zavannen IRDUFTUAL STANDARD Polymer-modified bitumen roofing sheets 1 Scope This Japanese Industrial Standard specifies polymer-modified bitumen roofing sheets used for waterproof construction of various structures (hereafter re- ferred to as “roofings’). Remarks : The following standards are cited in this Standard. JIS A 5304 Concrete flags JIS A 5430 Fiber reinforced cement boards JIS K 6223. Calcium carbonate for rubber JIS K 6250 General rules of physical testing methods for rubber, vulcanized or thermoplastic JIS K 6257 Accelerated aging test methods for vulcanized rubber JIS K 8575 Calcium hydroxide JIS Z 8401 Rules for rounding off of numerical values JIS Z 8703 Standard atmospheric conditions for testing 2 Classification Roofings are classified as follow: (1) Classification by use Exposed single-layer waterproofing Exposed multi-layer waterproofing Non-exposed single-layer waterproofing Non-exposed multi-layer waterproofing Table 1 Classification by material constitution Classification by [at constitution ‘Mark material constitution Material ‘te Reinforced type Roofing composed of polymer-modified bitumen as main Class R ‘component and fibrous sheet as reinforcement ‘Non-reinforced type | Roofing of polymer-modified bitumen as main component Class N2 A6013 : 1996 (3) Classification by temperature characteristic Table 2 Classification by temperature characteristic Unit: °C 3 Quality When the tests are carried out according to 6, the quality shall comply with Tables 3 and 4, 8 Quality When the tests are carried out according to 6, the quality shall comply with Tables 8 and 4. ‘Table 3. Quality according to classification by use and material constitution = Teedeninecaeet | Bgeeladamnee Canina ee SESE can | cuux | cumk | caun |B Treats [Nawend | tomin | min | tomm | comin | 6 Meet nar tatng | Natl has 0% avalon oto on nw eid rem a i Sea Baez [Ntwand | Wain |] somm | Baim [Omi aise + 1 i Aiea” | oxi thn 6 eh va a tee red “AR imaoerson | eae protec | Noctrated | 2500min. | r2000min. | 2000mia. | 12000min. Race Tearaeath W Dan = terete | ora o wow | Mat en tae Arman | Noting a nmin hl apr Dusen a sce | o0at0 eine | Same Cpaance | Recher warp ar Sa al opp Jeter New) | MMS 70 eile nag afome | Indentation reitanse ‘No hole sball appear 10) Paige naan Norah er or ba sal enSTD.JIS A GOL3-ENGL 199% MM WI33L08 054705" 565 Mm Note (?) In the case of roofing to be processed with using an tacky layer, it shall be at least 40 Niem or 70 % of lateral tensile strength of non-treated 4. Dimensions and mass per unit area 4.1 Dimensions The thickness shall be given in Table 5 and the width and the length shall be subject to agreement between the parties concerned with acceptance. ‘Table 5 Thickness ‘Now eapued sng layer waterpretng ‘Nom caged mal lner waterline Note (*) ‘The numerical values in ( ) are applied for roof- ings which are processed by using a torch burner. ‘Table 6 Tolerances on dimensions and masses per uunit area relative to marked values 5 Appearance When the test of 6.8 is carried out, the appearance shall comply ‘with the following requirements : (A) ‘There shall be no remarkable bend or roughness. (2) There shall be no tear, fold, wrinkle or through hole.A018: 1996 (8) There shall be no portion abnormally stuck, or such portions where a part of surface layer is Incking or reinforcing material in separated from the laminated material (A) The cut Kine at the end shall be almost at a right angle to the longitudinal di roction, (8) When the length of one coil is less than 8.0 m, the product shall not be cut. (@) When the length of one coil is not lege chan 8.0 m, the produet shall not be cut al two or more positions. (7) When the length of one coil is not less than 8.0 m und there is one cut in the coil, the length of one pivee sbull bu 3.0 m or more. 6 Tests 6.1 General cunditions for test The general conditions for test shall be as fol Tow (2) ‘Temperature and humidity conditions of test place and aging conditions of test specimens and teat pieces (@) The temperature and humidity eonditions at measurements of dimensions fund must per wait area shall be 20°C class 16, 65 % class 20 ((20 #15) °C, (65 £20) %] specified in JIS Z 8703. (bo) Thu temporuture conditions in uppearance text shull bu 20 ‘C elaae 15 120 16) °C. specified in JIS Z 8703. (©) Unloss otherwise specified, the conlitions for texts other than speciied in (a) and (b) shall be 20 °C’ Glass 2, 85 % class 20 [(20 42) °C, (65 £20) “) specified im JIS 2 8708. (@)_ Unless otberwige apecified, the aging time of test specimens and test picees shall be one hour or aiore before the test. (2) Preparation of test pieces Tho preparation of test pieces shall be as fol- lowe: ‘The size and number of test pieces sball be given in Table 7. The roofing is spread on a plane and exposed under the standard conditions for 24 h ot rare fas shown in Fig. 1 and then the test pieces shall be taken from the portion ‘adjacent to the thickness measurement sample. The portion within 100 em ‘apart from the oxtalde en of coil ahall be excluded from the partion where text pieces are sampled. For roofing with a width Tess than 85 em, the test pieces shall be taken from the roofing with a width not less than 35 cm manufactured ‘under the same conditions. Ir test pioves are additionally taken due to the cireumstaneos of the test, the test pieces shall be taken from the adjacont portion or tho thickness meusure:‘As royards the items for which the tout is difficult due to adhesion of the roofing, Une (eats shall be cacried out with the teat pitees of whicl adhesion part is powdered with precipituted eulcium earbunute light of class 1 xpecified in JIS K 6293 ‘Table 7 Sizo and number of lst pieces — wou Stir | pe gato _| 3) ears mora | : 02010518) Ate hati Sees a tate raion xa | eonmo0i0n10) Thactmcan [treat avec [aa aw 2009-10 jis Fe tn Aa [Ws Motion) Gurnee [sneaked dines |__| os Tat aon | wore Tet ioe © | marme imenion Ymettdinais |b | atone ay Laverton | meme umn ei | wosmawrn |? wa | amon ams70 [> eae CEA i Yorn 3 Fates oe @ | won 0 : | se | texgtoin | Bont ioe 1007 | EE erent areton er aae 00x00 a ye Eee: Lo ‘anating | diction Rear side a 1006 60 a Note (*) ‘The size in ( ) in applicable for routing of elass N. (8) Rounding off of numerical values Tho rounding off of numerical values such ‘as maaaured or calculated values shall be in aecordance with JIS Z 8401i # i 5 i 2 BL] cue nearer a sample A | BeSleannt oma per at par ana a Lateral dretion (whole width) Fig. 1 Shape of test piece and sampling method (example drawing) Measurement of dimensions Length Spread the specimen on a plane, and measure the overall length at the shortent part to the mearent 2 cm. If there in.» ent part in a coil, measure ‘the longth at the shortest part similarly, and take the gum of the Yengthe so measured minus 15 em sa the length of one coil.(2) Width Monsure the width at three points i.e. near both ends and middle in ‘the longitudinal direction to the nearest 1 mm and express the mican ofthe vale 0 meanured an the width. (8) ‘Thickness Mentors the thickneas by wring the thickness measuring instra- ‘ment specified in 6.6.1 (1.1) (Method A} of JIS K 6250: 1907 or a similar in- trament Take the thickness measuroment sumplo in such a way that the central part of the ruofing of which the Teryth und width have boen measured is ent at a right langle to the longitudinal direction ta have a length of 100 em aa shown in Fig. 2. ‘Measure the thickneea at two pointe (a and b) ue, 2em inside from.« cut end and 20 & of width inside from both Interal ends, and three paints (c, d and e) which fare divided the distance between a and b into four equal parts, namely at five points in total. Measure the thickness to the nearest 0.01 um and express the ‘ean of the measured valses to the firet decimal place. However, measuceaieats at points c and e may be omitted for products with a width less than 60 cas. Measure the thickness after removing the seperate paper. if attached. Unit: em at ine Loogttadina ireten Fig. 2 Measuring points of thickness 6.3 Appearance In the appearance test, spread the roofing on a plane und exam ine it visually. 6A Mass per unit area Measure the width and length of the sample of which the thickness has heen measured in 4.2 (8) at thrve points euch lv Uhe nearest 1mm, obtain the area from the mean value of them and measure the mags to the nearest 10 g. Caleulate according t0 the following formula. If separate paper is rattached to the sample, remove it after measurement of width and length and nea- ‘sure the mass.where, ME: meas per unit urou (yim) mm: maas (g) A ream?) 6.5 Tensile property 11 Test equipment The test equipment shall be as fellows (2) Tensile tester The tensile ester shall bo Ube ane of constant cromshond speed type equipped with an automatic recording device of lund and displacement. (2) Heating thermostat The heating thermostat shall be the equipment in 4.2 ‘of JIS K 6267 or a similar ono to be adjustable by 42 °C to the awl temper ture. 6.52 Preconditioning of test piece The preconditioning uf test pi ‘a8 follows: hull be ()) Heat treatment Carry out the heat treatment in a heating thermostat con- trolled at (80 42) °C for 168 h. Place separate paper on a flat board locaced horizontally and then place the test pisces gently ou the paper. Place the frout aide downwards for exposed roofings. Place the test pleces after heating under ‘the standard conditions for approximately 4 h. 2) Alkali treatment Immerse the tout pivces into « saturated aqueous olution ‘of calcium bydreaide (guaranteed yeade specified in JIS K 9576) for 163 h xt ‘eempratsre (20 22) °C for alkali trantment. Safficiently wash the test pieces after immersion by seater, wipe them with dry cloth and allow them to stand sill under the standard conditions fer approximately 4h, 6.5.2. Preconditioning of test plece The precoudilioning uf test piece shall be 8 follows: (1) Heat treatment Carry out the heat trearment in a heating thermostat con: trolled at (80 12) °C for 168 h. Place separate paper on a flat board located horizontally and then place the test pieoea gencly ou the paper. Place the frout aide downwards for exposed roofings. lace the test pieces after heating under ‘the standard conditions for approximately 4 h. 2) Alkali treatment Immerse the test pisces into a saturated aquaous solution of ealcium hydroxide (guaranteed yrude specified in JIS K 8575) for 163 b ut temperature (20 22) °C for alkali treatment. Safficiontly wash the test pieces after immersion by sater, wipe them with dry cloth and allow them to stand ‘ull undar the ntandard conditions for approximataly 4b. 6.5.8 Test method Measure the widths of the test pieces at three paints to the nearest 0.1 mm and ebtain the mean value. Carry out the measurement of widths ‘of test piecen prior to being subjected tn the preconditioning. ‘Mount the teat piece ‘on the tenvile tonter no that the length between the elarapit tx 100 mm, pull the tent piece at a tensile speed of 100 mm/min until it breaks, and obtain the rasximum Toadi*) and the digplacement at fracture(®). For tent pisces of class N, make the langth between clamps 20 mm and the tansile speed 20 mm/min, Calculate the strength by means of Uhe formula given below, and exprow the mean value of 5 teat pieces as the tonaile strength, > ree w where, T's tanaile atrangth (Siem) maximum load (S) width of tast piece (em)‘Calculate the clongation from the displacement on the reference length between clamps of the text piece, by means ofthe formula given below, and expreas the wean ‘value of 6 test pieces. If uny slippuye is found betwoon the test piece und the clamp, ‘measure the slippage and reduce the value so measured frvin the displacement. L Pa% x10 L where, Es elongation (%) Ly: displncoment at fracture (mm) Ly: lonyth butwuon clamps (mim) ‘Tensile product shall be caleulated from the mean valuon of tensile strength and tlongation according to the following formula: Tea Pek where, Ty: tensila product (N-S/em) Notes (4) If a peak load appears due to the effect of laminate materials having no relation with the fundamental properties of roofing much as lining material in the initial stage of tensile test, snch an effect shall be disregarded, © Tf the tent pinee doen not break after appearance of the mximnm load, the instant when the load decreases to 50 % of the mavirmam load aball be considered as the time of fracture. 6.6 Tear strength 6.6.1 Test equipment The Lest equipment shall be the tensile tester speeilied in 65.11). 6.6.2 Tost mothod As illustrated in Fig. 3, make o cut line of 78 mm in the ‘middle of the shorter side of tese pieces parallel to the longitudinal direction so that ‘wo tongues are formed. ‘The part 45 mm from each end of the tongues is the part ‘tg be clamped. Mount the test piece on the tensile tester so that the length between the clamps becomes 50) mm as illustrated in Fig. 4, and pull the test piece until it breaks at a tensile speed of 100 mm/min, and thon ubtin the maximum load. Express the tear strength by the meun value of 5 test piecesUnit: mm 100 | Papi 34. (Cut Hine “art tbe Samped Fig. Tearing test piece Fig. 4 Test method for tear strength 6. Heat resistance 6.7.1 Test equipment The test equipment shall be as follows : (2) Length measuring apparatus ‘The length measuring apparatus shall have accuracy of 1 mm oF better. (2) Heating thermostat The heating thermostat shall be as specified in 65.1 (2), 6.1.2 Test method As illustrated in Fig. 5, fix the upper end of test piece ao that it does not slip, and hang this assembly for 6 hin the heating thermostat controlled at (80 +2) °C. Take cut the test piece, measure the maximum length of sagging of covering layer and examine for the exiatence or nonexistence of dripping and foam- ing. Express the length of sagging by the maximum value on three test pieces.Unit: am Avores. 1 Pastore Fixing pate “Tost pines a Fig. 6 Tost mothod for heat resistance (example) 6.8 Dimensional stability 68.1 Test equipment The test equipment shall be as follows: (1) Length measuring instrument ‘The length measuring iasteument shall huve fan accuracy of 0.1 mn or better. (2) Heating thermostat The heating thermostat shall he specified in 6.5.1 (2) (Wh Thermastatie water bath ‘The chermoscatie water bath ahall be capable of controlling the temperature at (60 71) £C, (Low temperature thermostatic air chamber The low temperature ther- mostatie air chamber shall be capable of controlling the tomperature at (-10 22°C. 6.82 Test mothod Allow the test picees to stand still horizontally in the heating thermostat controlled at (60 22) °C for 23h, take them out and expose to the standard conditions for 1h and then measure the length of the middle part obtain the referonce length of the test picee. The test shall be carried out according (0 the following procedures. Procens 1. Tramerse the test pieces into the thermostatic water bath controlled at (00 =1)‘C for 19 h, take them out and wipe the water adhered on ‘the surface. This operation is called wetting. Process 2. Next, stand the test pieces still in the low temperature thermostatic air chamber controlled at (-U0 42) *C for 5h. This opaention in ealled cooling, Process 3. Next, stand them stil horizontally in the heating thormastat con- trolled at (60 °2) *C for 24 h, This operation is ealled drying. Process 4. Repeat the above wotting. cooliny and drying operations 4 times.Process 5. Furthermore, carry out the fifth operation of wetting. cooling and drying. At the finishing time of each operation, stand the test pieces still under standard conditions for 1h, and measure the length of them. Calculate the change rate of each test piece according to the following formula. Express the dimensional change rate by the mean value which has the maximum absolute value in 5 test pieces at wetting, cooling and drying. Examine the appearance on the test pieces subjected to the repeti- tive test by checking for the existence or nonexistence of wrinkles, warp and separation of layers. If it is necessary to interrupt this test sequence, interrupt the test after the drying operation. he where, change rate (%) ‘measured length (mm) reference length (mm) 69 Joint strength 6.9.1 Test equipment The test equipment shall be the tensile tester specified in 65.1 (0), 6.9.2 Preparation method of test specimen As illustrated in Fig. 6, place the test piece (E-2) on the test piece (E-1) and joint them with both edges of roofing being laterally overlapped by 80 mm for class R and 10 mam for class N and allow the assembly to stand still under the standard conditions for 24 h for aging. However, ifthe joint is done by adhesive, the duration of aging shall be 168 h. In this procedure, carry out the joint and edge treatment of test piece (E-2) in accor dance with the method specified by the manufacturer. After completion of aging, as illustrated in Fig. 6, cut this assembly at right angle to the longitudinal direction so ‘that 5 test specimens of 50 mm width for class R or of 10 mm for class N are produced discarding both ends by 25 mm each. .93 Test method Measure the width of the test specimen at 3 points on the joint part to the nearest 0.1 mm and obtain the mean value. Mount the test specimen to the tensile tester so that the length between clamps becomes 100 mm, pull it at a tensile speed of 100 mm/min until it breaks, and obtain the maximum Toad. For class N, make the length between clamps 20'mm and the tensile speed 20 mm/min. Caleulate the tensile strength according to the following formula, and express it by the mean valve of 5 test epecimens. n where, Ty: Joint strength (Nic P,: Maximum load (N) W,: Width of test specimen (c z(a) For class R (0) For class N eral iret toting os pice? mo ie | | Fig. 6 Preparation method of tat apesimen for joint strength 6.10 Indentation resistance 6.10.1 Test equipment The teat equipment shall bo an fallow : (1) Test indenter As illustrated in Fig. 7, the test indenter shall be « steel disk ‘of 200 mm in diamecer equipped with three ateel cylinders of 11.3 mm in diam- ‘ter, and the mass shall be 9.0 kg, (2) Comerete flag The concrete fag shall he normal concrete flag N'300 for pavement specified in JIS A 5904. 102 Test method Place the test pieve on the smooth surface of the conereta ‘lag with itn front side upwards, and then sland still the test indenter on the center of the test piece as illustrated in Fig. 8 for 24 4. After a lapse of 24 h, remove the test indonter and ceamine the existence or nonexistence of through holes.Steel eplinder Sa Fig. 7 Test indenter (example) Unit: mm =) Ls Tet indenter “Test piece Concrete ag Fig. 8 Test method for indentation resistance 6.11 Fatigue resistance 4.11.1 Test equipment The test equipment shall be the fatigue tester. ‘The fa- tigue tester shall be such a device(") capable of causing increase and decrease of crack of a prescribed magnitude on the backing board for test specimen, while the backing board held horizontal, and of controlling the number of times. This equip ‘ment is contained in a thermostatic air chamber which can control its inside tem- perature within 22 °C from the set temperature. Note (*) When a tensile tester capable of being used repeatedly is utilized, ssuch a measure is necessary, that a guide which maintains the backing board for test specimen in a plane is provided and the clamp on load cell side is fixed. 6.11.2 Preparation method of test specimen The test specimen shall be pre- pared as follows :(2) Bucking board Cut the flexible board of 8 mm thick epecified in JIS A 6430 {nto a wizo of 120 mm width and 400 mm length, and make a cutting of about 6 mom deep on the rear surface of the sheet at the middle ia the lateral direction. (2) Preparation method Prepare the test specimen by pasting the test pieve on ‘he middle part of front surface of the backing board in accordance with the method specified by the manufacturer und aye it being placed horizontally un- er the standard conditions for 24 b. However, if the tost piace in parted by an adhesive, the duration of aging shail be 168 h. 6.11.8 Test method After completion of the aging, aplit the eut part of backing, board by bending the board gradually, with the test piece being inside, paying atten: tion not to damage the test piece, fix the test specimen to the fatigue teater in the chamber kept at (20:22) °C of inside temperaLure and leuve the test xpecimen in the: chamber at the inside temperature for at least 1 h. Increase and decrease the split of the backing board from 0.5 sm to 2.5 mm repeatedly 200 times at u rate of once per two min, and then deerease the split to 0.5 mim. Next fix Une taat specimen t0 the fatigue tester in the chamber kept at (0 =2) °C of inside temporature, stand for at leaat 3 b and then repeat the above inerease and decrease 400 tins. After completion of the above procedures, make the split of backing board croased to 2.5 mm, observe the surface of the test piece viaually, and examine ‘whether any cracks, tears or breaks take place oF not 6.12 Wlexural property 6. ‘est equipment The Lest equipment shall be as follows (1) Bending dovieo The bending device shall consist of'a mandrat, a patr of sup- porting rollers, a supporting roller framo, a mandrel teunsfer doviee und ther- ‘mastatic chamber ax shown in Fig. 9 (a) Mandrel The mandrel ahall be a cylinder with » diameter 20.0 mm and ‘sTength 50 mm or more sehich can be vertically transforred. () Supporting roller The supporting roller chall have diameters of 19.5, mam, 20.5 mm, 21.5 mm, 22.8 mm, 23.6 mu, 24.5 ma, 26.5 mm and 26.5, ‘ma and a lengab of 60 mm or more. center distance of 51.5 mm. (@ Mandrel transfer device ‘The mandrel tranefer device shall be capable fof moving the mandrel at a constant rate (@) Thermostatic chamber The thermostatic chamber shall be capable of immersing the mandrel and supporting rollers of bending device into the liquid and controlling the temperature of liquid in tho chamber at the set temperature 11 °C. Note (?) "The liquid shall be a type of alcohnl or water. (2) Heating thermostat The heating thermontat shall be an speeiied in 6.5.1(2).6.12.2 Heat treatment of test piece The heat treatment of test pieces shall be 1s specified in 6.8.2 (1). 6.12.3 Test method Place the bending device in which the supporting rollers of the diameter selected from Table 8 corresponding to the marked value of thickness ‘of roofing and the test pieces in the thermostatic chamber controlled at a prescribed ‘temperature in Table 2 for 30 min or more for aging. Place the test piece on the horizontal rollers, immediately bend the test piece through 180" by moving the ‘mandrel at «speed of $00 mavimin, and examine whether cracks appear on the outer ‘surface or not") However, carry out the test by making the front surface inside only, for exposed ‘Table 8 Diameter of supporting roller corresponding to marked value of thickness Unit: mm ‘Marked vale of thiekness Diameter of supporting roller Toor overte and exch 20 2 20 or overt and enh 25 255 | ‘2B er over wand el 30 ms ‘Der ovr t and enh 35 as 35 er ovr toad ech 40 Bs Der ovr to and ech 45 a5 “Ser over te and eal 50 ms Note () Laminate materials having no relation with fundamental proper- ‘es of roofing such as lining materials are not the object.Seate that test piece is placed $ er inst rantor Sice fella frac Fig. 9 Bending device (example) 6.18 Conversion of numerical values In the euso of Lost with using of tester tor measuring apparatus with conventional unit, the conversion of numerical values tccnrding to the international unit system (ST) ahall be wx follows: 1 kgf = 9.80 N 7 Tnmpection’ In the inspostion, the texts ¢hall be carved ut in uecordance with 6 tend the pas or reject of rorults shall he determined uccurding, Uo the provisions of 8, 44 and 6. The inspection may be carried out based on u reasonable sainpling inspee- tion plan. ‘The innpection of fatigue resistance shall be carried out at the change of produc. ton conditions, 8 Designation of product The product shall be designated by the name of prod- ‘uct and by the classification of use, material constitution and temperature charae- teristic. Fxomple : Polymer-modified bitumen roofing sheet expased single-layer water: proofing, clus R, class 1 9 Marking The following items shall be marked on an et ‘each packaze of a coil product ily visible position of 41) Name of product (2) Class or mark (8) Thickness, width, length, mase per unit area, and exintence of cut in a eal Gf exists)8 A013: 1996 (4) Method of jointing roofings each other (6) Method of pasting on foundation sheet (©) Date of manufacture oF its abbreviat (1) Manufacturer's name or abbreviation (8) Name of manufacturing plant or its abbreviation 10 Matters to be attended to at handling The matter to be attended to on the {following items at least shall be described on catalogues, manuals, ete. of roofing. (1) Attention to handling and storage (2) Attention to exeention (a) Conditions of foundation (&) Mutual jointing of roofing