Page No,

FEXPERIMENHO
AIM: o e a P-nahhttol Bnilins dyn

APPHRATUS REQUIRED:
Conical Hask, Suakon,icaJath,glas d, Bucmaukumnul, uakx pump

CHEMICAS REQUIRED:
Amilima =5m Conc HCQ =lo ml
Sodiumm NitYile= 2mnL lolaNaCH80luHon= 60m
B-NapHhol= 35mL

HEORY:6-Naphal nilina dye phomyl-az0-B Naptaol ia an

MoMge u-TtleloMgs do a Jaug clax ot azo compoLna, all a
ushioh cotain tho ehakaceuiskie, Qu0uhinocNEN-CE.Azo comp
nunds oxo al calouwod oahounds kouHo hoha0dHOn ok
hia dun,uiline i diazatiaud ond hon diazoubn salt tius
oldainods suljenked to couhling sacttom.with -Napd.

PROCEDURE:
Hako a Loo ml. comical Rosk omd add 2.5mLof nllina, lOmLok c.HQ
Omd lOm. ok waku. Cool.tuis ADlukon cto 5°Cl hlacimg tho uonical
lorR_ in a tuouga contauning.ica cold_unkz
na loDml biaku, disanl ug eh Aodiun nivile in 20ml wale
Od colhis 20luhen also ta 5'C
No &louslu, odd Aodium nituik solution do ho olutiono eniltne
n come HCO
CLASSTIME
 Experiment: Date
Page No.

DibadlineRIg B-Naptmal in 6omL ok lo/ NaoH AoluHem frk

250 mL beoRaA andl caol this soluhen do5 C udy plaing.n.0 -

Lak3oma_couuahedia may ba added diot do.Jacilitale.coo

NouHadiazoHasd aoluton_uwas added veylously to Me P-Nap0
80ukon uih tonstat atiusdng.Yha mind aotuions immedkon
|daeloheda wd oloun amd P-Naptthol milinaMapidy_a
OMAMge d uyatals.
whwm tHh additon of_diazo 30lusio was_conmhla e mNLL
wsas allDLed uto atand in ica sat mintu kou B0min ualHa.
oOcaonal tiuuing.Eeu the 30lukion theaugna buchna n2
wwau 2uuntion Juom hafump. Nheuyatala uso washodl uulHa
wakx ad duy cuyAtals uu altained by Jusig Jetuser

a Paundust uwaasuuoatallized uom gtasial acekic.asid. Eir

e ouatals uas don.I waa washud uslt a huoms ethama
to moe ackc add. Phmyl azo-B-napHaol uoas oltained as
oxangasudustal. eapaed yietd is 2g aud nmelRna pointis1a7?c

RESULT: B-hapinAl amilima dyr uoasJuuhasuod

PRECAUON8
Alsays odd diazomium ehlouida Aslukon to B-naptthol aaluton
da matin and onat wce e a

AdAHoM o Sodium NihiBe alhAuld se uy alowJwcauantha

0Mahon Js eoHhaumic.and may cauas tho kemhuaku

CLASSTIME