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VOLUMETRIC
ANALYSIS

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THEORE TI CAL WEIGHT (AL(VLA TIDN

20
Moh | 000
dolution
whe,
M = Nolan mas y lshd hak = 392 q
M =
20

Aount Mah t.equind 342 xL Xl00

20
I000

DBsERVA TIONS AND CALCULA TIONS

10DX34 2
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ESTIMATDN DE kNnd4 RoLLmON
SoLUnON SIN M20 fERROUS
ANMONIUN SULPHATE CMOHR'SCALT] SOLUTIDN
AIN:

Ennous amanaonima
APPARATLS REQUIRED:
Wateh alawAsomL Lnical ask lDoml
Vlunmsti last, ppitt nett tunelalast
dette Fimua ammeniun Aulphati seutieay
kilaDt Jslutica, Dil lupausie auid aad chnual.
aalame
THEORY:

REACTION OF DÁ ALIC A
AciD wITH KNnl4

LA) NoLECULAR EQUATION:

2kMnl t 3HaSo4 > kso4 + NHn So4 t 3H0 +5[0]
2feSey-CNH4 so4: 6Hyo tAsSo4 f[o]->e, (serbt

KSo4 tANn 504 +5fe, (DAh +lo (NHu),S04 +6&H, 0

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DBSERVATION. TABLE

SND VOLUME OFBJRETTE READIN6VOLU ME OF kMn04

MOHR'S SALT INT IAL (m) FINAL (ml SOLUTION USED
SoLUTION

20:0
200 200

2 20'0
20'0200;
CONORDANT VALVE = 200 mL

A CAPAITY of PIPE TTE VsED = 20m

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CB) TONIIC EQUAION:
Mn Da t8Ht +5e >Nnt t4H,0
te 2+ fe 3+
+e- x5
Nnl4t gHt + 5Fe 2t ’ Nn2t +5fe 3t +4H,0
PROCEDURE:

PREPARATiON DE STANDARD R01UTION Df NOHRs SAL:

ueighin
'AN HS4 (to phostat ydalysis) aand make dup o
Imamk ueng distlbd wat
alath
ESTINATIQN CF KNnl4 uSINn Ml0 MOHR'S RALT:
20m. Mokad salk Ituisii pipetted_eut inta
la lonilallast aad teat tile s tN Hso4
i added dad taean tilaatzl agaisyt KNne4 talL
pade pinak. laleu
abbeane Repeat the abae_photedune titatian ta
qet at lbat kun konaxdant Aeadingi.

Teacher's Signature:
 KNnla: STRENGTH.
OF (2)
200 O.
05X20:o 2X0
020 X 05 D:
solution
alt Ne salt pha
t
Veume
kNnoy Soltin kMnly kMny
3OLUTON:: kMn04 OfRITY MoLA
Df ()
ALCULATIONS C
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LNDICATOR:
KNn D4 is a ll ndiuta.
END PoNT:

RESULT:

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THEORE TICAL WE IGHT CAL(ULATION
Fo pupang loom
fox M
.= MXMY
oLaie aud sution

M = 1268
50

V= Vme Dalis avd mae ub m ml =lo0ml

mont
50
000

= 0 2529
DBSERVAT)ONS AND CALCVLATIONS:

=
= 0252 9
aity o oralu auid oystel = 0252 X100o
I00 Xl26
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ESTIMATiON DF PoTASSIUM PERMANGANATE USÍNG M|50
OXALIC ACID
AIM:

DLalii aid

APPARATs REQUIRED:
250 ml. conital ask, Iooml Vumetii
ast, pipet,tunl, ash dst, unett Dxalie
aid iblutiem kunlyAolutien, diluka sulpluni aid,
hemital ualaneetc
THEORY

NOLEULAR EouATIDN:

2Kun04 t 3Hs SO4 >ko S04 tQNnso4 +3H,0 +501

2kNa O4 + 3H, SO t6HC04.2H,0 >k So4 t 2Mn So4 +(olo,t

TONIC EQUATION:
t 5e Hn2t. +440 X2

C204cgtle x5
Teacher's Signature :
 ml20 USED
= TTE PIPE CAPACITY
DF *
=60ml VALUE CoNCORDANT t
16-9 1
)(museD SOLUI
ON FINAL[ML) (ML) NIDAL ACID DXALIC
un04 VOLUME
0f READING BURETTE VOLUME
Of SNO
TABLEOBSERVATiON
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2 Mn D4tlbHt + 5G D4 (oto ta mn2t t&H0

PRDCEDURE:

PRERARATON DFS TANDARD SoLUNoN Of XALIC ACID

SOLUNON :

0:02 Mola Aolstinn is oali aia prepaned dey

mank uwiag distilled watin

ESTIMA TlON Of kMnD4 USING Ml5D 0XALIC ACID: -

|20m olali aud Aoldiem iu piptthd gut iuta a

liato HhA heated tota bo -0°c aned ditnatd
Lagaist
akpeans- Repeat the abee predune st titatias ta
qt atleast turo tenondant HUadini

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CALCULATIONS:
| : MOLARITY

kunOy ouihon

auid soltiau OLalie aud oution

Molant kMno stin x1 b : 0 2

Moaõut kunl4 = 2x0:02X 20

l6x5

(:) 9TRENGTH of kNno

I<Mnb.
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INDICATOR :
kun04i a
END POINT:
Lalounlem

LRESULT:

Teacher's Signature:Syon G