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Materials & Design 227 (2023) 111734

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Materials & Design


journal homepage: www.elsevier.com/locate/matdes

Flexural properties of 3D printed graded lattice reinforced cementitious


composites using digital image correlation
Can Tang a,b, Junwei Liu b, Wenfeng Hao c,⇑, Yuanyuan Wei c
a
College of Civil Science and Engineering, Yangzhou University, Yangzhou, Jiangsu 225127, China
b
Faculty of Civil Engineering and Mechanics, Jiangsu University, Zhenjiang, Jiangsu 212013, China
c
College of Mechanical Engineering, Yangzhou University, Yangzhou, Jiangsu 225127, China

h i g h l i g h t s g r a p h i c a l a b s t r a c t

 The failure behavior of 3D-printed


lattice-reinforced cement-based
materials is found to change from
brittle fracture to ductile failure.
 3D-printed PA6 lattice-reinforced
cementitious composite cannot
significantly improve the cracking
load of the cementitious matrix.
 3D-printed graded lattice is used to
strengthen the cement mortar, thus
realizing the multiple cracking of the
cementitious matrix.
 The preparation method of the
functionally graded lattice structure
uses fewer materials and can improve
the flexural bearing capacity and
ductility of the cementitious matrix.
 The weak interfacial adhesion
between the 3D-printed polymer and
cement-based materials is a problem
that must be solved in subsequent
research.

a r t i c l e i n f o a b s t r a c t

Article history: Three-dimensional (3D) printed polymer-reinforced cementitious composites are expected to be used to
Received 24 October 2022 improve the ductility of cement-based materials. However, research on the maximum flexural capacity
Revised 6 February 2023 and failure mode of lattice-reinforced cementitious composites remains insufficient. In this study, six
Accepted 11 February 2023
types of cells with different volume fractions are designed, and mainly undergo bending and tensile
Available online 13 February 2023
deformation. According to the load characteristics during a three-point bending test, five kinds of graded
lattice structures are designed. Moreover, a skin-lattice structure and uniform lattice structure are
Keywords:
designed, and plain cement mortar is set to comprehensively evaluate the bending mechanical properties
3D printing
Cement-based materials
of graded lattice-reinforced cementitious composites. The crack evolution and failure mode of these com-
Graded lattice reinforcement posites under three-point bending load are studied using digital image correlation (DIC). The results show
Digital image correlation (DIC) that compared with the uniform lattice, the graded lattice can improve the maximum bending capacity of
Flexural property cement-based materials, improve their cracking characteristics and failure modes during the bending
process, and enhance their toughness while reducing the amount of required material. Compared with

⇑ Corresponding author.
E-mail address: hwf@yzu.edu.cn (W. Hao).

https://doi.org/10.1016/j.matdes.2023.111734
0264-1275/Ó 2023 The Author(s). Published by Elsevier Ltd.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

the plain cement mortar specimen, the graded lattice-reinforced specimen with the largest bending peak
load is found to have a 175% increase in the bending peak load and a significant increase in the bending
bearing capacity.
Ó 2023 The Author(s). Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND
license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

1. Introduction Fiber-reinforced plastic (FRP) RC has been a popular research


direction in recent years. FRP bars are considered a new material
Because of their high compressive strength, cement-based that can solve the problem of reinforcement corrosion due to their
materials have become the most widely used building materials high tensile strength and corrosion resistance [10–12]. However,
in the field of civil engineering. However, cement-based materials the bond performance of FRP bars is low [13], and they can easily
have defects including low tensile strength, susceptibility to crack- experience sudden tensile fracture [14,15]. Moreover, the working
ing, and high brittleness [1,2]. These defects make it impossible to deflection is larger than that of RC members with the same rein-
use cement-based materials alone to resist tensile load in engi- forcement rate and the cracks are wider [16–18], which limits
neering. In engineering applications, steel bars with high plasticity the development of FRP bars.
and high tensile strength are combined with cement materials to To solve the problems of the brittleness, cracking, and poor ten-
make reinforced concrete (RC) structural members [3,4]. According sile properties of cement-based materials, many scholars have
to the calculated load of the building structure design, more steel devoted their attention to the field of three-dimensional (3D)
bars are arranged in the areas of the member with high tensile printing (additive manufacturing). Additive manufacturing has
and shear stress to resist the load and limit the generation and many advantages, such as a wide selection of materials, the high
extension of cracks. However, RC structures are characterized by utilization rate of materials, and customizability, and can be used
a fatal disadvantage, namely that the steel bars easily rust in corro- to manufacture complex parts [19–21]. The parts and components
sive environments. The corrosion of the reinforcement will lead to prepared by the existing additive manufacturing technology are
the increase of the reinforcement volume and the generation of almost isotropic, and metal parts and components can be directly
stress and cracks caused by internal expansion; this intensifies printed [22–23]. Polymer reinforcements prepared by 3D printing
the ability of corrosive substances to enter the concrete, which will can be deployed in a cement-based material to create a strain-
aggravate the corrosion of the reinforcement, thus causing a hardening (flexural) cementitious composite [24–26], which can
vicious cycle and ultimately leading to the failure of RC members significantly improve the inherent brittleness of the material. Far-
[5–9]. ina et al. [23] studied the mechanical properties of 3D-printed

Fig. 1. The elements of the unit cell.

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polymer/metal-reinforced cement mortar with different rough- [34] proposed a method by which to optimize the automatic distri-
nesses under three-point bending load. Nam et al. [26] studied bution of multi-TPMS lattice types by selecting lattice unit cells
the three-point bending mechanical properties of fiber-reinforced with maximum strain energy in combination with the lattice cell
cement mortar controlled by 3D printing with different spatial dis- database, and carried out numerical and experimental verification.
tribution types. Rosewitz et al. [27] studied the mechanical proper- Nazir et al. [35] studied the mechanical responses of four different
ties of a 3D bionic polymer building structure made of reinforced lattice structure cantilever beams composed of Schwarz-P,
cement mortar composites with different geometric structures Schwarz-D, Gyroid, and Octet-truss structural unit cells manufac-
under four-point bending load. Salazar et al. [25] studied the tured by Multi Jet Fusion 3D printing technology. These studies
mechanical properties of 3D-printed polymer lattice-reinforced demonstrate that it is feasible to use 3D printing technology to per-
ultra-high-performance cement-based materials under four-point form functional gradient forming on the lattice structure, and the
bending load, and successfully transformed the cement-based gradient lattice is characterized by a light weight and good
materials into ductile materials with strain-hardening behavior. mechanical properties. In addition, Xu et al. [29] studied the flexu-
Xu et al. [28] studied the mechanical properties of 3D-printed ral mechanical properties of cement-based materials reinforced by
polymer lattice-reinforced cement-based materials with different 3D-printed functional graded polymer octet lattice structures.
structures under four-point bending load, and prepared cement- Compared with that of a plain mortar, the flexural ductility of
based composites with flexural- or strain-hardening properties. the strengthened specimens was found to be significantly
This research shows that 3D-printed polymer reinforcements can improved. However, the developed cementitious composite could
improve the brittleness of cement-based materials, and can be not obtain multiple cracking and strain-hardening behaviors, and
used for the preparation of ductile cementitious composites. More- the maximum bending strength of the reinforced sample was not
over, the graded design and customized printing of polymer rein- improved as compared with the plain mortar. Therefore, the pre-
forcements can be carried out in combination with the sent work focuses on improving the brittleness, improving the
mechanical characteristics of bending members and the technical maximum flexural capacity, and obtaining the multiple cracking
advantages of 3D printing. On the premise of using fewer raw characteristics of cement-based materials under bending load.
materials, lattice-reinforced cementitious composites can demon- In this study, five kinds of cells based on the cubic unit cell were
strate better mechanical properties. Ejeh et al. [33] carried out designed. These five kinds of cells had different structural forms,
four-point bending tests and finite element simulations of 3D- deformation mechanisms (mainly tensile and bending deforma-
printed AlSi10Mg uniform, functionally graded, and hybridized lat- tion), and volume fractions. According to the stress and deforma-
ticed beams. They studied the bending performance of the relative tion characteristics of the three-point bending test, six kinds of
density gradation and hybridization of the lattice on prominent graded lattice structures were designed. The tests focused on the
sheet-based, triply-periodic, cellular minimal surfaces. Feng et al. differences between the mechanical properties of the plain cement

Table 1
The basic parameters of the graded lattice unit cells.

Number Type of cell structure Volume Dimension line volume of cell outsourcing(mm3) Relative density Constituent elements
I 407.91 1000 40.79 % 1+2+3+4+5

II 352.85 1000 35.29 % 2+3+4+5

III 297.79 1000 29.78 % 3+4+5

IV 242.74 1000 24.27 % 4+5

V 207.88 1000 20.79 % 1+2+4

VI 82.93 1000 8.29 % 4

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mortar group, the full-section uniform lattice-reinforced group, the 2. Experimental methods
single-layer uniform lattice-reinforced group, the graded lattice-
reinforced group, and the lattice-reinforced group with skin. The 2.1. Graded lattice design
strain, crack evolution, and failure mode of eleven kinds of cement
specimens under three-point bending load were analyzed using To facilitate the assembly of unit cells and control the volume
digital image correlation (DIC). fraction, the lattice was close to the structural form of the steel

Fig. 2. The schematic diagrams of the distributions of the unit cells with different relative densities in the multi-lattice with five different structural forms. Note: (1) ‘‘4”
represents the two bottom supports loaded in advance. (2) ‘‘s” represents the preset loading head (loading point).

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Fig. 3. Examples of PA6 printed products made by the MJF process.

Table 2
The mix proportion of cement mortar.

Cement Fly ash Sand(0.08 mm-0.63 mm) Water reducer Water


1.2 0.8 3 0.006 0.994

Note: The cement was ordinary Portland cement PO 32.5 produced by Jiangsu Helin Cement Co., ltd., and the sand was Chinese ISO standard sand produced by Xiamen Aisiou
Standard Sand Co., ltd. Moreover, the fly ash was Grade I fly ash produced by Gongyi Bairun Refractory Materials Co., ltd., and the water reducer was a high-efficiency water
reducer produced by the Shandong Laiyang Hongxiang Building Additive Factory. The water was tap water from Zhenjiang, China.

reinforcement cage. The lattice cells used in this research were all In the design of lattice cells, all elements shown in Fig. 1 were
designed based on the cubic unit cell (as shown in Fig. 1(4)). In used to assemble the unit cell with the largest volume fraction.
addition, previous studies [30,32] have shown that the cubic unit This type of cell is also called a BFVC cell [32], and its deformation
cell has a tensile deformation mechanism, while a body-centered mechanism is dominated by bending deformation. The diagonal
cubic (BCC) cell has a bending-dominant deformation mechanism. brace of the left and right opposite faces of unit cell I was removed
The detailed information of the six cells designed in this study with to obtain unit cell II, the diagonal brace of the front and rear oppo-
different structural forms is reported in Table 1, and the strut site faces of unit cell II was removed to obtain unit cell III, and the
diameter of all unit cells was 2 mm. The centerline size of each cell diagonal brace of the upper and lower opposite faces of unit cell III
was 10  10  10 mm3. was removed to obtain unit cell IV. Unit cell V was obtained by

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

the law of the decreasing volume fraction. The purpose of this was
to investigate the influence of the number of layers of graded lat-
tices on the bending performance of the specimens. On the basis
of single-layer graded lattice B-1, different cells were arranged
along the line between the loading point and the two bottom sup-
ports to form two-layer (B-2) and three-layer (B-3) graded lattice
structures along the preset shear interface. The purpose of this
was to study the influence of the number of layers in the graded
lattice on the shear resistance of the specimen. The volume fraction
distributions of the five graded lattices assembled by six different
cells are shown in Fig. 2(f) and (j).
A uniform lattice composed of single cells with the smallest vol-
ume fraction was also set as a control group for comparison with
the graded lattice-reinforced group. This included lattice A-1 with
uniform cells arranged in the whole section and lattice A-2 with
uniform cells arranged in the bottom tensile zone. Skins of 2 and
4 mm, respectively, were added to the bottom of lattice A-2 to form
a lattice structure with skin. In the design, the stress in the middle
Fig. 4. The cement specimens formed and cured for 28 d (partial). of the span may have been too large, so unit cell V with a larger
volume fraction was used to replace the four unit cells VI. To facil-
itate a comparative analysis, lattice A-3 was set as the transition
group. The plain cement mortar group without a lattice was set
removing the internal BCC cell of unit cell I and the diagonal brace when casting the cement-based specimen, which was also used
of the upper and lower opposite planes. for comparison. The structural diagrams of the uniform lattice
Computer-Aided Design (CAD) software was used to establish and the lattice with skin composed of a single cell are shown in
3D standard models of different structural forms of unit cells. Fig. 2(a)-(e).
The volume fraction distribution diagram was designed according
to the bending moment distribution characteristics of three-point
bending, and the graded lattice structure was formed by assem- 2.2. Preparation of lattice and cement specimens
bling cells in CAD. The single-layer graded lattice starts from the
middle of the span to arrange cell I with the largest volume frac- The lattice samples used in this study were prepared by multi
tion, and a pair of cells with a smaller volume fraction was then jet fusion (MJF) technology. MJF is a 3D printing technology in
arranged on both sides. Considering the large concentrated force which powder materials are used as the main molding materials,
at the two bottom supports, cell IV with a relatively small volume onto which flux and refiner are sprayed, and energy is applied in
fraction was not arranged at the two bottom supports, but cell II the molding area to melt the powder to achieve molding [30,31].
was adopted. Finally, cell VI (which only played a structural and MJF printing technology has the advantages of high product qual-
positioning role in the specimen) was arranged in the stress-free ity, high dimensional accuracy, and a fast molding speed. The parts
zone at the edges of both sides to form graded lattice B-1. On the manufactured by MJF technology are almost isotropic, and their
basis of the single-layer graded lattice B-1, two-layer graded lattice mechanical properties are almost unaffected by the construction
B-4 and three-layer graded lattice B-5 were designed according to direction.

Fig. 5. The diagrams of the loading and monitoring schemes.

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The raw material used for 3D printing technology in this study


was PA6, and Fig. 3 presents the lattice structure printed with PA6
as the molding material.
The mix proportion of cement mortar during the casting of
lattice-reinforced cementitious composite materials is reported in
Table 2.
The lattice-reinforced cementitious composite specimens were
cast according to the steps of weighing, sampling, feeding and mix-
ing, grouting, vibrating and compacting, and molding. They were
demolded 24 h after molding and placed in a standard curing
box for 28 d. Fig. 4 presents the specimens cured for 28 d under
standard curing conditions.

2.3. Experimental device and scheme

The experimental setup is shown in Figs. 5 and 6. A TH-8201S


Fig. 6. The test loading and DIC acquisition system. universal tester with a load capacity of 10 kN was used to carry
out three-point bending loading on the lattice-reinforced cement

Fig. 7. The force–displacement curves of all cement samples.

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Fig. 7 (continued)

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3.1. Force-displacement curve analysis

Fig. 7 presents the force–displacement curves of the three-point


bending tests (black, blue, and red solid lines) of the specimens in
groups A, B, and C (the control group, i.e., the unreinforced plain
cement mortar group). Regarding group C, when the maximum
tensile stress in the mid-span reached the tensile strength of the
cementitious matrix, an abrupt brittle fracture occurred, the spec-
imen split into two parts, and the specimen failed and could not
continue to carry the load. The lattice-reinforced group showed a
ductile response as compared with the plain cement mortar group,
which occurred in the later loading period; the deflection change in
the middle of the span was larger, while the load change was
smaller.
The cracking bending moments of all the reinforced specimens
were approximately the same, namely about 1500 N, which was
generally consistent with the fracture load of the plain cement
mortar specimens. This shows that the addition of the lattice did
not significantly change the cracking load of the cement-based
materials; instead of the cementitious matrix, the lattice bore the
tensile load after reaching the cracking load.
For the specimens in group A (A-1 and A-2) composed of uni-
Fig. 7 (continued) form lattices, the load dropped sharply after reaching the first peak
(cracking load), then rose again to reach the peak, and then gradu-
ally declined. It can be seen from the comparative analysis that the
uniform lattice in specimens A-1 and A-2 was arranged with a
specimens at a loading rate of 0.1 mm/min, thus simulating quasi- cubic unit cell in the middle of the span, while the graded lattice
static loading. in the specimens in group B was arranged with a BFVC unit cell
DIC was used to monitor the full-field deformation of the spec- in the middle of the span at the bottom layer. The deformation
imens, and the 2D-DIC system of the CSI Company (United States) mechanism of the cubic unit cell under bending load was mainly
was used to calculate the images of the whole loading process. The tensile deformation, while that of the BFVC unit cell was mainly
whole image acquisition system was supported by Weishi Digital bending deformation. Because the volume fraction and stiffness
Image Technology Co., ltd. The hardware equipment consisted of of the BFVC unit cell were larger than those of the cubic cell, the
an MV-EM510M/C CCD camera, a BT-23120 telecentric lens, a light deformation in tension was smaller. When the cracking bending
source, and a bracket. The CCD camera had 5 million pixels with a moment was reached, the cementitious matrix stopped working,
resolution of 2456  2058 pixels. The magnification of the telecen- and the load was borne by the internal lattice at the moment.
tric lens was 0.072. The image acquisition rate was set as 15 When the difference of the cracking bending moment was not
frames/second. large, the deformation of the BFVC unit cell dominated by bending
deformation was much smaller than that of the cubic unit cell
dominated by tensile deformation, so the load of the specimen
containing the BFVC unit cell had no sudden change.
3. Analysis of the experimental results
The maximum load-bearing values of all specimens are listed in
Table 3 in the order of greatest to least (see Fig. 8 for a more intu-
Three-point bending tests were carried out on the 3D-printed
itive presentation of the relationship of the peak bending load).
lattice-reinforced cement mortar specimens. There were three
It can be seen from the average values of the peak load reported
groups of specimens with 10 different volume fractions of graded
in Table 3 that the peak load of all lattice-reinforced groups was
lattice/lattice with skin-reinforced cement-based materials, and
higher than that of the plain cement mortar control group, and
there were three groups of plain cement mortar specimens without
the peak load of the full-section uniform lattice-reinforced group
a lattice as the control group. A total of 35 results were measured.
(group A-1) was higher than that of the single-layer uniform
For the control group and 10 types of lattice-reinforced specimens,
lattice-reinforced group (group A-2). The average peak loads of
the largest of the three groups in terms of the peak load was
lattice-reinforced groups B-3 and B-5 were approximately the
selected to analyze the strain evolution characteristics, as pre-
same. Moreover, the average peak loads of lattice groups B-1, B-
sented in Section 3.2.

Table 3
The peak load of the lattice-reinforced and plain cement mortar specimens.

Type A-1 A-2 A-3 A-4 A-5 C B-1 B-2 B-3 B-4 B-5
Peak load I (N) 1899.078 1565.063 1544.175 2999.266 4287.389 1705.848 3374.566 3205.421 3658.783 3444.547 3748.769
Peak load II (N) 1796.853 1541.430 1444.618 2882.174 3319.355 1170.640 3055.596 3151.642 3502.367 3090.095 3703.128
Peak load III (N)  1401.842 1382.032 2806.781 2802.918 1076.025 s 2980.241 s 3025.803 3404.771
Average (N) 1847.97 1502.78 1456.94 2896.07 3469.89 1317.50 3215.08 3112.43 3580.58 3186.82 3618.89

Note: (1) ‘‘s” indicates that data interruption was not recorded completely during loading. (2) ‘‘” indicates that the data was lost during the test.

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Fig. 8. The peak bending strength of the lattice-reinforced and plain cement mortar specimens.

Fig. 9. The evolution of the horizontal strain field (exx) of the specimens in group C.

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Fig. 10. The evolution of the horizontal strain field (exx) of the specimens in group B-1.

2, and B-4 were approximately the same, but much of them were near the mid-span of these two specimens under bending load. The
lower than those of lattice-reinforced groups B-3 and B-5. The strain concentration region then evolved into a crack that extended
specific failure mechanism is explained in Section 3.2. from the bottom to the loading point during continuous loading,
forming a main vertical crack. After the crack was formed, the
cementitious matrix exited the work, the internal lattice bore the
3.2. Analysis of the DIC-monitored strain field
stress, and the specimen finally failed due to the damage of the
internal lattice. By comparing the specimens in group C with those
The strain field at the corresponding time during loading was
in group A-1, it can be seen that the lattice used as the reinforce-
obtained using VIC-2D software to process the acquired images.
ment changed the brittle fracture failure of the plain cement mor-
The transverse expansion of the cement specimens under vertical
tar under bending load into ductile failure with certain toughness.
load exhibited positive strain. The transverse strain of the speci-
The comparison between the specimens in groups A-1 and A-2
men during bending was selected for analysis, and the correspond-
shows that the arrangement of a layer or a full-section lattice com-
ing strain evolution and crack formation processes are shown in
posed of a single cubic unit cell at the bottom of the tensile zone
Figs. 9-19.
had no significant effect on improving the failure mode of the
Consider the plain cement mortar specimen (group C, as shown
cement-based materials. This is mainly due to the low volume frac-
in Fig. 9), which experienced sudden brittle fracture under bending
tion and stiffness of the cubic lattice, and the relatively low stiff-
load. Before fracture, there was no obvious strain concentration
ness after cracking. Therefore, a uniform lattice layout in the full
area at the bottom of the mid-span, and there was no obvious crack
section is not the best way to strengthen cement-based materials,
formation. By comparing the full-section uniform lattice-
as it may lead to unnecessary material waste. According to the
reinforced specimens (group A-1, as shown in Fig. 15) with the bot-
bending stress distribution characteristics of cement-based mate-
tom uniform lattice-reinforced specimens (group A-2, as shown in
rials, graded design was carried out for the lattice structure. The
Fig. 16), it can be seen that a strain concentration area was formed

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Fig. 11. The evolution of the horizontal strain field (exx) of the specimens in group B-2.

customized advantage of 3D printing can perfectly solve this nated by bending deformation); this had a strong ability to limit
problem. crack extension and crack width expansion (as shown in Fig. 10
The strain evolution laws of the specimens in group B-1 (as (c) and 11(c), in which dark areas representing large strain
shown in Fig. 10) and group B-2 (as shown in Fig. 11) were similar. appeared in the middle layer). The maximum tensile strain in the
At the initial loading stage, the strain distribution in the whole middle layer of the span evolved into a main vertical crack during
region had no obvious rule. In the subsequent analysis, the area continuous loading, which also shows that the effect of limiting
with a short distance on the left and right sides of the central axis cracks in the middle layer without a lattice was poor. With the
of the specimens was approximately treated as a pure bending sec- increase of the load, many regions with large strain were formed
tion. With the increase of the load, strain concentration occurred in near the vertical crack in the abdomen of the specimen. These
the mid-span area of the specimens, which was consistent with the strain concentration areas gradually evolved into secondary cracks
maximum bending moment in the mid-span area under three- in the subsequent loading and extended to the loading point and
point bending load. The maximum bending moment at the bottom the bottom support, which was accompanied by the expansion of
of the mid-span means that the tensile stress was also the maxi- the crack width. During the evolution process, the small fractures
mum, so the maximum tensile strain occurred. When the maxi- connected with each other and extended, and, finally, main diago-
mum tensile stress exceeds the maximum tensile strength of the nal cracks were formed on both sides of the main vertical crack.
cementitious matrix, micro-cracks will occur. The maximum ten- The evolution process of diagonal cracks shows that the specimens
sile strain did not occur at the bottom of the mid-span because experienced shear failure. This proves that the single-layer graded
the specimens were preloaded with a single-layer graded lattice lattice used in this study can change the failure mode of cement
at the bottom. The lattice was arranged with BFVC unit cells in mortar under three-point bending load from flexural tensile failure
the mid-span (the deformation mechanism of which was domi- to flexural shear failure. During the loading of the specimen, when

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Fig. 12. The evolution of the horizontal strain field (exx) of the specimens in group B-3.

the main diagonal cracks formed, a large number of diagonal structures, the lattice and the cementitious matrix were debonded.
micro-cracks appeared on the surface of the bottom lattice of the The crack width of the debonded specimen interface caused by
specimen, and some cracks continued to extend to the loading continuous loading increased while the load on the specimen con-
point during the subsequent loading. The comparison of the crack tinued to increase. This is because the position of the neutral axis
evolution processes of the specimens in groups B-1 and B-2 with moved up and the maximum tensile strain increased with the
that of the specimens in group C shows that the graded lattice- interface cracking and the debonding of the lattice structure. In
reinforced cement mortar used in this study can achieve multiple the graded lattice specimens of group B, the failure of groups B-
cracking behaviors under bending load. 1, B-2, B-4, and B-5 was caused by the debonding failure of the
At the later stage of loading of the specimens in groups B-1 and cementitious matrix and lattice edges (as shown in Fig. 10(i), 11
B-2, in the area where the diagonal crack intersected the top lattice (i), 13(i), and 14(i)). No cement mortar crushing occurred in the
strut, the diagonal crack began to extend and expand to both sides compression area or tensile fracture of the lattice strut in the ten-
along the interface between the lattice structure and the cementi- sion area, which experienced local shear failure. According to the
tious matrix. This was due to the sudden change of the stiffness at strain evolution analysis of the specimens in groups B-1 and B-5,
the interface between the cementitious matrix and the lattice, with the increase of the number of layers of graded lattice, the time
resulting in the disharmony of the deformation in this area and taken for cementitious matrix and lattice debonding increased (i.e.,
the stress concentration. Simultaneously, under the three-point the maximum load during debonding increased). This is because as
bending load, the left and right spans were bending shear sections, the number of lattice layers increased, the interface between the
which were subjected to shear forces in the oblique direction. cementitious matrix and the lattice, which experienced a sudden
When the shear force generated on the inclined section exceeded change in stiffness, moved upward, and the bending moment at
the bonding strength between the cementitious matrix and lattice the corresponding height decreased (i.e., the shear stress at the

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Fig. 13. The evolution of the horizontal strain field (exx) of the specimens in group B-4.

interface decreased). This increased the time taken for the load at During the subsequent loading, the cement mortar in the gap
the interface to reach the bonding strength of the cementitious was completely debonded due to the extrusion of the lattices on
matrix and the lattice structure. both sides, thus forming a columnar cement block (as shown in
The lattice in the specimens in group B-3 included one addi- Fig. 20(i)). In the later loading stage, the cementitious matrix in
tional layer as compared to that in the specimens in group B-2, the gap was compressed, and the lower single-layer lattice was
but there were gaps near the mid-span. By comparing the strain tensioned. Finally, the single-layer lattice failed with the tensile
and crack evolution of groups B-2 and B-3, it can be seen that there fracture of the single-layer lattice.
was no vertical crack in the mid-span of the specimens in group B- Groups B-4 and B-5 are respectively the two- and three-layer
3 under loading, but two cracks appeared in the mid-span abdom- graded lattice-reinforced groups without gaps in the mid-span.
inal area (the cracks occurred roughly along the interface between During the loading of the two lattice-reinforced groups, there were
the lattice and the cementitious matrix) and extended to the load- no penetrating vertical cracks in the mid-span area, but there were
ing point. This may be because the cementitious matrix near the many diagonal cracks in the left and right bending shear sections.
mid-span bore similar tensile forces, whereas at the interface These diagonal cracks were formed in the area with a large strain
between the cementitious matrix and the lattice, the shear bearing at the bottom of the specimens (the tensile stress in these areas
capacity was much less than the tensile load capacity. At the inter- exceeded the maximum tensile strength of the cement mortar,
face between the cementitious matrix and the lattice, the bond resulting in micro-cracks) and extended to the loading point.
strength was lower than the tensile strength of the cementitious Among these cracks, only two continuously penetrated and
matrix, and the shear resistance was weak. Shear failure occurred extended, and two main diagonal cracks were finally formed. After
before tensile cracks occurred. Another reason may be that the ten- that, the evolution processes of these two main cracks were similar
sile stress near the mid-span was large, which directly led to the to those of the cracks in the specimens in groups B-1, B-2, and B-3
debonding of the cementitious matrix and the lattice structure. in the later loading period, which extended along the interface

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 14. The evolution of the horizontal strain field (exx) of the specimens in group B-5.

between the cementitious matrix and the lattice to both sides. The the specimens in group A-3. At the initial stage of loading, the spec-
final mode of failure for both types of lattice-reinforced specimens imens in group A-4 had vertically distributed strain concentration
was a reduction in the load-bearing capacity due to the debonding areas in the mid-span. With the increase of the load, the strain
of the cementitious matrix from the lattice, and no cement mortar exceeded the maximum tensile strain of the cementitious matrix,
crushing or lattice breaking occurred. Based on the deformation cracks were generated and extended to the loading point, and
capacities of the specimens in groups B-4 and B-5 under load, the crack width was enlarged. At this time, the mid-span crack
the two lattice-reinforced groups had greater resistance to bending divided the specimen into two parts, which were connected by
deformation. This is reflected in the fact that compared with the the bottom skin. During subsequent loading, several micro-cracks
bending process of the specimens in groups B-1, B-2, and B-3, initiated from the bottom of the specimen. These micro-cracks
the specimens in groups B-4 and B-5 formed more cracks, but these emerged and continued to extend toward the loading point, form-
cracks did not penetrate each other to form larger cracks. From the ing one diagonal crack with the greatest width and length in each
process of strain and crack evolution, it can be seen that the lattice of the multiple diagonal cracks in the left and right bending shear
had the effect of limiting crack propagation and aggregation. sections. In the early stage, the specimen was divided into two
Compared with the specimens in group A-2, those in group A-3 parts by vertical cracks in the mid-span, and two diagonal cracks
were arranged with four unit cells (cell V) with diagonal bracing divided the specimen into four parts; this resulted in the shear fail-
added outside in the mid-span area. Although the added support ure of the inclined section of the specimen. The vertical and obli-
was limited, the strain evolution performance was similar to that que cracks caused the specimen to form a ‘‘comb” structure, and
of the graded lattice in the specimens in group B. the bottom was connected by the skin. This phenomenon is similar
The specimens in groups A-4 and A-5 respectively included the to the failure mode of beams without stirrups under bending load.
addition of 2- and 4-mm skins (i.e., the base plate) on the lattice of The failure pattern of the specimens in group A-5 was similar to

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 15. The evolution of the horizontal strain field (exx) of the specimens in group A-1.

those in group A-4 during the entire loading process, but no verti- The failure mode of the single-layer lattice specimens with skin
cal cracks appeared in the mid-span. Compared with that of the (groups A-4 and B-5) under bending load was mainly characterized
specimens in group A-4, the skin of the specimens in group A-5 by the tensile fracture failure of the skin (as shown in Fig. 20(e)
was thicker, and its maximum bending bearing capacity was also and (f)). During the loading process, vertical cracks first appeared
increased. Therefore, there were more diagonal cracks during the in the mid-span, and micro-cracks then appeared from the bottom
loading process, and the bottom skin also ultimately failed due to of the bending shear area. With the increase of the load, the micro-
the tensile fracture. cracks continued to expand and the width increased. Some micro-
cracks penetrated and gathered, thus forming a main diagonal
crack with the greatest width and length among multiple diagonal
4. Discussion and summary cracks, which led to the failure of the inclined section of the spec-
imen. With the penetration of the diagonal cracks, the specimen
The bending tensile fracture damage of the cementitious matrix was divided into a ‘‘comb” structure by the vertical cracks in the
occurred in the plain cement mortar specimen (C). The specimens mid-span or the diagonal cracks on the left and right sides. At this
with uniform lattices arranged in the full section and single-layer time, the tensile load generated by the bending moment was com-
lattices arranged in the bottom layer (groups A-1, A-2, and A-3) pletely borne by the skin at the bottom until it was pulled to fail-
suffered ductile failure. After the tensile cementitious matrix ure. The maximum flexural capacity of the single-layer lattice-
cracked, the load was borne by the internal lattice strut, and the reinforced cement-based specimens with skin was determined by
lattice finally failed after being broken. the tensile strength of the underlying skin.

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 16. The evolution of the horizontal strain field (exx) of the specimens in group A-2.

The failure mode of the graded lattice specimens (groups B-1, B- and the lattice bore the tensile load. As the load continued to
2, B-3, B-4, and B-5) under bending load was mainly characterized increase, diagonal cracks appeared in the bending shear areas on
by damage due to the debonding of the lattice from the cementi- both sides and extended to the loading point. With the gathering
tious matrix (as shown in Fig. 20(g), (h), (k)), and damage due to and penetration of diagonal cracks, a main diagonal crack was
the tensile fracture of the lattice at the bottom of the specimen formed, and most of the cementitious matrix at the bottom of
without debonding (as shown in Fig. 11(i)). There was also a case the specimen was subjected to multiple cracks and withdrew from
in which the debonding damage of the lattice from the cementi- the work. With the further increase of the load, the stress of the
tious matrix occurred first, followed by the tensile fracture damage specimen was redistributed continuously, and the stress of the lat-
of the bottom lattice (as shown in Fig. 11(j)). At the initial stage of tice strut was gradually increased. The tensile stress on the normal
loading, the load was very small, and there was no crack on the section was borne by the horizontal or diagonal strut of the lattice
surface of the specimen. At this time, the stress was less than the at the bottom, and the shear stress on the inclined section was
compressive strength of the cementitious matrix, which was borne by the vertical or diagonal strut of the lattice. This also sug-
shared by the cementitious matrix and the lattice. With the gests that the use of a lattice in the cementitious matrix can either
increase of the load, when the maximum tensile stress at the max- improve the overall toughness of the specimen, limit the formation
imum bending moment (near the mid-span) exceeded the tensile and extension of diagonal cracks and improve the aggregate bite
strength of the cementitious matrix, vertical cracks occurred. At between cracks, or transform a single crack under cement mortar
this time, stress redistribution occurred in the specimen, the bending into dispersed multiple cracks to display multiple cracking
cementitious matrix near the mid-span withdrew from the work, behaviors.

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 17. The evolution of the horizontal strain field (exx) of the specimens in group A-3.

In combination with the strain evolution and crack analysis pre- to monitor the formation process of strain concentration areas
sented in Section 4.2, the plain cement mortar specimen suffered and their evaluation into cracks under load. Moreover, it can be
from brittle failure. There was no strain concentration during the identified via the increase in the number of cracks on the surface
whole loading process, and the specimen finally failed due to a sin- of the specimen, the crack extension, and the crack width
gle crack (as shown in Fig. 20(a)). The failure mode of the plain expansion.
cement mortar specimen under bending was characterized by sud- In this study, because most of the specimens in group B did not
denness and low ductility, and there was no warning of impending undergo the tensile failure of the lattice, but instead underwent the
failure. The specimen reinforced by the uniform lattice composed debonding failure of the lattice and the cementitious matrix, it was
of low-volume-fraction cells in the full section or bottom layer impossible to quantitatively analyze the relationship between the
was subjected to ductile failure, and its strain evolution and strain volume fraction of the graded lattice and the bending capacity. A
concentration distribution in the whole process of loading were qualitative analysis was carried out on the lattices with similar vol-
monitored via DIC technology. The bending failure of this type of ume fractions, as well as their bending bearing capacities and
lattice-reinforced specimen first occurred during the tensile frac- cracking characteristics, in combination with Table 4. The volume
ture of the cementitious matrix, and then during the layer-by- of the specimens in group A-1 with uniform lattices arranged in
layer tensile fracture of the lattice strut, which had certain ductil- the full section was larger than those of the specimens in group
ity. The ductile failure of the lattice with skin and the graded A-4 with lattices with skin and those in group B-1 with single-
lattice-reinforced specimens can be identified by DIC technology layer graded lattices. Additionally, the maximum bending bearing

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 18. The evolution of the horizontal strain field (exx) of the specimens in group A-4.

capacity of the specimens in group A-1 was far less than those of The mechanical properties of the 3D-printed graded lattice-
the specimens in groups A-4 and B-1. Moreover, the lattice with reinforced cementitious composites under three-point bending
skin represented by group A-4 and the graded lattice represented load were studied using DIC. Some important conclusions are listed
by group B-1 achieved multiple cracking behaviors. This demon- as follows.
strates that the graded lattice structure designed based on the
loading characteristics can reduce the amount of materials used (1) In terms of the maximum bending bearing capacity, the lay-
and effectively improve the maximum bending bearing capacity out of the uniform lattice with a low volume fraction of unit
and cracking characteristics of cementitious composites. cells in the whole section and the single-layer lattice in the
tensile zone did not significantly improve the maximum
bending bearing capacity of cement-based materials. All
5. Conclusion the lattices did not increase the cracking load of the
cement-based materials.
In this paper, 10 kinds of lattice structures were printed using (2) A customized graded lattice and a lattice with skin can sig-
MJF technology. According to the stress distribution characteristics nificantly improve the maximum flexural capacity of
of three-point bending, the graded lattices were designed and cement-based materials, and can also improve the cracking
strengthened in specific areas to study the advantages of 3D- characteristics and failure mode. The failure modes of the
printed graded lattice as compared with a single uniform lattice- cementitious composites reinforced with a 3D-printed
reinforced cement mortar in terms of the bearing capacity, crack- graded lattice and a lattice with skin respectively changed
ing characteristics, failure mode, and other flexural properties. from the brittle fracture failure of a single crack to the duc-

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C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 19. The evolution of the horizontal strain field (exx) of the specimens in group A-5.

tile failure of multiple cracks, and from the tensile failure of has the excellent effect of limiting cracking and preventing
the plain cementitious matrix to the flexural shear failure of crack propagation. The dowel action of the lattice improves
the lattice and cementitious matrix. the overall flexural performance of cement-based materials.
(3) The experimental analysis demonstrated that the deforma-
tion mechanism of the lattice-reinforced cement-based For graded lattices, the lattice structure can be strengthened at
material specimens with skin was similar to that of beams specific locations according to the customized characteristics of 3D
without stirrups in concrete structures. The deformation printing, thus allowing for the achievement of local reinforcement
mechanism of the graded lattice-reinforced cement-based at the vulnerable parts of cement-based materials and the parts
material specimen was similar to that of beams with stirrups with a large preset load; ultimately, the amount of materials can
in concrete structures. be reduced and the performance can be improved. The lattice with
(4) The lattice in the specimen can change the stress transfer skin has the potential to be applied in formwork engineering in
path, which can then affect the distribution of stress and civil engineering construction. It can be considered a permanent
strain. The presence of a lattice in cement-based materials formwork to replace concrete and coordinate the reinforcement

20
C. Tang, J. Liu, W. Hao et al. Materials & Design 227 (2023) 111734

Fig. 20. The failure modes of the cement specimens.

Table 4
The volumes of various lattice structures.

Type A-1 A-2 A-3 A-4 A-5 B-1 B-2 B-3 B-4 B-5
Volume/mm3 23783.6 8467.5 10407.9 17376.3 27744.3 22920.8 28155.6 31011.5 32608.1 36548.6

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