Date Entry Sheet for DUC

Env. Temp. & 24.6 °C Env. Temp. & 25.1

Humidity Before Humidity After
53 %RH 56
DUC Name DTI With Sensor (Refrigerator) Range 0 to 200 °C
Make Multi L. Count 0.1 °C
Model ----- Sr.No. -------
ID CWC/NRWQL/Reftr-04

Temperature (°C)

30 °C 50 °C 100 °C 150
Standard
Calibraiton Standard DUC Standard DUC Standard DUC Standard
Point Readings Reading Readings Reading Readings Reading Readings

°C °C °C °C °C °C °C °C

30.125 30.0 50.155 50.0 100.205 100.0 150.255

30
30.126 30.0 50.156 50.0 100.206 100.0 150.256
30.128 30.0 50.158 50.0 100.208 100.0 150.258
50
30.129 30.0 50.159 50.0 100.212 100.0 150.259
30.131 30.0 50.162 50.0 100.214 100.0 150.262
100
30.134 30.0 50.164 50.0 100.216 100.0 150.264
30.136 30.0 50.166 50.0 100.218 100.0 150.266
150
30.138 30.0 50.168 50.0 100.219 100.0 150.268

30.139 30.0 50.169 50.0 100.221 100.0 150.269

200
30.141 30.0 50.172 50.0 100.223 100.0 150.272
Average 30.133 30.00 50.163 50.000 100.214 100.000 150.263
ate Entry Sheet for DUC & Observation
°C Location At Site
%RH SRF No 62/20
Calibration Date 15-0-2021
ID ----
Master RTD With Indicator
QL/Reftr-04 Loction of InstrumentGeneral Lab

°C 200 °C
DUC Standard DUC
Reading Readings Reading Error Resolution of Uniformity of Stability of
DUC Source Source

°C °C °C °C °C °C °C

150.0 200.275 200.0

-0.133 0.1
150.0 200.278 200.0
150.0 200.279 200.0
-0.163 0.1
150.0 200.282 200.0
150.0 200.284 200.0
-0.214 0.1
150.0 200.285 200.0
150.0 200.286 200.0
-0.263 0.1
150.0 200.288 200.0

150.0 200.289 200.0

-0.284 0.1
150.0 200.292 200.0
150.000 200.284 200.000
 °C

Master Expanded
Uncertainty Uncertainty

±°C ±°C
0.59
0.6

0.59
0.6

0.69
0.7

0.88
0.9

0.88
0.9
 Calibration Certificate
ULR No.: CC309622000000896F
Certificate No.: CCTPL/TC/0116/04 Field: Mechanical
SRF No.: 100/22 Date of Receipt: 02/06/2022
SRF Date: 29/05/2022 Date of Calibration: 02/06/2022
M/s. ARC Testing Laboratory Recommended Due Date.:
01/06/2023
Company Name & (As per agreed by cusmtomer)
Address Kh. No.42/9/4, Village-Badli, Near Astha
Hospital, New Delhi-110042
Certificate Issue Date: 05/06/2022

DUC* Details
Instrument Name: Temprature Controller (Tile Autoclave) Instrument Sr. No.: -----
Make: SSI Instrument Id No.: ATL/TC-15
Model No.: ----- Location: Lab
Range: 0 to 200 °C DUC Condition: OK
Readability: 0.1 °C Calibration Performed at: At Site
Standard Equipments Used(Traceable to National Standard)
Sr. No Instrument Name Cert. No Cal. By Calibration Due Date

1 SPRT With Super DAQ TL/021/1001.1.1 Tempsens 01/10/2022

Temperature Humidity Reference Standard Calibration Procedure No.

Environment Condition
25.7 ºC 56 %RH DKD-R-5-7 CCTPL/TH/CP/05S

Calibration Result
Nominal Temperature Standard Reading DUC* Reading Deviation Expanded Uncertainty
Sr. No.
(°C) (°C) (°C) (°C) ±(°C)
1 30 30.133 30.0 -0.133

2 50 50.163 50.0 -0.163

3 100 100.214 100.0 -0.214 0.6

4 150 150.263 150.0 -0.263

5 200 200.284 200.0 -0.284

Note : DUC* : Device Under Calibration
Uncertainty of measurment at approx 95% Confidence Level with coverage factor k = 2.

Calibrated By : Amit Pal Approved By : Sandeep Sharma

Calibration Engineer Director

Note. 1.This Certificate only to the particular instrument submitted for calibration.
2.This Calibration Result reported in this certificate valid at the time of and under the stated condition of measurement.
3.This particular certificate can not be reproduce except in full, without prior permission of CCTPL.

`--- End of Certificate --- Page 1 of 1

 Calibration Observation Sheet for Thermal
Calyss Calibration & Testing Pvt. Ltd.
CCTPL/QF/6.4/05/T-01
Issue Date:08/07/2019 Amd Date:00
F-40, Sector-9, Noida-201301,UP
Issue No: 01 Amd No: 00

1 S.R.F. No.: 2 Job Order Number:

3 Calibration Date: 15-0-2021 4 Rcoommended Date of Next Calibration : Err:509
5 Instrument Details(DUC) :
Temprature Controller (Tile SSI
Name: Readablity : 0.1 °C Make/Model :
Autoclave) -----

Range : 0 to 200 °C ID/Sr.No: ATL/TC-15 / ----- Location: At Site

6 Instrument Details (Standard):

Name: Err:509 ID/Sr.No: CCTPL/TH/R-1909 Calibrated By: Err:509
Make/Model : Fluke/5609 Cert. No: Err:509 Cal.Valid upto: Err:509
7 Instrument Details (Source):
Name : ID/Sr No.: Make/Model :
8 Enviromental Condition :
Before: 24.6 Before: 53
Temperature (ºC): Humidity(%RH):
After : 25.1 After: 56

9 Observations:
Set Value: 30 ˚C Set Value: 50 ˚C Set Value: 100 ˚C
Display Value: Display Value: Display Value:
Sr. No.
Reading of Std Reading of DUC Reading of Std Reading of DUC Reading of Std Reading of DUC
(˚C) (˚C) (˚C) (˚C) (˚C) (˚C)

1 30.13 30.0 50.16 50.0 100.21 100.0

2 30.13 30.0 50.16 50.0 100.21 100.0
3 30.13 30.0 50.16 50.0 100.21 100.0
4 30.13 30.0 50.16 50.0 100.21 100.0
5 30.13 30.0 50.16 50.0 100.21 100.0
6 30.13 30.0 50.16 50.0 100.22 100.0
7 30.14 30.0 50.17 50.0 100.22 100.0
8 30.14 30.0 50.17 50.0 100.22 100.0
9 30.14 30.0 50.17 50.0 100.22 100.0
10 30.14 30.0 50.17 50.0 100.22 100.0

Remarks: ..........................................................................................................................................................

Calibrated by: Checked by:

Prepared By: Approved By: Issued By:

Quality Manager Director Quality Manager
 Calibration Observation Sheet for Thermal
Calyss Calibration & Testing Pvt. Ltd.
CCTPL/QF/6.4/05/T-01
Issue Date:08/07/2019 Amd Date:00
F-40, Sector-9, Noida-201301,UP
Issue No: 01 Amd No: 00

10 Observations:
Set Value: 150 ˚C Set Value: 200 ˚C Set Value: %RH
Display Value: Display Value: Display Value:
Sr. No.
Reading of Std Reading of DUC Reading of Std Reading of DUC Reading of Std Reading of DUC
(˚C) (˚C) (˚C) (˚C) (%RH) (%RH)

1 150.26 150 200.28 200

2 150.26 150 200.28 200
3 150.26 150 200.28 200
4 150.26 150 200.28 200
5 150.26 150 200.28 200
6 150.26 150 200.29 200
7 150.27 150 200.29 200
8 150.27 150 200.29 200
9 150.27 150 200.29 200
10 150.27 150 200.29 200

11 Observations:
Set Value: %RH Set Value: %RH Set Value: %RH Set Value: %RH
Disp. Value: Disp. Value: Disp. Value: Disp. Value:
Sr.No.
Reading of Reading of Reading of Reading of Reading of Reading of Reading of Reading of
Std (%RH) DUC(%RH) Std (%RH) DUC(%RH) Std (%RH) DUC(%RH) Std (%RH) DUC(%RH)
1
2
3
4
5
6
7
8
9
10

Remarks: ….......................................................................................................................................................

Calibrated by: Checked by:

Prepared By: Approved By: Issued By:

Quality Manager Director Quality Manager
 Uncertainity Calculation Sheet
1. Laboratory : CCTPL

3. Standard / Equipment Used for Calibration

Details of Standard Used Standard1 Source

Instruments Name : SPRT with Indicator Low temp. Negative Bath
Manufacturer/Model : Fluke/5609 Tempsens
Sr.No./I.D.No: CCTPL/TH/R-1909 CCTPL/TH/R-1915
Range : (-15 to 660 degree C) (-145 to 110 degree C)
Certificate No. FL/CAL/TH/07082019-C001
CalibrationDate&validity 28.08.2019 & 28.08.2020
Traceability: Farelabs Gurugram

4.Environmental Condition During Calibration

Temperature 25±2 0 Humidity 55±10 % RH

5. Evaluation
30 °C 50 °C 100 °C 150
Standard Standard DUC Standard DUC Standard DUC Standard
Calibraiton Readings Reading Readings Reading Readings Reading Readings
Point

°C °C °C °C °C °C °C °C
30.125 30.000 50.155 50.000 100.205 100.0 150.255
30 30.126 30.000 50.156 50.000 100.206 100.0 150.256
30.128 30.000 50.158 50.000 100.208 100.0 150.258
50 30.129 30.000 50.159 50.000 100.212 100.0 150.259
30.131 30.000 50.162 50.000 100.214 100.0 150.262
100 30.134 30.000 50.164 50.000 100.216 100.0 150.264
30.136 30.000 50.166 50.000 100.218 100.0 150.266
150 30.138 30.000 50.168 50.000 100.219 100.0 150.268
30.139 30.000 50.169 50.000 100.221 100.0 150.269
200 30.141 30.000 50.172 50.000 100.223 100.0 150.272
Average 30.133 30.000 50.163 50.000 100.214 100.000 150.263
Standard 0.01 °C 0.01 °C 0.01 °C 0.01
Deviation

TYPE B UNCERTAINTY EVALUATION

Ub1: Source: Uncertainty of Reference Instruments SPRT with Indicator

(Taken from the calibration certificate)

b1 = num˚C Diviser-k: 2
Assuming Normal Distribution,Ub1= b1/k=
Degree of freedom V1 = infinite

Ub2: Source: Uncertainty due to Uniformity of Bath (Source)

(Taken from Manufacturer's Specification of Bath)

b2 = num ˚C Diviser-k: 1.7320508

Assuming Rectangular Distribution,Ub2= b2/k=
Degree of freedom V1 = infinite
Ub3: Source: Uncertainty due to Stability of Bath (Source)
(Taken from Manufacturer's Specification of Bath)

b3 = num #REF! Diviser-k: 1.7320508

Assuming Rectangular Distribution,Ub3= b3/k=
Degree of freedom V1 = infinite

Ub4: Source: Uncertainty due to Reolution of DUC)

Since the limits given are half the count, and assuming Rectangular Distribution

Resolution Multiplier b4 Diviser Ub5

o
C Sqrt(3)
0.01 0.5 0.005 1.732051 0.0028868

Uncertainty,Ub5 = b4 / √3

Combined Uncertainty Range

Ua
𝑼𝒄=√(∑129_(𝒊 Ub1
=𝟏)^𝑵▒𝑼_𝒊^𝟐
) Ub2
Ub3
Ub4
Uc = √ [(Ua)2+(U1)2+(U2)2+…+(Un)2] Uc
Coverage
Factor
Expanded
Expanded Uncertainty at 95% Confidence level :- Uncertainity
Expanded Uncertainty U = k x Uc

Effective degree of freedom :- Range

Veff
Veff = Uc4(Y)
[Σ{(ui4(Y / Vi)}] Range
Final Result= 30
50
100
150
200
Uc=√(∑1
𝑼𝒄=√(∑129_(𝒊 With Coverage Factor K=2 at 95 %Confidence Level
29_(i=1)^
=𝟏)^𝑵▒𝑼_𝒊^𝟐
N▒U_i^2
) )
 ˚C

°C 200 °C
DUC Standard DUC Standard Type A Uncertainty
Reading Readings Reading Deviation Uncertainty of Standard
Error Instrument Uniformity
(±)

°C °C °C °C °C °C °C °C
150 200.275 200
-0.133 0.01 0.0018015 0.6 0
150 200.278 200
150 200.279 200
-0.163 0.01 0.0018466 0.6 0
150 200.282 200
150 200.284 200
2.000 0.01 0.0019989 0.7 0
150 200.285 200
150 200.286 200
-0.263 0.01 0.0018466 0.9 0
150 200.288 200
150 200.289 200
-0.284 0.01 0.0016852 0.9 0
150 200.292 200
150.000 200.284 200.000
°C 0.01 °C

T with Indicator

Range
30 50 100 150 200
0.6 0.6 0.7 0.9 0.9
0.30000 0.30000 0.35000 0.45000 0.45000

Range
30 50 100 150 200
0 0 0 0 0
 0.00000 0.00000 0.00000 0.00000 0.00000

Range
30 50 100 150 200
0 0 0 0 0
0.000000 0.000000 0.000000 0.000000 0.000000

ar Distribution

Range
30 50 100 150 200
0.1 0.1 0.1 0.1 0.1
0.02887 0.02887 0.02887 0.02887 0.02887

30 50 100 150 200

0.001802 0.001847 0.001999 0.001847 0.001685
0.300000 0.300000 0.350000 0.450000 0.450000
0.000000 0.000000 0.000000 0.000000 0.000000
0.000000 0.000000 0.000000 0.000000 0.000000
0.028868 0.028868 0.028868 0.028868 0.028868
0.301391 0.301391 0.351194 0.450929 0.450928

1.96 1.96 1.96 1.96 1.96

0.5907265 0.590727 0.6883405 0.8838204 0.88381912

30 50 100 150 200

7.05E+09 6.39E+09 8.58E+09 3.20E+10 4.61E+10

30.000 ± 0.59
50.000 ± 0.59
100.000 ± 0.69
150.000 ± 0.88
200.000 ± 0.88
Stability Resolution

°C °C
0 0.1

0 0.1

0 0.1

0 0.1

0 0.1