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Chemistry Students' Lab Guide

The document describes an experiment to determine the aniline point of a sample using a thermometer, heating mantle, and sample mixture of aniline and diesel. The procedure involves cleaning and setting up the apparatus, adding the aniline and diesel sample to a test tube, heating and stirring the mixture while monitoring the temperature, and noting the aniline point temperature where the liquids become miscible. The results show the aniline point of the sample tested was 56°C.

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Rishi Kesh
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134 views4 pages

Chemistry Students' Lab Guide

The document describes an experiment to determine the aniline point of a sample using a thermometer, heating mantle, and sample mixture of aniline and diesel. The procedure involves cleaning and setting up the apparatus, adding the aniline and diesel sample to a test tube, heating and stirring the mixture while monitoring the temperature, and noting the aniline point temperature where the liquids become miscible. The results show the aniline point of the sample tested was 56°C.

Uploaded by

Rishi Kesh
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Ain: To detenine the andine nont

noint the n
Olaerticnsi T, 66'c andine point uc
7, 57c syation ont
weight ju 1) :018 g /1o
Lt, jadirel= 22:87Sg/bpl.
t.of j+ nlne 25.7s99lol
Diagnn:
&Anilnu noint themomde

tet e.
sl
yacted

Aniine noint annantus


Dotg 4/2/2
Expt.No. 3 Page No.

Exreimnt No- 3.
Aun: To detemine the Ariline ont of be
Sample id Dierel and Aniline(só2e )
Amarastus and chemicalb uied i Heating and
cooing wate thenomet sti, wiyhiny mehirn,
tle anilinedieuil tet
tae jacket, iesel - Aniline miatue.
Theoyi Aniline ntint is the mirinun gililn
sodetion temnwatuc Foz lqual votume ariline
and ethanoi disel, it sens as an indicatin
tynes hydoalon pent in sodst and pnt
Ehe degee amakcity
proredue
dean and dy the aprantus
2 Pou5nd ofaniline and s m f sanple il to a
tert tule.
3.ente the thmonete n the t t tede matisg
sese that hulk dont touh the side f tule
stir the mixtue anidy wning stie.
SAyy heat to the eguiment and contiree stimg
bil miscility à atained.
b.The point uhee minitility of liguids in ttaired
ae anidine noints
2.Nou allou itt to cot for a cetain tine nL then not
the temment. f lay Jtamed
Taachar's Signatura
Expt.No.
Arilin
dilt S ml
Sod B.No
Amunt o sample
Anulirepoind
srntitn noint s>'c
11-08&g Pro
sample g.070
t.ot ja O18 =
4-088 - l:
Hrce s. =
ten
at room temy
f.gr of diyel conction fator =
oooY6.
eonding
o 8074 000
.: S. G. at 6o/so F O81|b

A I = 141:5-3/-Sc 42-8
08|b

eel Index - AI x Ayire int

100

odar nwdy 0-72 x DI) +10 ).


2.
3
303L
Dato

Expt. No. Page No. 13.

ANde the adig (seejfie aaniy) j disel uning


etie grty otle.

Prrzei lean and dy the v tula and auang tha


4yant desined. Nou add sml of diitilled, nd Snl
11 duel Sarnl gff iren Samnle n the u' tue,
Aage the aaats uith stisen in such way
that lquid in u' tle and the nans ff the
haker ae stind sinultanonly. suiteh on the
heatw to heat the nanpFn at a contoledd ate
so thue is no such ditfene in tennatse f
paain lateh and u' tule.
Rerulti
Aniline noint of28:22
iren samle b6c.
Diesel
’ Mised Anilinepint of girn samle se
>octan nuner = 30:36

Peautins:
LDo not toeh r tast any wntrtun sulatance
2 Do not mie sample y j t
3.Use ony
out rwiment.

Teacher's Signatura

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