QUY TRINH SAN XUAT Md s6: NCPT/QTSX/0OI

u6N DICH cAN QUANG LAn ban hdnh : 01

Ngdy ban hdnh :
Ipn t6m vi sirc kh0e 4;ffiRISULFAT 08 10312020
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2. Phdng DBCL B6n copy

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4. Phdng k6 hopch - vflt tu BAn copy

5. Xuong sin xu6t BAn copy

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 QUY TRTNH SAN XUAT Md s6: NCPT/QTS)VO0I
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# r,"pHAnM u6N DICH cAN QUANG Ldn ban hdnh : 01
Ngdy ban hdnh :
BARI SULFAT 08 103t2020
Phdng: Nghi0n crfru phit Trang 215

G TIN SAX PHAM

phAm: Hdn dich cin quang Bari sulfat
bdo ch6: H6n dich- 550g/chai
3. Y6u cAu ch6t lugng:
- 56 luqng: 55kg - 100 chai
- Mdu sdc: miu tring dgc
4. C6ng thirc cho 55kg - 100 chai
A
56 luqne
STT NGUYEN PHUaa LIBU DVT Ghi chri
Dinh mrl'c Thuc tli
1
Bari clorid kg 30.68 Bari
Natri sulfat 21.84 sulfat
2 kg 26ks.
a
Na CMC
J
(Natri carcoxylmethylcellulose) kg 1

4 Nipagin o 10
t)
5 Nipasol o 5
b

6 Saccarin o 30
7 Vanilin o
D 20
8 Acid hydroclorid l0% ml 450
9 Nudc RO lit Vd

rr.QUY TRiNH SAN XUAr

1. So dd quy trinh
. Scr dd bho ch6 nguyGn liQu Bari sulfat:

Dung dichNazSO+
L-
gan Dao noa

D0ling, lqc
Dung dich BaCl2 sQCh,

acid h6a bAng HCI l0%

 QUY TRiNH SAN XUAT Md s6: NCPT/QTS)U001
'Sarrex-ffiE u6N DICH CAN QUANG LAn ban hdnh : 01
*r\\ * r'pHAflM Ngiy ban hdnh :
BARI SULFAT 0810312020
tfim vi silc kh0e Trang:415
Phdng: Nghi0n crlu Phft
t/"*4
c,i lC9
= lujo
uAn bi nguy6n phg liQu, dqng cg miy m6c, con ngudi:
s w liQu:
16 rdng dring quy ch5.
- Thtrng carton, chai/lq dirng quy c6ch'
z.t.z. Dlrng cy mdY mdc:
- phdng lim viQc, m5y m6c, dqng cg cdn, pha ch6 phii s4ch, kh6ng 16n mtri lp,

chiSng nhiSm ch6o. C5c thiiSt bf phii an todn v6 Aign'

z.t.s. Nguydn fiQu:
- Linh nguyen lieu theo dfnh mirc k! thuQt. Khi linh nguyen liQu
phii c6 02 nguli,
liQu, d6i chitiu
trong d6 01 nguoi le IPC, ki6m tra ch6t luqng vd sd lugng nguyen
v6i phii5u xu6t kho, phiiSu kitim nghiQm nguy6n liQu'
z.t.t. Con ngwdi:
- Ngudi pha chti ph6i thlrc hiQn dirng quy chi5 vA vQ sinh an tol:r lao d6ng.
2.2. Pha ch6:
* CAn:
- CAn nguy6n liQu theo c6ng thric pha ctrti. Ctri ttrOi luqng ttrng lo4i vAo h6 so 16
s&n xu6t.
* Bho ch6 nguy6n liQu Bari sulfat:
- Hda tan 30.68kg Bari clorid vio 140 lit nu6c RO, dc !6ng llh, gan, b6 c6n, lgc
t0%,
trong qua 4 lop vii phin vdo thtng chira k1r6c c6 sin 450m1 Acid hydroclorid
thingr thoang khu6y dO acid phdn t6n dAu' (2)
>25oC , d€ llng l2h,
- Hda tan ZL g4kg Natri Sulfat vdo 100 lit nu6c RO c6 nhiet dO
g4n. b6 cin, 19c trong qura|lorp v6i phin' (1) ,
-> Cho tt tir (2) vdo (1) (khdng lirm ng*gc t4i), vira cho vira khu6y nhp nhdng, cho
ddv thtng
d6n Hri h6t dung dich (2). Khu6y ky d6 tria sulfat lang xu6ne
(250 1i0 th6m
- Rtra 1o4i t4p: Chia sin phAm Bari sulfat vira tpo ra vdo 2 thtng nhga
ti6p nu6c
nu6c RO dAy thtng, khu{y dAu, dC ling 5h, g?n b6 16p nu6c tr6n. Th6m
RO vio dAy thung, khu6y ky, de 16ng 5h, gan b6 l6p nu6c trong b6n
tr6n' Lhm nhu

v$y nhi6u 6n tl6n khi nu6c rfra kh6ng cdn phin rfrng cfra ion sulfat,
ion clo.
dugc
- Loai nu6c vi thu h6i eari sulfat: SAn phAm Bari sulfat clflc thu dugc & tren
chuy6n ,arrg 16 nhga c6 16t 4 lotp vii nilon, d6 r6c nu6c trong 24h
(him lugng nu6c
nA +rntrn R,rri srrlfat tir 48-52% ld duoc).
 QUY TRINH SAN XUAT Md s5: NCPT/QTS)U001
swru*.ffifr UON DICH cAN QUANG L6n ban hdnh : 01
Ngdy ban hdnh :
T0n tdm vi sfc khoe
BARI SULFAT 08 10312020
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R o6 tirrg, g4n rira nhiiru lAn

\&oru"-r*E
Nguy6n liQu BaSOa
Lo4i bot nudc qua vii

Nguydn liQu BaSOa

Chuy0n sang pha ch6

h6n dlch

.4r: .
-qtq1[ So tlti biro ch5 h6n dich Bari sulfat
ffi'
ONG fY (
tcpain.r
vflA na

lAt DUo! Ngflm 12h

SeJ-u.

Ch6t phs gia

(Saccarin, nipagin,
nipasol, vanilin)

Khu6y dAu lAn 2

Ki6m nghiQm b6n

thanh phAm

Ki6m nghiOm thdnh

,^
pnam
Ki6m nghiQm brin
thdnh phAm
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H6N DICH cAN QUANG Ldn ban hdnh : 01
Ngdy ban hdnh :
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NHA U&Y
\\1 h5n dich Bari sulfat:
\\ A*
dung dich keo Na CMC: NgAm Na CMC trong 10 lit nu6c RO dun n6
g nhiet dO 70"C, d0 y6n trong 12h, khu6y trQn d6u tpo thanh dung dfch keo.
- PhOi hogp durrg dich keo v6i Bari sulfat, khu6y dAu tpo hdn hqp d6ng nh6t.
- Thdm saccarln, nipagin, nipasol, vanili khudy dAu.
- Th0m nudc vla dri theo c6ng thrlc, khu6y dAu.
- D6 y6n h6n dfch trong 20 ph:frt.
- Lgc h6n dlch qua 4 lorp v6i mdn.
- Dem dich tgo thenh qua m6y d6ng ntrAt.
* Ki6m nghiQm bin thinh ph6m:
- Theo ti6u chuAn, dpt ti6u chu6n chuy6n sang giai do?n tiQt khuAn
* TiQt khu6n:
- Tiet khuan o nhiQt do 100"c, thli gian 30 phrit.
- Khi nhiet d0 h5n dlch gi6m xu6ng 60oC ti6n hanh d6ng vdo rfil chai/ lq.
*
@ D6ng lg/ chai:
- Xt li 19, nEp:
+ Rria chai: Chai nhua, dugc rua bing nudc RO, dC 16o nudc, s6y bing gi6, hoflc
nhiQt dQ th6p (duti 40"C).
+ Nip nhga: Rua bdng nu6c RO, di5 16o nu6c, s6y bing gi6, ho{c nhiQt dq thdp
(du6i 40"C).
- D6ng chai, xi6t n8p hoan chinh sin ph6m chuy6n sang d6ng thung carton.
* D6ng g6i:
- D6ng thirng carton hoan chinh san phdm.
* Ki6m nghiQm thinh phAm:
- Ki6m nghiQm thAnh phAm theo ti6u chuAn thenh ph6m, clpt ti6u chuAn, chuy6n
sang nhfp kho.
* Nh$p kho