SURFACE

CHEMISTRY
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PRLPARANON OF LYOPHILIC SOL

AIM: l o pretaae colloidal coution (sol)oE
ar ch
HEORY Slash fanos a uophiic wbencol
uatexis_used as the dkpersion rmediuro.
Ihe tbnoalion_of sol fs _aueloraled y haatira
The staachsol can be me pared by dea
ting
Stash and uiales at aheut 100:OIEsquute
stable and ic nof affeuked by the pzecoce
of anu eluknlytic inoput
APPARATUS Pake ys_(250M and soml,aaks
nd ,funnel, iltex_papex Pestle ard rvota
pod etam wine-qauzeand euaDey.

MATERALS REQUIRED Goube staah 50oa

and distilled watex

PROCEDDORE: I) lake boorog of staah in a

Motaand add tav m of _distilled water
2 i n d the stasdh t ake a thin paste and
tanste this paxte to_a bOM beaker
3 acouLoo distiled_wate in a
25Dm beaker and beat he beaker so that
watey etaits boilinq
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into
4ouhe pasle slowly wth sl inD
boi ling watey în te beake
C o i n e boiling o about lo Minute ord
then allaw the ) beaker b coo
JeFikex he Loptents o be beaka hmuah
A HRtex-papez medin a:lunnel: labe W
ilorake Gtasch sol
Sot
KESULT2Starckh sabpieg przpaiLd
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PREPARATION OF LYDPHOBIC SOL

AIM lo paepise aic hucovnide He (DH),sol
HEORY eic hudaonide dros a yopho bíc
so heSsulbstancde. suuh_asmetal ydronides
OYSulphides wbich ane fnsoluble on do o
adily Qve_colloidal Coluions DD eatroerH
with baley aue called yophobie
Loll01ds
Eezi byudapude so is pzepaaed e
hydnlysis"ol fic chlid with koili
dstied_uyakex.The xLactionHhat takes
place Can be e.poes.ented ak
Fela(aa)+ 3Hhol)oil FeOH),(6) +3H(lag
Feaic chlonide Redsol
he hudio usis xactioD pmducLer îcoluble
Acic bydkomid. astices which uodngo
agalorodisation i l d bigy pastila
o (olloidal_diroenian H_paaticles
ahsoo Fe 2t ions prtexentialy i n a thbe.
Solutioo fo giveositive_chashe to the solL
pastiles Shlility o the so (s_duu to the
chasqoh
chaiq be s paticda. tlsdaochloic aud
w h t s pwduced duMna hydioyss
disabflizesthe coland hince it out MUAt

be xenOOVed_too tkhe so_by dialusis_proCEAs,

othenwe sol uill_pet be _aulilable
 ATEARATUG(onical Lak (250 mL), beakeY
250 ML)a bDiina-uke alass- Dd Aunnel
2aund battono -[lask ixco clandwHha clannp
IKe=qauze, taipod-sland buuney anda
busete ora_daoppe

MATERIALS REQUIRED 2%solulicon of tenic

chtoide Cpepased u disc.olving 24 0
pule lecl, Lonal istilled whlen)apd
disti Pled waker
PROCEDURE:) Take a 2500l_conicel taxk
ard clean it h steanoin4-Dut pmLeSS
To hisdeaned 0-ask add lool of disilled
oakey and heat lt to kail by placna ihe
40axk On awine-QAuze
Addfenic chloil edlulion doupuice (a te
Use ota bumette tra doppe) o the boilirg|
waker
GCortinul healing until deup ed pboon
Solution f teic hydoide is obtained
Replace. 1he waler Post le2vaporakion dunng|
boilinq_ at xequlas intewdls_
5 Kecp UHhe Lontents of Conicco ILaxk undis-
4uabed to Sanetioe at roonoLpopexatuae.
abel he colutin as Feric yduide Sol
sal
IKESUL Earic bud nnide sotttioen is pepased