Course Short Syllabus

MEDAN STATE UNIVERSITY

FACULTY OF MATHEMATICS AND NATURAL SCIENCES
DEPARTMENT OF CHEMISTRY
SHORT SYLLABUS
Nama Separation Chemistry
Course Name Kode 3KIM48320
3KIM47318
Kredit 3 CREDITS
Semester Odd 2021/2022
DESCRIPTION OF COURSES
This course discusses the concepts and procedures in separating analytes from a sample using the separation methods by distillation,
extraction, sublimation, centrifugation, chromatography, and electrophoresis as well as identifying them qualitatively and/or
quantitatively.
ACHIEVEMENT OF COURSE LEARNING (CPMK)
1 With program learning in this course, students are able to understand about the concepts and procedures in separating analytes
from a sample using distillation, extraction, chromatography, and electrophores separation methods and identifying them
qualitatively and/or quantitatively
SUB-ACHIEVEMENT OF LEARNING COURSES (SUB-CPMK)
1 Able to explain concepts in various methods of separation
2 Able to explain concepts in various methods of distillation

1
3 Able to explain concepts in various sublimation methods
4 Able to explain concepts in various extraction methods
5 Able to explain concepts in various centrifuge methods
6 Able to explain concepts in various chromatography methods

7 Able to explain concepts in various methods of electrophoresis

LEARNING MATERIALS
1 Semester Learning Plan and Course Contract
2 Introduction to Separation
3 Distillation
4 Sublimation
5 Extraction
6 Centrifuge
7 Chromatography
8 Electrophoresis
MAIN LIBRARY
1. Suharta. 2009. Dasar Pemisahan analitik.Medan: FMIPA Unimed
2. Harvey, D. 2000. Modern Analytical Chemistry. US: McGraw Hill
3. Christian, G. D. 1994. Analytical Chemistry. 6th Ed. New York: John Willey and Sons.
4. Anderson. 1991. Sample Pretreatment and Separataion. London: John Willey and Sons.
SUPPORT LIBRARY
1. J.Chemical Education
2
 2. J. of Physical Chemistry
3. Journal of Chemistry Education and Learning
4. Journal of Chemical Research
5. Indonesia Journal of Chemistry
6. Indonesian Journal of Chemical Science and Technology
PRECONDITIONS (If there are)
Passed Quantitative and Qualitative Course

3
 Document
Code:
MEDAN STATE UNIVERSITY
FACULTY OF MATHEMATICS AND NATURAL SCIENCES
DEPARTMENT OF CHEMISTRY

COURSES CODE FIELD OS STUDT WEIGHT (credit) SEMESTER Tgl Drafting

Separation Chemistry 3KIM48320 ANALYTICAL CHEMISTRY T/P=3/1 6 February
3KIM47318 2021
AUTHORIZATION RPS Developer: RMK/ KDBK Coordinator Head of Prodi:
Team Teaching: Dr. Ely Djulia, M.Si
Prof. Drs. Manihar Situmorang,
M.Sc, PhD
Elfrida Ginting, PhD

CPL Prodi
Learning CPL-2 Upholding human values in carrying out duties based on religion, morals, and ethics;
Achievements CPL-3 Contribute to improving the quality of community life, nationhood, state, and the advancement of civilization based on
Pancasila;
CPL-9 demonstrate a responsible attitude to work in his area of expertise independently;
CPL-13 Mastering theoretical concepts, principles, methods, and techniques of identification, characterization, isolation
(separation), and analysis of molecular reactivity;
CPL-14 Mastering the concepts and principles of environmental conservation in general;

4
CPL-15 Mastering general concepts, principles, methods, techniques, and complete operational knowledge of functions, how to
operate common chemical instruments;
CPL-16 Mastering the concepts and methods of analyzing data and information resulting from chemical experiments;
CPL-18 Mastering the principles, methods and techniques of implementing Safety, Occupational Health and environment (K3L)
in laboratories and in the field, in particular the handling of hazardous chemicals;
CPL-20 Mastering general concepts, principles, and techniques of effective communication orally and in writing, on the scope
of chemical science;
CPL-24 Able to conduct experiments (experiments) identification, analysis, isolation, transformation and synthesis of chemical
molecules responsibly, analyze data and information obtained from experiments, and produce appropriate conclusions
in accordance with scientific ethical standards;
CPL-27 Able to utilize chemical science in everyday life;
CPL-32 Able to explore the potential of natural resources to be utilized as a base of learning, research and devotion;
CPL-34 Able to apply logical, critical, systematic, and innovative thinking in the context of the development or implementation
of science and technology that pay attention to and apply humanities values in accordance with their area of expertise;
CPL-35 Able to demonstrate independent, quality, and measurable performance;
CPL-38 Able to make decisions appropriately in the context of problem solving in their area of expertise, based on the results of
information and data analysis;
CPL-40 Able to be responsible for the achievement of the results of group work and conduct supervision and evaluation of the
completion of work assigned to workers under his responsibility;
CPL-41 Able to conduct a process of self-evaluation of working groups under his responsibility, and able to manage learning
independently;

5
 CPL-42 Able to document, store, secure, and rediscover data to ensure validity and prevent plagiarism;
CPL-43 Able to adapt, work together, create, contribute, and innovate in applying science to community life and able to act as
a globally minded citizen of the world;
CPL-44 Able to uphold academic integrity in general and prevent the occurrence of plagiarism practices;
CPL-45 Able to use information technology in the context of scientific development and implementation of areas of expertise;
CPL-46 Able to use at least one international language for oral and written communication.
Achievement of Course Learning (CPMK)

CPMK With program learning in this course, students can understand concepts and procedure in analyte separation from
sample using separation methods such as distillation, extraction, chromatography, and electrophoresis. Furthermore,
students should be able to identify the analyte quantitatively and qualitatively.

Indicator -CPMK Master and understand concepts and procedures in analyte separation from sample by using separation methods by
distillation, extraction, chromatography, and electrophoresis and identifying them qualitatively and/or quantitatively.

CPL-Sub-CPMK
Sub-CPMK 1 Able to explain concepts in various methods of separation
Sub-CPMK 2 Able to explain concepts in various methods of distillation
Sub-CPMK 3 Able to explain concepts in various sublimation methods
Sub-CPMK 4 Able to explain concepts in various extraction methods
Sub-CPMK 5 Able to explain concepts in various centrifuge methods
Sub-CPMK 6 Able to explain concepts in various chromatography methods
Sub-CPMK 7 Able to explain concepts in various methods of electrophoresis
Short This course discusses the concepts and procedures in separating analytes from a sample using distillation, extraction,
Description of chromatography, and electrophoresis separation methods and identifying them qualitatively and/or quantitatively.
MK

6
Study 1. Semester Learning Plan and Course Contract
Materials / 2. Introduction to Separation
Learning 3. Distillation
Materials 4. Sublimation
5. Extraction
6. Midterm Test
7. Centrifuge
8. Chromatography
9. Electrophoresis
10. Final Exam
Main:
Book 1. Suharta. 2009. Dasar Pemisahanalitik.Medan: FMIPA Unimed
2. Harvey, D. 2000. Modern Analytical Chemistry. US: McGraw Hill
3. Christian, G. D. 1994. Analytical Chemistry. 6th Ed. New York: John Willey and Sons.
4. Anderson. 1991. Sample Pretreatment and Separataion. London: John Willey and Sons.
5. Sri Adelila Sari. 2019. Separation Chemistry. Jakarta: TSmart.

Supporter:
- J.Chemical Education
- Journal of Chemistry Education and Learning
- Journal of Chemical Research
- Indonesia Journal of Chemistry

Lecturer: Team Teaching

Prof. Drs. Manihar Situmorang, M.Sc., PhD
Elfrida Ginting, PhD
Requirements Passed Qualitative and Quantitative Analysis Chemistry Course
Courses

7
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
1 Understand and There is an agreement spelled out There is an • College: • Lecture contract and -
agree on rights and in the college contract and RPS agreement • Discussion, lecture order.
obligations related to spelled out in [TM:1x(3x50")] • Provide routine tasks
Chemistry Separation the college of literacy (reading and
courses that include contract and Online understanding)
study materials, RPS material to be learned
learning systems, Explaining RPS, college at the next meeting.
types of tasks and contracts, lecture materials,
assessment systems. supporting literature, how to Semester learning Plan
assess and bill tasks (routine file and College Contract.
assignments, CBR, CJR, Idea Username and Class
Code
Engineering, Mini Research,
https://elearningfmip
Project)
a.unimed.ac.id/

2 Explain concepts in Accuracy explains the basic Routine Tasks Lectures + Group Discussions 1. Basic concepts of TR1
various methods of concepts of separation methods (TR1) and CBR Lecturers give lectures on the separation part of
separation • Accuracy in classifying separation topic of the basic concepts of 2. Classification of F1;
methods separation methods. Students separation
• Able to perform filtering do exercises in the form of CBR part
techniques routine tasks (TR1) and CBR Material uploaded at of F2 (see
[TM:1x(3x50")] https://elearningfmipa.un assessme
imed.ac.id/
nt
Online
system)

8
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
Assignment:
Routine Tasks (TR1)
Critical Book Report (CBR)
Task Design
• Students provide
Texbook or teaching
books that have to do
with topics about
various methods of
separation
• Books that will be
reviewed at least 2
pieces
• Review results are in
written format

Learning Resources and Media

used:
1. Laptop
2. Google Meet/Zoom
3. Texbook/ Teaching
Books
3,4 Students are able to Accuracy in classifying the types of Routine Tasks Lectures+ Group Discussions • Simple distillation TR2
explain concepts in distillation (TR2) and Lecturers give directions and • Fractional part of
various methods of • simple distillation, Projects (PR1) students have discussions on distillation F1;
distillation • Fractionation, the topic of distillation • Azeotrope
• azeotrope, distillation PR part
• Low pressure of F3
9
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
Students work on exercises in • Distillation with
the form of routine tasks (TR2) low pressure
and Projects (PR)

[PT+TM:(1+3)x(2x50")]

And

[BL:1x(3x50")]

Blended learning through:

https://elearningfmipa.unime
d.ac.id/

Online

Assignment:
Routine Tasks (TR) and Projects
(PR)

Learning Resources and Media

used:
1. Laptop
2. Google meet/Zoom
3. Texbook/ Teaching
Books
4. Practicum equipment
and materials

10
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
5 Students are able to • Accuracy in understanding Routine Tasks Lectures + Group Discussions • Understanding TR3 part
explain concepts in the meaning of sublimation (TR3) and Idea Lecturers give directions and Sublimation of F1
various sublimation • Accuracy in understanding Engineering (RI) students have discussions • Sublimation
methods about the basic concepts of RI
terms, equipment, and Requirements
sublimation part of F2
sublimation applications • Equipment and (see
Students do exercises in the applications assessme
form of routine tasks (TR) and nt
Engineering Ideas (RI) system)

[BL:1x(3x50")]

Blended learning through:

https://elearningfmipa.unime
d.ac.id/

Online

Assignment:
Routine Tasks (TR) and Idea
Engineering (RI)

Learning Resources and Media

used:
1. Laptop
2. Google
Meet/Zoom

11
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
3. Texbook/
Teaching
Materials
6,7 Can explain concepts • Accuracy in understanding the Routine Tasks Lectures + Group Discussions • Distribution law TR4 part
in extraction methods laws of distribution (TR4) and Mini Lecturers give directions and • Extraction of F1
• Accuracy in understanding Research (MR1) students have discussions on Techniques
extraction techniques the concept of extraction MR part
• Solid extraction
• Accuracy in understanding solid of F3
extraction Students do exercises in the • Use of Extraction
• Accuracy in understanding the use form of routine tasks (TR).
of extraction
[PT+TM:(1+3)x(2x50")]

Online

Assignment:
Routine Tasks (TR)

Learning Resources and Media

used:
1. Laptop
2. Google
Meet/Zoom
3. Texbook/
Teaching
Materials

12
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
4. Practicum
equipment and
materials
UTS part
of F4 (see
8 MIDTERMS (UTS)
Rating
system)
9 Can explain concepts Accuracy in understanding TR5 and CJR Lectures + Group Discussions 1. Classification of TR5
in various • classifications, Lecturers give lectures on the chromatography Part of F1
chromatography • terminology, concept of chromatography 2. Chromatography
methods • developments and Terminology CJR
• working procedures Students do exercises in the 3. Development and part of F2
of chromatography form of routine tasks (TR) and working procedures of (see
CJR chromatography assessme
nt
[PT+TM:(1+3)x(2x50")] system)

Online

Assignment:
Routine Tasks (TR) and CJR
Learning Resources and Media
used:
1. Laptop
2. Google Meet/Zoom
3. Texbook/ Teaching
Books
4. Journal

13
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No

10- Students are able to • Accuracy in understanding Routine Tasks Lectures+ Group Discussions • Solid-liquid TR5
11 explain the concepts the principles of solid-liquid (TR6) and Mini Lecturers give directions and adsorption part of
of various column adsorption Research (MR2) students conduct group chromatograph F1;
chromatography chromatography discussions with the basic y
methods • Accuracy in understanding topic of column spectroscopy • Partition MR part
the concept of partition chromatography of F3
chromatography Students do exercises in the • Chromatography
• Accuracy in understanding form of routine tasks (TR) and of ion exchange
the concept of Mini Research (MR2) • Gel
chromatography of ion chromatography
exchange [PT+TM:(1+3)x(2x50")] • HPLC
• Accuracy in understanding
the concept of gel and
chromatography
• Accuracy in understanding [BL:1x(3x50")]
the concept of HPLC Blended learning through:
https://elearningfmipa.unime
d.ac.id/

Online

Assignment:
Routine Tasks (TR5)

Learning Resources and Media

used:
1. Laptop
14
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
2. Google Meet/Zoom
3. Texbook/ Teaching
Books
4. Practicum equipment
and materials
12 Can explain the • Accuracy in understanding paper Routine Tasks Lectures+ Group Discussions • Introduction to field TR1
concepts of chromatography (TR6) and Lecturers give directions and chromatography part of
chromatography field • Accuracy in understanding thin Projects (PR2) students conduct group • Paper Chromatography F1;
layer chromatography discussions with • Thin Layer
chromatography topics in Chromatography PR part
the field of F3

Students work on exercises in

the form of routine tasks (TR)
and Projects (PR)

[PT+TM:(1+3)x(2x50")]

Online

Assignment:
Routine Tasks (TR6) and
Projects (PR2)

Learning Resources and Media

used:
1. Laptop

15
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
2. Google Meet/Zoom
3. Texbook/ Teaching
Books
4. Practicum equipment
and materials
13- Can explain the • Accuracy in understanding Routine Tasks Lectures+ Group Discussions • Introduction to gas TR1
14 concepts of gas equipment in gas (TR7) and CJR Lecturers give directions and chromatography part of
chromatography chromatography students conduct group • Silent phase and F1;
• Accuracy in understanding the discussions on the topic of gas motion phase in gas
stationary phase and the motion chromatography chromatography CJR part
phase • Application of of F3
• Accuracy in understanding Students do exercises in the qualitative and
qualitative & quantitative form of routine tasks (TR) and quantitative analysis
applications CJR

[PT+TM:(1+3)x(2x50")]

and

[BL:1x(3x50")]

Blended learning through:

https://elearningfmipa.unime
d.ac.id/

Online

Assignment:
Routine Tasks (TR) and CJR
16
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No

Learning Resources and Media

used:
1. Laptop
2. Whiteboard
3. Texbook/ Teaching
Books
4. Practicum equipment
and materials
5. Journal

15 Can explain the • Accuracy inunderstanding the Routine Tasks Lectures+ Group Discussions • Introduction to TR1
concepts of various classification of electrophoresis (TR8) and CBR Lecturers give directions and electrophoresis part of
methods of • Accuracy in understanding zone students conduct group • Electrophoresis zone F1;
electrophoresis electrophoresis discussions on the topic of • Gel medium
• Accuracy in understanding the electrophoresis electrophoresis CBR part
technique of electrophoresis technique of F2
medium gel Students do exercises in the
form of routine assignments
(TR) and Critical Book Report
(CBR)

[TM:1x(3x50")]
Online

Assignment:
Routine Tasks (TR) and Critical
Book Report (CBR)

17
 Sub-CPMK (Final Form, Learning Methods & Assessme
We Criteria & Form Learning Materials
ability of each stage Assessment Indicator Assignments (Media & nt
ek of Assessment (Library)
of learning) Learning Resources) Weights
No
Learning Resources and Media
used:
1. Laptop
2. Google
Meeting/Zoom
3. Texbook/ Teaching
Books
UAS part
of F4 (see
Assessme
16 FINAL SEMESTER EXAM (UAS)
nt
system)

18
RATING SYSTEM
The Assessment System refers to the academic regulations of Unimed, by determining in advance the final score with the following formula:

Component Definition
F1 Routine Tasks
F2 Critical Book Riview (CBR), Critical Journal Review (CJR) /Critical
Research Review(CRR) and Engineering Idea (RI) with the provisions
F2 = 0.2 CBR + 0.3 (CJR/CRR) + 0.5 RI
F3 Mini Research(MR), Project (PR) with
F3= 0.4 MR + 0.6 PR
F4 a. Knowledge/Skills Exam (Midterms)
b. Knowledge Exam / Skills (End of Semester)
With provisions
F4 = 0.5 F4a + 0.5 F4b

Final Value (NA) = 0.1F1 + 0.2,F2 + 0.15 F3 + 0.65 F4

With the provisions:
Grade A, If 90 SA 100
Grade B, If 80 SA 89
Value C, If 70 SA 79
Grade E, If 0 SA 69 (not passed)

19