corresponding to a relative bandwidth
of 88.1%. By using a conductive patch array as the IRSL, a low infrared emis-
sivity of 0.49 can be realized in the infrared region from 8 to 14 lm. Moreover,
by rational designing both the structures and materials, the metasurface in this
work cannot only achieve bi-stealth functions with low infrared emission and
broad microwave absorption, but also shows optically transparent and flexible
properties, thus quite suitable for practical applications. Both the simulated and
experimental results suggest that the proposed metasurface is promising in the
multispectral stealth fields.

1 Introduction and radar stealth compatibility (also known as mul-


tispectral stealth) has drawn much attention [2, 5, 6].
Modern reconnaissance involves radar detection, To realize infrared stealth, the infrared radiation
infrared detection and visible detection etc., there- intensity can be controlled by reducing the temper-
fore, multispectral stealth is essential for objects to ature of the body or by decreasing the infrared
counter multiband reconnaissance [1–6]. Since infra- emissivity of the surface according to the Stefan–
red reconnaissance together with radar reconnais- Boltzmann equation [7]. Based on the Kirchhoff law,
sance has been widely used in nowadays, infrared infrared emissivity is equal to absorptivity under

Address correspondence to E-mail: zwang0417@outlook.com

https://doi.org/10.1007/s10854-020-04967-3
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thermal equilibrium, therefore, objects with low by the infrared stealth layer due to its high reflection
absorption and high reflection are desirable for the property. Therefore, the infrared stealth layer should
infrared stealth. From the aspect of radar stealth, in be carefully designed to ensure that it has low
order to avoid radar detection, objects with high infrared emissivity and also little effect on radar
absorption and low reflection are required. Since wave propagation, so that most of the radar wave can
there is an obvious difference between the infrared transmit through the infrared stealth layer to reach
and the microwave wavebands, this provides an the radar stealth layer. Unfortunately, little literature
opportunity to realize infrared and radar stealth has paid attention to the adverse influence of the
compatibility by rationally designing materials or infrared stealth layer on the radar wave propagation
structures with a function of frequency dispersive and the infrared and radar stealth compatibility
responses. needs to be further improved. In addition, it is
Metamaterials and their two-dimensional equiva- desirable that the microwave absorption bandwidth
lents (known as metasurfaces) are artificial structures can be further expanded for enhancing the radar
which can flexibly manipulate the electromagnetic stealth performance. Moreover, most of the reported
responses through the selection and optimization of bi-stealth structures are inflexible, which cannot meet
the cellular architecture and the chemical composi- the conformal requirements of military equipment in
tion [8]. Due to their unique properties, metamateri- practice [29–33].
als and metasurfaces have received much attention In this work, we provide a rational design of an
and been widely used in many fields, such as infrared stealth layer with low infrared emission as
nanophotonics, energy harvesting, sensing and well as little influence on the radar wave propaga-
healthcare etc. [9–19]. In addition, researches about tion. Then, by using the impedance matching theory
metamaterials and metasurfaces applied in the combined with the equivalent circuit method, the
stealth field have been widely reported with fre- microwave absorption bandwidth broadens com-
quencies ranging from low microwave to high pared with the most reported results. Moreover, by
infrared wavebands [20–28]. Since the electromag- using the ITO-coated-PET films and a polyvinyl
netic responses of metamaterials and metasurfaces chloride (PVC) substrate, the radar and infrared bi-
are frequency selective, they can be used to realize stealth metasurface is both transparent (thus meeting
radar and infrared stealth compatibility [29–34]. the window application) and flexible (thus meeting
Cheng et al. firstly presented a thin radar-infrared the conformal demands).
stealth-compatible structure, which consists of
metallic frequency selective surface (MFSS), resistive
frequency selective surface (RFSS) and metal backing. 2 Theory and design
Reflectivity is below - 10 dB in the whole radar X
wave band and infrared emissivity is less than 0.3 in 2.1 Structure
the infrared region of 8–14 lm [29]. Zhong et al.
reported a multifunctional metamaterial composite A cell of the proposed radar and infrared bi-stealth
structure that not only provided radar and infrared metasurface structure is shown in Fig. 1. The multi-
bi-stealth function but also possessed an in-band layered structure consists of an infrared shielding
microwave transmission window and high optical layer (IRSL), a radar absorption layer (RAL), a PVC
transparency by using the indium tin oxide (ITO)- flexible substrate and a backplane. The IRSL, RAL
coated polyethylene (PET) films [33]. and backplane are ITO-coated-PET films with the
Typically, the radar and infrared bi-stealth struc- same depth of d_PET = 0.175 mm for each layer, and
tures consist of an infrared stealth layer, a radar the relative dielectric constant of the PET is ePET-
stealth layer, a substrate and a backplane. The infra- = 3.0(1 - j0.006). The IRSL consists of ITO patch
red stealth layer is always on top of the radar stealth array with 5 9 5 patches in each cell, while the RAL
layer in the reported literature [29–34]. As mentioned is composed of ITO Jerusalem cross array. The sur-
earlier, in order to realize good infrared stealth, face resistance of the IRSL, RAL and the backplane is
objects with low absorption and high reflection are 5 X/sq, 8 X/sq and 5 X/sq, respectively. The depth
desirable as the infrared stealth layer. On the other and the relative dielectric constant of the PVC sub-
hand, the radar wave would be significantly reflected strate is d_sub = 3 mm and ePVC = 2.4(1 - j0.06),
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Fig. 1 Schematic diagram of


the radar and infrared bi-
stealth metasurface. a Cross-
sectional view of one cell;
b multilayers of one cell;
c front view of the IRSL for
one cell; d front view of the
RAL for one cell

respectively. Other geometrical sizes labeled in Fig. 1 Table 1 Area ratio of ITO and emissivity of the IRSL under
are a = 5 mm, b = 0.7 mm, g = 0.3 mm, l = 4 mm, various b and g
w = 0.2 mm, lJ = 1.3 mm and wJ = 0.3 mm.
Case b (mm) g (mm) sm (%) e
2.2 Design of the infrared shielding layer 1 2.4 0.6 64.0 0.38
2 0.9 0.1 81.0 0.24
The infrared emissivity of the radar and infrared bi- 3 0.8 0.2 64.0 0.38
stealth metasurface is mainly determined by the 4 0.7 0.3 49.0 0.49
emissivity value of the infrared shielding layer. An 5 0.5 0.1 69.4 0.33
ITO conductive film presents a low infrared emission. 6 0.4 0.1 64.0 0.38
However, a whole continuous ITO film would cause
strong reflection in the microwave bands, and
therefore the whole ITO film needs to be divided into
a form of discrete pattern for suppressing the where e is the emissivity of the IRSL, em and ed are the
microwave reflection, as seen in Fig. 1c. Then, the emissivity of ITO (the measured value is about 0.09
corresponding infrared emissivity of the IRSL can be [34]) and PET (the value is about 0.9 [33]) respec-
calculated by using the empirical formula in this tively. sm is the ratio of the ITO area to the whole
condition [29] IRSL area, and sd is the ratio of the PET area to the
whole IRSL area. The calculated sm and e under
e ¼ em sm þ ed sd ; ð1Þ
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Fig. 2 The reflection coefficient, transmission coefficient and c


microwave absorption of the IRSL for all of the six different cases
listed in Table 1. a The reflection coefficient; b the transmission
coefficient; c the microwave absorption

various patch length b and gap size g are listed in


Table 1.
As shown in Table 1, all the calculated e is below
0.5, indicating that the IRSL can realize low infrared
emissivity by choosing appropriate values of b and g,
and the larger sm is, the lower e is. Case 1, 3 and 6
have the same infrared emissivity e, however, the
microwave propagation properties of these three
infrared shielding layers are quite different from one
another.
To approve the above statement, the microwave
reflection and transmission properties of the IRSL are
simulated by commercial software CST Microwave
Studio. Boundary conditions and floquet ports are set
in the simulations, and the ITO surface resistance of
the IRSL is 5 X/sq. For all of the 6 cases listed in
Table 1, the reflection coefficient S11, the transmission
coefficient S21 and the microwave absorption are
shown in Fig. 2. The microwave absorption is calcu-
lated by
A ¼ 1  R  T; ð2Þ
2 2
where R ¼ jS11 j is reflectance and T ¼ jS21 j is
transmission.
Figure 2 proves that though the area ratio of ITO sm
is the same for the Case 1, 3 and 6, the reflection
coefficient, transmission coefficient and the micro-
wave absorption are quite different. That’s because
the ITO patch array structure is a typical low-pass
filter [35], whose propagation properties are mainly
determined by the values of b and g. In addition,
Fig. 2a, c show that the microwave reflection and
absorption of the Case 4 and 6 are lower than the
other cases, which means that more radar wave can
transmit through these two kinds of infrared shield-
ing layer to reach the radar absorption layer, as
demonstrated in Fig. 2b. This suggests that these two
kinds of sub-cell not only have low infrared emis-
sivity (as seen in Table 1) but also have little influence
on the microwave propagation. Therefore, the issue
of the infrared and radar stealth compatibility can be
well addressed based on the metasurface structure
combined with the rational material and geometrical
design. The ITO patches with dimensions of
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b = 0.7 mm and g = 0.3 mm is finally chosen to Zin  Z0


C¼ ; ð5Þ
comprise the IRSL with comprehansive considera- Zin þ Z0
tions of low infrared emissivity, little influence on the
microwave propagation and easy fabrication where Z0 is the characteristic impedance of the air
processes. and approximates 377 X. According to the impedance
matching theory, the surface reflection of the struc-
2.3 Broadband microwave absorption layer ture is 0 when Zin equals to Z0. If the transmission is
also 0, the structure can realize perfect absorption. In
The impedance matching theory is used to realize our design, since the surface resistance of the ITO-
broadband microwave absorption for the RAL, and coated-PET backplane is as low as 5 X/sq, the
the equivalent circuit of the multilayered metasurface transmission can be ignored. If Zin approximates Z0
structure is shown in Fig. 3. in a wide frequency range, broadband absorption can
The infrared shielding layer and the radar be realized.
absorption layer can be equivalent as RLC series After optimization, the simulated reflectance and
circuit and their corresponding impedance is ZIRSL absorption of the bi-stealth metasurface under nor-
and ZRAL respectively. The impedance ZIRSL and mal incidence are presented in Fig. 4a. From Fig. 4a,
ZRAL can be retrieved from numerical simulation. it can be seen that the absorption is higher than 90%
Zsub can be calculated through transmission line in the radar waveband ranging from 7.3 to 18.8 GHz,
theory and the expression is as following realizing a broad relative bandwidth of 88.1% even
Zplane þ jZPVC tanðkc d sub Þ though the whole thickness of the metasurface
Zsub ¼ ZPVC ; ð3Þ
ZPVC þ jZplane tanðkc d sub Þ structure is only 3.5 mm. The input impedance of the
structure normalized to Z0 is presented in Fig. 4b,
where ZPVC, kc and d_sub are the characteristic impe-
and it shows that the real part of the normalized
dance, propagation coefficient and depth of the PVC
input impedance is close to 1 while the imaginary
substrate, and Zplane is the impedance of the ITO-
part approximates 0 within a broad frequency band.
coated-PET backplane, which equals to 5X/sq for
The absorption of the bi-stealth metasurface under
minimizing transmission. To simplify the calculation,
different incident angles is also simulated. The
the interaction between the IRSL and RAL is neglec-
xoz plane (shown in Fig. 1) is chosen as the incident
ted. The input impedance of the whole structure Zin
plane, and the simulated results under the TE
can be expressed as
(transverse electric) wave and TM (transverse mag-
1 netic) wave incidences with the incident angles of 0°,
Zin ¼ : ð4Þ
1=ZIRSL þ 1=ZRAL þ 1=Zsub 10°, 20°, 30° and 40° are shown in Figs. 5a, b,
respectively. It can be found that the absorption
Then, the reflection coefficient of the metasurface
performance varies as the incident angle increases for
can be calculated as
both the TE and TM waves, and the variation for the
TE wave is more obvious than that for the TM wave.
For the TE wave, the metasurface maintains good
performance when incident angle h B 30°, while for
the TM wave, the absorption higher than 90% can still
be achieved in a broad frequency band when incident
angle is 40°.

3 Experiment and discussion

To confirm the simulated results, a 200 mm 9 200


mm sample was fabricated. Geometrical sizes of the
sample and surface resistance of the ITO-coated-PET
films are determined according to the simulation
Fig. 3 Equivalent Circuit of the bi-stealth metasurface structure optimization discussed above. The ITO arrays of the
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Fig. 5 The simulated absorption of the bi-stealth metasurface for


Fig. 4 a Reflectance and absorption of the bi-stealth metasurface; different incident angles. a Under the TE wave incidence and
b normalized input impedance of the bi-stealth metasurface b TM wave incidence

IRSL and RAL are fabricated via high-precision laser From Fig. 7a, it can be seen that, for the TE wave
etching. The four layers (IRSL, RAL, PVC substrate incidence, the simulated reflection coefficient is lower
and backplane) are assembled by dual-side adhesive than - 10 dB (thus the corresponding absorption is
tapes. Photographs of the sample are presented in higher than 90%) in the radar waveband ranging
Fig. 6, which demonstrate its good optical trans- from 7.3 to 18.8 GHz, and the corresponding experi-
parency and high flexibility. mental frequency band is from 8.4 to 19.4 GHz. As
The microwave performance of the sample is shown in Fig. 7b, for the TM wave incidence, the
measured by using an arch measurement system, simulated reflection coefficient is lower than - 10 dB
which is mainly based on an Agilent N5224A net- from 7.4 to 18.9 GHz, while the corresponding
work analyzer and a pair of broadband horn anten- experimental result is from 8.1 to 19.4 GHz. The
nas. The measured reflection coefficients under the microwave absorption characteristics of the experi-
TE and TM wave normal incidences are shown in mental results have similar trends to that of the
Fig. 7a, b respectively, and the simulated results are simulated results for both the TE and TM wave
also added for comparison.
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Fig. 6 Photographs of the


fabricated sample. a A paper
with logo; b the sample
covered on the logo; c the
sample under the bending state

normal incidences. Compared with the simulated for measurement. For comparison, a piece of metal
results, the whole frequency bands of the experi- with low emissivity (\ 0.1) and a piece of PET with
mental results shift slightly toward the high fre- high emissivity (* 0.9) are also used as the reference
quencies and also the measured reflection coefficient samples. Both the reference samples have the same
is higher than the simulated reflection coefficient. The sizes (5 mm 9 10 mm 9 0.175 mm) as the IRSL one.
above discrepancies should be due to the following These three samples were placed on a heating plate
three reasons: (i) the relative permittivity of the PET with a constant temperature of 80 °C to ensure that
films and the PVC substrate may be different they have the same background temperature. Their
between the simulated value and the actual value; (ii) thermal IR images were captured by using a thermal
the surface resistance of the ITO-coated-PET film cameral (HIKVISION H10) working in the range of
sample deviates from the simulated value; (iii) the 8–14 lm. As shown in Fig. 8, the measured temper-
fabrication tolerance. atures of the PET, metal and IRSL samples are
The infrared stealth properties of the sample are 79.2 °C, 32.6 °C and 57.9 °C, respectively, which
also characterized. As mentioned above, the infrared indicate that our IRSL sample indeed has a low
emissivity of the radar and infrared bi-stealth meta- infrared emissivity and it can satisfy the infrared
surface is mainly determined by the emissivity value stealth demands. By combining the results of Fig. 7
of the infrared shielding layer (IRSL). According to with Fig. 8, it can be seen that multispectral stealth in
Eq. (1), the calculated emissivity value of the IRSL is the radar and infrared frequency bands is realized by
0.49, indicating that the IRSL has low infrared emis- using this metasurface.
sion properties. To prove this theoretical conclusion, The optical transparency of the bi-stealth meta-
a 5 mm 9 10 mm piece of the IRSL sample was used surface is realized by using the ITO-coated-PET films
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Fig. 8 Thermal IR images of the PET, metal and IRSL samples on


a heating plate with temperature of 80 °C

Fig. 7 Comparison of the reflection coefficients between the


measured and simulated results under a TE wave normal incidence Fig. 9 Optical transmittance of the IRSL, RAL, PVC, backplane
and b TM wave normal incidence and whole structure

and a PVC substrate. The optical transmittance of the 4 Conclusions


IRSL, RAL, PVC, backplane and whole structure is
measured by using a spectrophotometer (SHI- A flexible metasurface with low infrared emission
MADZU UV 3600) and shown in Fig. 9. The total and broadband microwave absorption is achieved.
optical transmittance of the metasurface can be also The low infrared emission is realized by using ITO
calculated by multiplying the transmittances of each patch array and the broadband microwave absorp-
layer (the IRSL, RAL, PVC, backplane), and it is also tion is achieved based on the impedance matching
shown in Fig. 9. The total optical transmittance theory. The metasurface is transparent and flexible by
reaches 30% at 620 nm, which demonstrates the good rationally designing the materials. Both the simulated
optical transparency of this metasurface. It is also and experimental results verify that the metasurface
found that the measured and calculated transmit- has broadband microwave absorption, low infrared
tance coincide well with each other. emission and high optical transmission properties.
These results suggest that the proposed metasurface
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is promising in the applications of multispectral biological applications. IEEE Trans. Ind. Electron. 65(4),
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