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Construction and Building Materials 333 (2022) 127418

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Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Study on flexural properties of 3D printed lattice-reinforced concrete


structures using acoustic emission and digital image correlation
Junwei Liu a, Humaira Kanwal a, Can Tang a, Wenfeng Hao b, *
a
Faculty of Civil Engineering and Mechanics, Jiangsu University, Zhenjiang, Jiangsu 212013, China
b
College of Mechanical Engineering, Yangzhou University, Yangzhou, Jiangsu 225127, China

A R T I C L E I N F O A B S T R A C T

Keywords: Lattice-reinforced concrete is considered to be a new method to improve the quasi-brittleness, ductility and
3D printing fracture toughness of concrete. 3D printing technology provides the possibility for lattice molding with complex
Lattice reinforcement concrete structures structures. Therefore, 3D printed lattice-reinforced concrete structures have aroused great interest. However,
Digital image correlation
there are relatively few studies on the mechanical properties of 3D printed lattice-reinforced concrete, and the
Acoustic emission
Three-point bending
effects of lattices with different structures are not considered. In this paper, the three-point bending properties of
Unit cell 3D printed lattice-reinforced concrete with different reinforced structures are tested. Five different structures of
lattices with identical volume reinforced ratio are designed and printed by selective laser sintering (SLS). The 3D
printed lattice-reinforced concrete structures are prepared, and the plain concrete without lattice is set as the
control groups. Acoustic emission (AE) and digital image correlation (DIC) technologies are combined to monitor
the specimens from the surface to inside, and the differences in mechanical properties between the control
specimen and lattice reinforcement specimens with different structures were compared. The test results show
that the lattice can significantly improve the mechanical properties of concrete, and the rhombicuboctahedron
(RO) lattice can significantly improve the maximal bearing capacity of concrete specimens under three-point
bending. This test further demonstrates the feasibility of 3D printed lattice-reinforced concrete structures, pro­
vides a new method to improve the quasi-brittleness and ductility of concrete.

1. Introduction straw fiber [9,10]) and mineral fiber (such as glass fiber [11,12], carbon
fiber [13,14]) into concrete and achieved success. These fibers have
Concrete is one of the most widely used building materials in the more or less deficiencies in high cost, poor durability, poor construct­
world [1,2]. Because of its high compressive strength, concrete structure ability, low rupture strength, large density difference and poor mixing
has become the most important structural form in building structure. performance, which limits the development of fiber-reinforced concrete
However, concrete has the characteristics of low tensile strength [2], to a certain extent. At the same time, the fiber is easy to agglomerate
and the brittleness will increase with the increase of compressive when casting concrete, and the cement slurry is difficult to fully wrap
strength, which makes concrete not used as a material to bear tensile and fill, and its distribution difficult to control [15,16], resulting in the
load in practical engineering application. In addition, factors such as formation and development of cracks difficult to control, so it can not
temperature stress [3,4], shrinkage [5,6] and external force (such as achieve the expected performance.
earthquake, explosion load, etc.) may make the internal stress of con­ Textile reinforced concrete uses two-dimensional mesh cloth as
crete exceed the ultimate tensile strength and produce cracks. The for­ reinforcement material, as a two-dimensional directional reinforcement
mation of cracks will pose a great challenge to the durability of concrete method, it has higher reinforcement efficiency than two-dimensional or
structures. Therefore, improving the ductility of concrete and limiting three-dimensional random reinforcement formed by one-dimensional
the development of concrete cracks are the research hotspots in recent short fibers. However, it is only strengthened in two dimensions,
years. which often leads to bond failure and insufficient overall performance.
In order to improve the ductility of concrete, people have tried to mix Textile reinforced concrete has limited application in engineering
metal fiber (such as steel fiber [7,8]), plant fiber (such as jute fiber and practice and is mainly used for structural reinforcement [17,18] and

* Corresponding author.
E-mail address: hwf@yzu.edu.cn (W. Hao).

https://doi.org/10.1016/j.conbuildmat.2022.127418
Received 13 February 2022; Received in revised form 27 March 2022; Accepted 5 April 2022
Available online 11 April 2022
0950-0618/© 2022 Elsevier Ltd. All rights reserved.
J. Liu et al. Construction and Building Materials 333 (2022) 127418

lightweight sandwich panels [19,20]. Three dimensional fiber spacer is necessary to monitor the whole field deformation and the entire
textile reinforced concrete can carry out three-dimensional spatial process of damage. The inherent damage has a greater impact on the
orientation distribution, further improve the reinforcement ratio, and mechanical properties of concrete, so the non-destructive testing
play a revolutionary role in promoting fiber reinforced concrete. method is the most suitable method for detecting cracks and other de­
When the traditional reinforced concrete structure is in a corrosive fects in concrete structures. Digital image correlation (DIC) and acoustic
environment, the protective coating concrete is easy to crack and spall, emission (AE) technology are two relatively conventional non-
and the steel bar is easy to rust, resulting in a sharp decline in the destructive testing methods. AE technology has the advantages of real-
durability of the reinforced concrete structure, damaging the integrity of time monitoring and no external energy supply [34]. DIC technology
the structure and reducing the service life of the structure. As a new type has the advantages of full field measurement and high measurement
of composite reinforcement, FRP bar is considered to be an ideal sub­ accuracy. These advantages make them especially suitable for dynamic
stitute for steel bar in corrosive environment [21,22]. However, the safety detection and monitoring of concrete structures. At present, AE
brittle failure characteristics of FRP bar concrete members and the de­ and DIC technologies have been widely used in the monitoring of
fects of excessive crack width and deflection under normal use limit its damage, deformation and cracks of concrete structures. Domenico et al.
application [23,24]. 3D printing [25] (additive manufacturing) is an [35] used DIC technology to study the interface behavior between the
emerging technology developed in recent years. It has the characteristics externally bonded fabric-reinforced cement mortar (FRCM) board and
of personalized manufacturing, fast printing speed, and can print com­ the concrete matrix, and realized the local interpretation of the evolu­
plex structures [26–28]. The printing technology can accurately control tion of the strain distribution of FRCM concrete interface obtained by
the distribution of fibers in concrete. DIC before and after cracking. Aghlara et al. [36] used two-dimensional
3D printing technologies can be roughly divided into three categories digital image correlation (2D-DIC) technology to measure the steel­
according to different processes [48]. Powder bed fusion process is to –concrete bond strain on the concrete surface. The results show that the
fuse and melt the microscopic particles of powder to construct 3D ob­ displacement and strain measured by 2D-DIC technology is largely
jects. This process is used in printing technologies such as SLS, EBM, acceptable. Soulioti et al. [37] studied the influence of different contents
SLM, SHS and DMLS. Photopolymerization process is an AM technology of steel fibers in concrete slabs on fracture process and acoustic activity,
that customs a liquid polymer resin to create 3D objects. This method and described the AE behavior of concrete under four-point bending.
includes curing photopolymer resin with UV laser to create prototypes, Topolá et al. [38] analyzed the AE signals in the three-point bending
models and patterns. Stereolithography (SLA) technology often adopts fracture test of alkali slag mortar with different steel fiber content,
this process. Extrusion-Based systems is an extrusion-based method for identified the typical parameters of AE signals of different mixtures, and
prototyping, modelling and fabrication claims. Fused Deposition further described its behavior and failure development under stress. Dai
Modeling is the most widely utilized this process. In the future, whether et al. [39] used DIC and AE technology to obtain the displacement field
3D printed lattice can form a new structure type like FRP bars (partially on the surface of the specimen and the AE signal inside the specimen in
or completely replace steel bars, solve the problem of insufficient real time, and studied the characteristics of concrete fracture process
durability of reinforced concrete structures, and improve their me­ zone (FPZ). The experimental results show that the distribution of AE
chanical properties) is worthy of in-depth study. events is consistent with the distribution of FPZ determined by the
In recent years, scholars have conducted in-depth research on 3D sample surface deformation measured by DIC. Sutter et al. [40] evalu­
printing technology to prepare complex structure reinforcements ated and monitored the mechanical properties of hybrid beams made of
instead of traditional fibers to reinforce cement-based composites. fiber reinforced cement (TRC) hollow boxes using AE and DIC. Karaiskos
Farina et al. [29] used 3D printing technology to prepare polymers and et al. [41] introduced an experimental configuration using an integrated
metal steel-bars with different surface morphology and roughness to ultrasonic, acoustic (AE) and optical (DIC) monitoring system to detect
reinforce cement mortar, and explored the influence of different and locate the four-point bending fracture mode on a large concrete
roughness reinforcements on the cement mortar under the three-point beam and detect healing activation process and evaluate subsequent
bending test. Nam et al. [30] used 3D printing technology to control concrete repairs.
the position and orientation of fibers in concrete, and studied the me­ In this paper, lattices with five different structures are designed and
chanical properties of fiber-reinforced cement mortars with different printed using selective laser sintering technology. The 3D printed
spatial distribution types under a three-point bending test. Rosewitz lattice-reinforced concrete structures are prepared and standard curing
et al. [31] used 3D printed bionic polymer building structures as rein­ for 28 days. The three-point bending properties of 3D printed lattice-
forcement materials for cement mortar, and studied the mechanical reinforced concrete structures are tested. The damage inside the speci­
properties of cement-based composites reinforced by different geometric mens and the strain field on the outer surface are analyzed by AE and
structures. Salazar et al. [32] prepared a 3D printed polymer lattice DIC technology respectively during the loading process, so as to realize
reinforced ultra-high performance concrete (UHPC) specimens, and the synchronous monitoring of the inside and outside of the concrete
conducted a four-point bending test on the specimens. The results structures.
showed that the lattice was very successful in transforming brittle ultra-
high performance concrete into ductile material with strain hardening 2. Specimens preparation
behavior. Xu et al. [33] used 3D printing technology to prepare polymer-
reinforced lattices with different structures, which were cast into 2.1. Lattice design
cement-based materials to prepare specimens and then tested under
four-point bending. The results show that cement-based composites with In order to select different structures of unit cell to construct lattice
flexural hardening or strain hardening properties can be prepared by structures and compare the three-point bending properties of lattice-
reasonable design of polymer reinforced lattices. The research of the reinforced concrete, according to reference [42], this paper selects five
above scholars shows that compared with traditional fiber-reinforced types of unit cell structures: circular, octagonal, strengthened octagonal,
cement-based materials, the reinforcement prepared by 3D printing Rhombicuboctahedron (RO), cubic and uses computer aided design
technology has a significant effect on the improvement of the mechan­ software (CAD) establish a three-dimensional standard model.
ical properties of cement-based composites, and has great research sig­ The five different structural forms of unit cells have different cell
nificance and application prospects. edge deformation mechanisms [42] (such as bending, stretching and
Concrete is a non-homogeneous quasi-brittle material. During the flexion), aiming to consider the influence of the lattice structures with
failure process under loading, the formation of damage and cracks often different unit cells deformation mechanism on the bending mechanical
occur at an instant, and the difference before and after failure is large. It properties of lattice-reinforced concrete. The unit cell of “Circular”

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

lattice is constructed from three perpendicular crossed rings. Its a value. Therefore, the volume fraction of lattice structure is only deter­
structure dominated by bending deformation. The unit cell of “Octag­ mined by the strut diameter of unit cell. If the diameter of the column is
onal” lattice is constructed from three crossed octagons, which deform determined according to only one cell, when the lattice is assembled by
by bending and buckling of the cell edges under uniaxial compressive CAD modeling, the volume fraction of the final lattice will be affected
loading. The unit cell of “Strengthened Octagonal” lattice is constructed because the overlap between the edges and nodes of the unit cell
by “Octagonal” lattice unit cell by adding inclined struts in the interior. structure is removed [43]. Therefore, according to the CAD modeling,
Its vertical edges is deformed by buckling in the loading direction. The the relationship between the diameter variable and the volume of the
unit cell of “RO” lattice is constructed from rhombicuboctahedron cells, lattice is expressed as equation (1) by polynomial function.
which deformation mechanism is stretching-dominated. The unit cell of
V = f (d) = α0 + α1 d + α2 d2 + α3 d3 + ⋯ (1)
“Cubic” lattice is constructed from simple cube cells, which deform by
buckling of the vertical struts under uniaxial compressive loading. By changing the strut diameter of different unit cell, copying and
Table 1 shows the CAD model of the five cells, the connection mode assembling the lattice with CAD, and calculating the final volume, the
between the cells, and side view of the lattices constructed by unit cells. relationship between the diameter variable and the lattice volume is
For the outsourcing size of unit cell, we use reference [42]. The fitted to the cubic polynomial(in equations (2)–(6)).
centerline size of each cell is 10 × 10 × 10 mm3, and it is geometrically
symmetrical around the three vertical planes intersected by its center VCircular = f (d1 ) = 309.7d1 + 12645d12 − 1219.4d13 (2)
point. Each lattice structure is replicated by a unit cell in the x, y and z
directions, and is composed of 16 × 3 × 4 cells (Table 2). VOctagonal = f (d2 ) = 5 × 10 - 5 d2 + 12044d22 − 1017.6d23 (3)
In order to facilitate the later comparison and study the three-point
bending response of lattice-reinforced concrete structures, the volume VStrengthened Octagonal = f (d3 ) = 0.0002d3 + 21087d33 − 2712.7d33 (4)
of lattice is adjusted by changing the strut diameter of unit cell in design,
so as to ensure that the relative density of different lattices built in VRO = f (d4 ) = 4 × 10 - 5 d4 + 24087d42 − 3456.3d43 (5)
concrete structures is identical. The relative density is the ratio of the
apparent density of a cellular material to that of the parent solid material VCubic = f (d5 ) = 0.0001d5 + 6652.3d52 - 353.21d53 (6)
from which the cell edges are made, which is also equal to the volume For the selection of the thickness of the struts and member of the unit
fraction of solid in the cellular material [42]. cell, we first determine that the size of the lattice-reinforced concrete
The centerline size of lattice unit cell has been specified as a fixed specimen is 170 mm × 40 mm × 50 mm, and volume is 340000 mm3.

Table 1
Unit cell and overall specimen design and dimensions for the examined 3D structures of 8% volume fraction.
Structure serial Lattice unit cell Unit cell design Cell design A 2 × 2 × 2 cells structure The CAD model of overall The side length of the
number type parameters showing lattice specimen Overall concrete specimen
the way the cells joined (mm)
D or l d
together
(mm) (mm)

1 Circular D = 10 1.579 170 × 40 × 50

2 Octagonal l = 4.14 1.617 170 × 40 × 50

3 Strengthened l = 4.14 1.239 170 × 40 × 50


octagonal

4 RO l = 4.14 1.164 170 × 40 × 50

5 Cubic l = 10 2.149 170 × 40 × 50

* The struts of all unit cell are circular cross-sections with a diameter of “d”. For unit cell of the circular lattice type, “D” represents the diameter of three crossed rings.
For all other unit cell types, “l” represents the length of polygon equilateral members.

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Table 2
3D printing / PA6 related parameters used in this study.
Thermal deformation Hardness/ Tensile strength Tensile strength Bending Bending Stamping Sintering
temperature/℃ HRC (tensile)/MPa (fracture)/MPa strength/MPa modulus/MPa strength/KJ/cm temperature/℃

153 86 50 70 72–80 2800 2.7 1200

* This information on this table is provided by the manufacturer entrusted by 3D printing (Jiaxing Zhiyin Technology Co., Ltd.).

Then, according to the volume fraction of 8% of the lattice in the lattices itself.
specimen, the volume of each lattice is controlled at about 27200 mm3, The lattice structure printed with PA6 as molding material is shown
and the diameters of unit cell struts and members are inversely solved in Fig. 2 (taking cubic lattice as an example).
according to eq. (2)–(6). The strut diameter of the calculated unit cell is PA6 (nylon 6, polyamide 6, PA6) is a plastic composed of polyamide
shown in Table 1. resin. It has low melting point, light weight, high strength, good ther­
moplastic and excellent mechanical properties. It has excellent wear
2.2. Lattice preparation resistance, high heat resistance, self lubrication, toughness and good
processing performance. At the same time, it has good solvent resistance
Selective laser sintering (SLS) technology is a 3D printing technology and corrosion resistance, and is widely used in industrial field and daily
with powder material as the main molding raw material and infrared life.
laser as energy [44]. SLS printing technology uses powder spreading to
lay a layer of powder material on the upper surface of the formed parts 2.3. Lattice-reinforced concrete specimens preparation
and heat it to a temperature just below the powder sintering point. The
control system controls the laser beam to scan on the powder layer ac­ According to test method of cement mortar strength [49], the mix
cording to the cross-sectional profile of the layer, so as to raise the proportion of lattice-reinforced concrete (generalized concrete includes
temperature of the powder to the melting point for sintering and cement mortar) is determined as 450 g cement, 1350 g standard sand
bonding with the formed parts below. After the completion of one layer, and 225 g water. The cement is ordinary portland cement P.O 32.5
the worktable will drop by one layer, and the spreading roller will produced by Jiangsu Helin Cement Co., Ltd., the standard sand is Chi­
spread a layer of uniform and dense powder on it to sinter the section of nese ISO standard sand produced by Xiamen ISO standard sand Co., Ltd.,
a new layer until the whole model is completed. SLS molding technology and the water is Zhenjiang tap water.
is shown in Fig. 1. The specimens shall be manufactured according to the steps of
SLS has the advantages of wide range of material selection, high weighing and sampling, feeding and mixing, grouting and casting,
precision, no support structure, and can form complex components [45]. vibrating and compacting, forming and curing. The lattice-reinforced
The disadvantages are high manufacturing cost, large material loss, long concrete structures are prepared by mold pouring, demoulded after
processing time, difficult process, rough sample surface, easy shrinkage 24 h and cured in a standard curing box for 28 days. The specimens
and warpage after forming [46]. cured for 28d under standard curing conditions is shown in Fig. 3.
Because the lattice structures designed in this test are complex and it In order to control the lattice location within the concrete samples
is not easy to form by using other 3D printing technologies, SLS tech­ and ensure that different lattices are centered in the x, y and z directions
nology is adopted. When the lattice structure printed by different ma­ in the mold, and avoid the situation that the lattice touches the base of
terials strengthens concrete, the adhesion between it and cement matrix the sample, we use 6 improved wooden sticks to fix each type of lattice
will be greatly different, which will affect the evaluation of test results. respectively. For different lattice types, the notch size and position of
Shalchy et al. [47] conducted quantitative research on the adhesion small wooden sticks are determined according to the diameter and
energy between several polymers and cement matrix, and found that relative position of unit cell strut. The shape, relative size, position in the
PA6 has the highest adhesion with cement matrix. Therefore, PA6 was mold and actual photographic of the six small wooden sticks are shown
used as the material to prepare the lattice in this test. All lattice samples in Fig. 4.
are printed in the same direction with the same 3D printer (the con­
struction direction is consistent with the loading direction), so as to 3. Experimental details
reduce the difference between different printers and the difference of the
printing construction direction on the mechanical properties of the 3.1. Experimental methods and setups

In order to ensure that there are no holes and other non-compactness

Fig. 2. Example of PA6 finished products made by SLS process (taking cubic
Fig. 1. SLS technology forming diagram. lattice as an example).

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in the test is 12 frames / s.

3.2. Experimental steps

(1) Connect universal tester, AE instrument, DIC device and


computer.
(2) Spray the speckle on the surface of the specimens with paint,
place it in front of the lens for observation, and decide whether to
optimize the speckle according to the clarity.
(3) After speckle fabrication, place the specimen on the support of
the universal tester, adjust the span according to the scale, and

Fig. 3. Concrete specimen formed and cured for 28 days (taking control
specimen as an example).

in the hardened specimens, ultrasonic testing is used to detect whether


there are defects in the specimens. They are used in this test after they
have been tested without defects. This study needs to evaluate the me­
chanical properties of different structural lattice-reinforced concrete
specimens under bending loads. The three-point bending experiment is
carried out in the form of a simply supported beam, with only one
loading point above the sample. DIC was used to monitor the whole
deformation field, and AE was used to monitor the whole damage
process.
The experimental setups are shown in Figs. 5-7. Using the TH-8201S Fig. 5. Loading diagram of three-point bending loading test (unit: mm).
universal testing machine with a load capacity of 10kN, three-point
bending loading was performed on the lattice-reinforced concrete
specimens at a loading rate of 0.05 mm/min to simulate quasi-static
loading.
During the loading process, the DS2-8A (four-channel) type full in­
formation AE signal analyzer produced by Ruandao was used for AE
signal collection and analysis. The diameter of the sensor is 16 mm. In
the experiment, ordinary electrical insulating tape is used to fix the
sensor and the specimens to reduce the loss of waveform, and vaseline is
used as the coupling agent at the contact part between the sensor and the
specimens to improve the sensing effect. The sensor is connected to the
device using a 60 db Smart AE preamplifier. The experimental acquisi­
tion accuracy was 16 bit, the sampling rate was 3 M, the sampling time
interval was 0.3333 μs, the threshold trigger mode was adopted, and the
channel threshold value was 100 mV.
The 2D-DIC system of CSI company is used to calculate the image of
the whole loading process. The whole image acquisition system is pro­
vided with technical support by Weishi Digital Image Technology Co.,
Ltd. the hardware equipment is composed of MV-EM510M/C CCD
camera, BT-23120 telecentric lens, light source and a support. The CCD
has 5 million pixels and a resolution of 2456 pixels × 2058pixel. The
Fig. 6. Schematic diagram of test monitoring system.
magnification of telecentric lens is 0.072. The image acquisition rate set

Fig. 4. The shape, relative size, position in the mold and actual photographic of the six small wooden stick (taking cubic specimen as an example).

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(a) Test loading and acquisition system (b) Data monitoring and analysis system
Fig. 7. Test instrument.

ensure that the indenter of the tester is located on the center line 4.1. Load-displacement curve analysis
of the two supports.
(4) Start the AE software, set parameters, and conduct a broken-lead Fig. 8(a) is a general conclusion abstracted from the test results of
test on the specimen to ensure that the AE system is in normal Fig. 8 (b). The existing theories show that the deformation under loading
working state. of cement-based materials will go through the initial compaction stage,
(5) Carry out test preloading at the loading speed of 0.01 mm/min. elastic deformation stage and plastic deformation stage. Therefore, ac­
When the sensor has force, immediately suspend the loading and cording to the test results, this work defines that the mechanical
clear the displacement and force. response process of 3D printed lattice-reinforced concrete specimen
(6) Officially start the test and load at the loading speed of 0.05 mm/ under three-point bending load is divided into the following stages:
min until the specimen is damaged.
(1) Initial compaction stage (o-a): the local indentation of the spec­
4. Results and discussion imen surface near the indenter caused by the stress concentration
in the loading process, and the displacement of the test system.
Three points bending tests were carried out on 3D printed lattice- On the curve, the displacement changes greatly and the curvature
reinforced concrete specimens with different structures. There are 3 of the curve is big in this stage.
groups of lattice-reinforced concrete specimens with 5 different struc­ (2) Elastic deformation stage (a-b): the mid span deflection of the
tures, and a total of 18 test results are measured. For the lattice rein­ specimen changes little, and the bending bearing capacity of the
forcement specimens with five different structures, the group with large specimen increases rapidly. At this time, the mechanical response
difference is removed according to the first peak load in each group, and of the specimen can be regarded as elastic deformation, and the
then the smaller group of data in the two groups is selected for analysis. load displacement curve changes linearly.
(3) Plastic deformation stage (b-c): the curvature of the curve de­
creases relatively, the slope decreases, the specimen has

(a) Typical load-displacement curve of (b) Measured load displacement curve of control
lattice reinforcement specimen and lattice reinforcement specimens
Fig. 8. Load–displacement curve of concrete specimens.

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irreversible plastic deformation, and the resistance to deforma­ 4.2. DIC analysis
tion decreases.
(4) Brittle failure stage (c-d): the concrete near the bottom span of the DIC can effectively measure the whole deformation fields of lattice-
specimen cracked after reaching the ultimate flexural strength. reinforced concrete specimen in the whole process of loading. The
Once the crack appears, it propagates rapidly from bottom to top, collected images are processed by VIC-2D software to obtain the hori­
the bearing capacity decreases rapidly, the specimen is damaged zontal strain field (exx) of each characteristic point before brittle failure
and the brittleness is significant. in the whole loading process, as shown in Figs. 9 - 14.
(5) Reloading stage (d-e): after brittle failure, the compressive stress Under the action of three-point bending load, the section bending
is borne by the uncracked concrete on the upper part of the moment of the specimen shows decreasing from the middle of the span
specimen, and the tensile stress is continuously borne by the to the two supports. The shear force is equal to the value of the whole
lattice structure inside the specimen. The flexural bearing ca­ section, and the left and right directions are reversed with the mid-span
pacity rises again and reaches the peak value. At the same time, as the boundary. All sections are subjected to bending and shearing. The
the crack extends upward slowly and the width increases maximum bending moment will appear in the mid-span area, which is
continuously. the most prone to damage and failure.
(6) Failure stage (e-): after the stress reaches the maximum bending During the loading process of control specimen, there is no obvious
bearing capacity of the lattice structure inside the specimen, the boundary and distribution law between the compression area and ten­
members of the lattice structure are damaged from bottom to top, sion area in the whole strain field. According to the distribution of strain
the load is continuously borne by the undamaged upper mem­ field in elastic deformation and plastic deformation stage, there is no
bers, and the bearing capacity gradually decreases until it is obvious compression area near the indenter and no obvious stress con­
completely damaged. centration. Before brittle failure, there is no obvious tensile strain region
in the mid-span region at the bottom of the specimen.
In addition, we define the maximum load of lattice reinforcement As a quasi-brittle material with various anisotropy, concrete has
specimen before brittle failure as the first peak load (point c in Fig. 8 large stiffness and high elastic modulus after hardening. The strain field
(a)), regard the first peak load as the bending limit load, and evaluate nephogram in Fig. 10 (b) - (e) confirms that the deformation of pure
the mechanical properties of lattice-reinforced concrete specimens. Take concrete specimen under loading is small and the ductility is low, so
20% of the first peak load value as the dividing point between the initial there is no compressive stress concentration near the indenter. At the
compaction stage and the elastic deformation stage. same time, it is also confirmed that the brittleness of concrete is high.
The load displacement curve of lattice-reinforced concrete specimens Once the crack is formed, it propagates and penetrates from bottom to
measured in the test is shown in Fig. 8 (b). It can be seen from Fig. 8 (b) top rapidly. Therefore, there is no obvious tensile strain region at the
and Table 3 that the first peak load of octagonal, strengthened octagonal bottom of the mid-span before brittle fracture failure.
and cubic lattice reinforcement specimens are lower than that of the It can be found from the cloud diagram of strain fields in Figs. 10-14
control specimen, and the first peak load of circular and RO lattice that during the whole loading process of lattice reinforcement speci­
reinforcement specimens are higher than that of the control specimen. mens, the distribution of compression area and tension area shows
From the analysis of the first peak load of lattice-reinforced concrete obvious regularity, and the strain field is approximately symmetrically
RO lattice-reinforced concrete specimen has the strongest flexural distributed bounded by mid-span. According to the strain field distri­
bearing capacity, and its first peak load reaches 3210.23 N, which is bution in the elastic deformation and plastic deformation stages of the
13.29% higher than that of the control specimen. The first peak load of lattice reinforcement specimens, there are obvious compression areas
circular lattice-reinforced concrete specimen is slightly higher than that near the indenter and obvious stress concentration in the whole process
of the control specimen, an increase of 0.28%. Compared with the of loading. In addition, the strain cloud diagram is roughly bounded by
control specimen, the first peak load of octagonal and strengthened the connection line between the indenter and the two supports, showing
octagonal lattice-reinforced concrete specimens decreased slightly by the compressive strain at the upper part and the tensile strain at the
6.0% and 8.7% respectively. The lattice-reinforced concrete specimen lower part, which is close to the bending moment distribution charac­
with the weakest flexural bearing capacity is cubic specimen, and its first teristics of three-point bending. Before brittle failure, there is an obvious
peak load is 2461.59 N, which is 13.13% lower than that of the control tensile strain region near the mid-span at the bottom of the lattice
specimen. reinforcement specimen.
We calculated the peak strength (ff) of the specimen according to From the elastic stage, the tensile strain of the lattice reinforcement
formula (7) and listed it in Table 4 in detail. specimen is approximately banded along the vertical direction (in these
areas, it is easy to form damage bands, which corresponds to the analysis
3Ff L
ff = (7) of AE characteristic parameters in the next section). With the increasing
2bh2
load, the internal structure of the specimen is constantly adjusted and
where Ff is the first peak load of the specimen; L is the center distance of the stress is redistributed. The small banded tensile strain area continues
bending support cylinder, L = 140 mm in this study; b is the width of the to gather and form a larger banded tensile strain area. Finally, the
specimen, b = 40 mm in this study; h is the height of the specimen, h = maximum tensile strain concentration area before brittle failure is
50 mm in this study. formed, resulting in the brittle failure when the stress in this area ex­
Since the bearing capacity of lattice-reinforced concrete specimens ceeds the maximum tensile strength of lattice-reinforced concrete.
will be greatly reduced after brittle failure, and the load will continue to Compared with the control group, the strain field cloud diagram in
be borne by the lattice inside the specimen, which means structures Figs. 10-14 (b) - (e) can prove that the addition of lattice changes the
failure in the practical application of structural engineering, the subse­ stress transfer path inside the concrete specimen, improves the inherent
quent sections will focus on the stage analysis before brittle failure. anisotropic characteristics of concrete, increases the flexibility of the
specimen, increases the deformation and ductility of the specimen under

Table 3
First peak load of control and lattice reinforcement specimens.
Specimen type Control Circular Octagonal Strengthened octagonal RO Cubic

First peak load/kN 2833.789 2841.87 2662.937 2587.76 3210.423 2461.587

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

Table 4
First peak strengthened of control and lattice reinforcement specimens.
Specimen type Control Circular Octagonal Strengthened octagonal RO Cubic

First peak strengthened/MPa 5.95 5.97 5.59 5.43 6.74 5.17

loading, and thus the compressive stress concentration occurs near the (1) For AE hits, we can use it to measure the severity of damage in­
indenter. At the same time, it is confirmed that the concrete of lattice side the structure. When the total amount and frequency of
reinforcement specimens are brittle failure caused by tension, so there is damage exceed a certain threshold, it indicates that the damage
obvious tensile strain at the bottom of the mid-span before brittle failure. inside the structure develops rapidly, and an early warning
According to the cloud diagram of strain fields, the maximum strain should be issued in time.
before brittle fracture of lattice reinforcement specimens are sorted in (2) For energy, we can use it to measure the strength of a structural
Table 5. Combined with Table 3, we can find that brittle failure occurs in damage and the amount of energy released. When the energy
the mid-span area of all lattice reinforcement specimens due to occur the exceeds a certain threshold, it indicates that a large degree of
maximum tensile strain, and the order of maximum strain values are damage may occur inside the structure, and an early warning will
consistent with that of the first peak load. be issued if necessary.
The strain near the middle of the span before brittle failure is the (3) For peak frequency, we can use it to judge the type of damage or
largest in the RO lattice-reinforced lattice, reaching 0.017. Compared failure of the structure (such as brittle failure, plastic failure,
with the RO lattice-reinforced specimen, the maximum strain of circular, etc.), and judge whether the damage comes from an internal
octagonal, strengthened octagonal and cubic lattice-reinforced speci­ component to further judge whether the structure is in a safe
mens decreased by 21.2%, 31.8%, 51.8% and 57.6% respectively. state.
Based on the use of DIC technology in the whole field deformation
monitoring of lattice-reinforced concrete in the whole process of According to the hits of control specimen in Fig. 15 (a) the AE
loading, we believe that with the high-precision and non-contact mea­ characteristics of the first three stages of brittle failure of concrete
surement characteristics of DIC, it can be applied to the actual mea­ specimens are analyzed as follows:
surement of engineering structures (such as long-span beams, shear
walls, structural columns, etc.). Monitor the surface of the structure or (1) Initial compaction stage: at the beginning of this stage, with the
component to obtain accurate displacement or deformation information increase of load, the number of AE hits increases slowly, but the
of the whole field of the structure or component, so as to evaluate the total number is small, and the time interval is large, indicating
safety and reliability of the structure or component. When the that there is little damage inside the concrete specimen during
displacement and deformation of structures or components are large, this period. In the middle of this stage, with the increase of load,
give early warning in time and take measures to avoid major accidents. stress concentration occurs in the area near the indenter, making
the concrete reach the ultimate compressive strength and local
4.3. AE analysis collapse failure, with more local damage, so AE hits increases and
Hits time interval is small. In the later stage of this stage, with the
AE refers to the phenomenon that materials or structures deform or increase of load, the stress concentration is redistributed and
break under the action of external or internal forces and release strain reduced with the adjustment of internal structure of concrete, and
energy in the form of stress waves [34]. AE testing is a non-destructive the increase of AE hits slows down. Generally speaking, the
testing method. The AE signal collected by AE sensor comes from the damage of concrete in the initial compaction stage is small and
deformation or damage of the specimen, which can detect the specimen the energy release is low.
in real time. (2) Elastic deformation stage: after the initial compaction stage, the
The characteristic parameters commonly used in AE analysis include specimen is in elastic deformation state during loading. This work
AE hits, amplitude, duration, rise time, ringing counting, energy, uses the generalized concrete, which is mixed and hardened by
centroid frequency, peak frequency, etc. In this paper, hits, energy and cement paste and fine aggregate, and belongs to multiphase
peak frequency are selected as evaluation indexes, and time-force, time- composite material. There are micro-cracks inside the hardened
hit, time-energy and time-peak frequency curves are drawn for further cement slurry and at the interface between the hardened cement
analysis. The meanings of hit, energy and peak frequency are as follows: slurry and fine aggregate. With the increase of load, the elastic
deformation increases and the micro-cracks increase, which will
(1) Hits: any signal that exceeds the threshold and causes the channel produce more AE hits and release energy.
to obtain data is called an impact, and the number of measured (3) Plastic deformation stage: after the concrete reaches the elastic
impacts is called AE count. It reflects the total amount and fre­ limit load, it will enter the plastic deformation stage and the
quency of AE activities and is often used for AE activity deformation cannot be recovered. At this stage, AE hits increases
evaluation. rapidly, a large number of damages appear in the concrete, micro-
(2) Energy: the area under the AE signal envelope, the relative energy cracks increase and propagate rapidly, and energy is released
and intensity of the reaction event, which is insensitive to the rapidly. The internal structure of the specimen is adjusted due to
threshold, propagation characteristics and operating frequency. energy release, and the internal stress is redistributed. The in­
(3) Peak frequency: the frequency corresponding to the peak point in crease of load aggravates the damage and overlaps with each
the frequency domain of AE signal. The distribution of peak fre­ other to form a damage areas. The micro-cracks propagate and
quency can roughly reflect the occurrence of different types of form macro-cracks. The macro-cracks propagate and penetrate
damage. from bottom to top, resulting in the brittle failure of concrete
specimen.
The following explains the guiding significance of these three AE
characteristic parameters for the application of acoustic emission in It can be seen from Table 6 that the peak frequency of AE signal in the
practical engineering. process of crack increase and propagation of concrete specimen is
mainly distributed in two sections: 50–100 kHz and 150–200 kHz. The
low frequency part is caused by the cracking of hardened cement slurry,

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a)Control specimen displacement-load curves.

(c)Horizontal strain field at t = 125.82s (near


(b) Horizontal strain field at t = 0s (near o point)
a point)

(d)Horizontal strain field at t = 628.82s (near (e)Horizontal strain field at t = 629.09s (near
b point) c point)
Fig. 9. Control specimen load–displacement curve and horizontal strain field of corresponding characteristic points.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a)Circular specimen displacement-load curves.

(b)Horizontal strain field at t =0s (near o (c)Horizontal strain field at t = 179.7s (near
point) a point)

(d)Horizontal strain field at t = 544.3s (near (e)Horizontal strain field at t = 544.8s (near
b point) c point)
Fig. 10. Circular specimen load–displacement curve and horizontal strain field of corresponding characteristic points.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a)Octagonal specimen displacement-load curves.

(b)Horizontal strain field at t = 0s (near o (c)Horizontal strain field at t = 327.68s (near


point) a point)

(d)Horizontal strain field at t = 764.76s (near (e)Horizontal strain field at t = 765.68s (near
b point) c point)
Fig. 11. Octagonal specimen load–displacement curve and horizontal strain field of corresponding characteristic points.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a)Strengthened octagonal specimen displacement-load curves.

(b)Horizontal strain field at t =0s (near o (c)Horizontal strain field at t = 180.07s (near
point) a point)

(d)Horizontal strain field at t = 543.2s (near (e)Horizontal strain field at t = 543.62s (near
b point) c point)
Fig. 12. Strengthened octagonal specimen load–displacement curve and horizontal strain field of corresponding characteristic points.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a)RO specimen displacement-load curves.

(b)Horizontal strain field at t = 0s (near o (c)Horizontal strain field at t = 179.7s (near


point) a point)

(d)Horizontal strain field at t = 544.3s (near (e)Horizontal strain field at t = 544.8s (near
b point) c point)
Fig. 13. RO specimen load–displacement curve and horizontal strain field of corresponding characteristic points.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a)Cubic specimen displacement-load curves.

(b)Horizontal strain field at t = 0s (near 0 (c)Horizontal strain field at t = 158.69s (near


point) a point)

(d)Horizontal strain field at t = 588.81s (near (e)Horizontal strain field at t = 589.85s (near
b point) c point)
Fig. 14. Cubic specimen load–displacement curve and horizontal strain field of corresponding characteristic points.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

Table 5 aggregate. Therefore, the peak frequency of AE signal is mainly low


Maximum strain before brittle failure of lattice reinforcement specimens. frequency, and the peak frequency is distributed around 100 kHz. In the
Lattice Circular Octagonal Strengthened RO Cubic later stage of loading, with the further increase and propagation of
type octagonal micro-cracks, it mainly causes the fracture of fine aggregate in the
Strain 0.0134 0.0116 0.0082 0.017 0.0072 specimen and the cracking of a small amount of hardened cement slurry.
Therefore, the peak frequency of AE signal is mainly high frequency, and
the peak frequency is distributed around 480 kHz.
and the high frequency part is caused by the fracture of fine aggregate The failure characteristics of the lattice-reinforced concrete speci­
particles. According to Fig. 15 (a), in the early stage of loading, there are mens at three-point bending are similar to that of control specimen.
few micro-cracks in the concrete specimen, mainly the cracking of Comparing the AE hits parameters of the lattice reinforcement speci­
hardened cement slurry and a small amount of weak or defective fine mens with the control specimen, it can be found that before the brittle

(a) Control (b) Circular

(c) Octagonal (d) Strengthened Octagonal

(e) RO (f) Cubic


Fig. 15. Time-Force, Time-Hit, Time-Energy and Time-Peak Frequency curves: (a) Control, (b) Circular, (c)Octagonal, (d) Strengthened Octagonal, (e) RO, (f) Cubic.

Table 6
AE hits and peak frequency classification (ratio) before brittle failure of specimens.
Number Specimen type Hits/n 0 kHz 0–50 kHz 50–100 kHz 100–150 kHz 150–200 kHz ≥200 kHz

① Control 544 105(19.30%) 60(11.03%) 145(26.65%) 16(2.94%) 218(40.07%) 0(0.00%)


② Circular 230 18(7.83%) 199(86.52%) 6(2.61%) 0(0.00%) 7(3.04%) 0(0.00%)
③ Octagonal 401 39(9.73%) 337(84.04%) 4(1.00%) 4(1.00%) 15(3.74%) 2(0.50%)
④ Strengthened octagonal 154 25(16.23%) 99(64.29%) 2(1.30%) 1(0.65%) 25(16.23%) 2(1.30%)
⑤ RO 182 21(11.54%) 153(84.07%) 5(2.75%) 1(0.55%) 2(1.10%) 0(0.00%)
⑥ Cubic 74 20(27.03%) 41(55.41%) 2(2.70%) 1(1.35%) 10(13.51%) 0(0.00%)

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

failure of the lattice reinforcement specimen under three-point bending degree, failure mode and loading stress level is established, which pro­
load, the total number of AE hits decreased significantly compared with vides a theoretical basis for determining the loading health state of in-
the control specimen (Hits = 544), and the cubic lattice reinforcement service concrete structures or components, so as to make effective
specimen (Hits = 74) decreased the most, by 86.40%. Octagonal lattice early warning and timely reinforcement in case of serious damage pro­
reinforcement specimen (Hits = 401) decreased the least, with a cess of structures or components.
decrease of 26.29%. The above analysis shows that the addition of lat­
tice can effectively reduce the number of internal damage of concrete 4.4. Failure characteristics
specimen in three-point bending test and improve the mechanical
response of concrete. Fig. 16 shows the crack location and morphology of control and
Secondly, the number of AE hits in the initial compaction stage, lattice reinforcement specimens. Through the analysis of test results, it
elastic deformation stage and plastic deformation stage of the concrete can be seen that the control and lattice reinforcement specimens have
specimens of the lattice reinforcement decreased, which is specifically relatively low tensile strength and relatively high brittleness, and all
reflected in the following aspects: samples fail due to a single crack. The cracks in all specimens were
formed from the bottom and propagated upward. Because there is no
(1) There was no AE hits in the early period of the initial compaction lattice inside the control specimen, when the first peak stress is reached
stage for the lattice reinforcement specimens of octagonal, RO and failed, the specimen is brittle fracture, directly broken into two
and cubic structures. The number of AE hits of lattice reinforce­ parts, and makes a huge sound at the same time. Although the lattice
ment specimens with five different structures in the initial reinforcement specimen is also brittle failure when failed, there will be
compaction stage is lower than that of control specimen. secondary peak load after the first peak load, and the speed of crack
(2) Except cubic lattice reinforcement specimen, the AE hits in the propagation from the bottom to the upper is relatively slow, and there
early stage of elastic deformation of concrete specimens in the will be no loud noise at the moment of failure. This is because there is a
other four lattices reinforcements is equivalent to that in the large difference between the elastic modulus of the lattice and the elastic
control specimen, but the increase in the later stage is signifi­ modulus of the concrete. Under the same load, the deformation of the
cantly slower. lattice is greater than that of the concrete. After the concrete near the
mid-span at the bottom of the lattice reinforcement specimen reaches
With the addition of lattice, the AE hits of concrete specimens under the ultimate bending capacity, it breaks and exits the work. The un­
three-point bending test are reduced mainly due to the following two cracked concrete on the upper part bears the pressure, and the internal
reasons: lattice continues to bear the tension. Therefore, the lattice-reinforced
concrete specimens will have a secondary peak load after the first
(1) The 3D printing PA6 lattices have good ductility and can produce peak load.
large deformation under the action of load. The lattices are added Comparing the crack positions at the bottom of control and lattice
to replace the original concrete, so that part of the original stress reinforcement specimens, it can be found that the crack formation po­
in the concrete is borne by the lattice. Due to the large elastic sition of control specimen is closest to the mid-span, the crack formation
modulus of the lattice, under the reinforcement of the lattice, the position of RO and octagonal lattice reinforcement specimens is second,
lattice reinforcement specimens deforms and absorbs energy and the crack formation position of circular, strengthened octagonal and
under loading, which reduces the generation of AE hits. cubic lattice reinforcement specimens are farthest. According to the
(2) Concrete is an anisotropic material with uneven stress distribu­ previous mechanical response under three-point bending load, the mid-
tion under loading, which is easy to produce stress concentration. span of concrete specimen is the most prone to failure under three-point
The addition of the lattices transfers the stress inside the concrete bending load. Therefore, we can be sure that using 3D printed lattices as
specimens to the lattices, and then the lattices are transferred to reinforcement in concrete can significantly change the crack formation
the nearby lattice members or concrete, which effectively elimi­ position of concrete under three-point bending load, and then improve
nates the phenomenon of stress concentration, changes the stress the brittle mechanical response of concrete.
transfer path, and the stress redistribution phenomenon is more Combined with the analysis of the first peak load of control and
obvious. lattice reinforcement specimens in Table 3 and the analysis of five
different structures of unit cell in reference [42], we can find that the
According to Table 6, it can be found that the AE peak frequency of deformation mechanism of RO lattice is mainly tensile, circular lattice is
the control specimen is mainly distributed in the high frequency region mainly bending. Under the three-point bending load, the bottom surface
of 150–200 kHz, while the AE peak frequency of the lattice reinforce­ of the specimen is subject to the bending action dominated by tensile
ment specimens are distributed in the low frequency region of 0–50 kHz. force. Therefore, the reinforcement effect of RO lattice is the largest,
The main reason is that the addition of lattice makes the concrete more followed by circular lattice. Reference [42] does not give much expla­
ductile and flexible. Concrete itself is a quasi-brittle material, which can nation for the bending response of octagonal, strengthened octagonal
be regarded as a rigid body. When cracks and brittle fracture occur in it, and cubic. At the same time, some analysis is also made for the first peak
the elastic waves are mainly concentrated in the high frequency band. load of octagonal, strengthened octagonal and cubic lattice reinforce­
Compared with plain concrete, the flexibility of lattice-reinforced con­ ment specimens is less than control specimen. This paper believes that
crete is improved, so that when cracks and brittle fracture occur in the the diameter of octagonal and cubic unit cell struts is relatively large,
interior, the elastic wave is mainly concentrated in the low frequency resulting in excessive concentration of lattice in unit volume. If the crack
band. This also fully shows that the addition of lattice can effectively is formed near the geometric center, due to the brittleness of concrete, it
reduce the peak frequency of AE of brittle failure of concrete. will extend quickly, resulting in difficulties in controlling the crack, then
Based on the above AE technology for the damage monitoring of affect the reinforcement effect. The porosity of strengthened octagonal
lattice-reinforced concrete in the whole process of loading, we believe unit cell is small, and when casting concrete (cement mortar) in this
that with the characteristics of real-time monitoring and nondestructive work, only cement slurry enters the interior, and fine aggregate rarely
testing of AE, it can be applied to the dynamic monitoring of the internal enters, and poor aggregate gradation, resulting in the decline of
damage process of engineering structures or components to evaluate the comprehensive performance. Whether the addition of octagonal,
damage location and degree of structures or components. The charac­ strengthened octagonal and cubic lattices will really reduce the flexural
teristic parameters of AE are used to analyze the damage and failure capacity of concrete and the response mechanism need to be further
process of concrete, and the qualitative relationship between damage studied and demonstrated.

16
J. Liu et al. Construction and Building Materials 333 (2022) 127418

(a) Control specimen. (b) Circular specimen.

(c) Octagonal specimen. (d) Strengthened octagonal specimen.

(e) RO specimen. (f) Cubic specimen.


Fig. 16. Fracture location of control and lattice reinforcement specimens.

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J. Liu et al. Construction and Building Materials 333 (2022) 127418

5. Conclusions Acknowledgment

In this paper, lattices with five different structures are designed and The authors are grateful for the financial support provided by the
printed by selective laser sintering technology. The lattice was placed in National Natural Science Foundation of China (Grant Nos. 11872025)
the concrete as the inner core, and the three-point bending test was and the Six Talent Peaks Project in Jiangsu Province (Grant No. 2019-
carried out after 28 days of standard curing. The mechanical properties KTHY-059).
of lattice-reinforced concrete structures under three-point bending were
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