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A laboratory and filed evaluation of Cold Recycled Mixture for base layer
entirely made with Reclaimed Asphalt Pavement
Cesare Sangiorgi, Piergiorgio Tataranni ⇑, Andrea Simone, Valeria Vignali, Claudio Lantieri, Giulio Dondi
DICAM-Roads, Dept. of Civil, Chemical, Environmental and Materials Engineering, University of Bologna, V.le Risorgimento 2, 40136 Bologna, Italy
h i g h l i g h t s
Main research goal: use of 100% RAP for Cold Recycled Mixture base layers.
Laboratory and trial field comparison between Cold Recycled Mixture and Hot Mix Asphalt.
The presence of 100% RAP does not seem to worsen the compactability of the bituminous mixture.
ITS and ITSM test results confirmed the difference in terms of resistance and stiffness between CRM and HMA.
The mechanical and physical properties of CRM are strictly related to the mix design and to the quality of RAP.
a r t i c l e i n f o a b s t r a c t
Article history: Asphalt concrete (AC) recycling is probably the most cost-effective technique for the rehabilitation of
Received 4 July 2016 stressed road pavements and for the construction of new ones. The increased interest in this technology
Received in revised form 31 January 2017 comes from the need of reducing the costs connected to the production processes and to the use of virgin
Accepted 1 February 2017
raw materials. In fact, the benefits connected to the use of Reclaimed Asphalt Pavement (RAP) are related
Available online 16 February 2017
to the possibility of substituting the natural aggregates and the virgin binder of an AC mixture, without
negatively affecting its mechanical properties. When this process is made at ambient temperature (Cold
Keywords:
Recycled Mixes – CRM), more advantages are brought about with, above all, the reduction in energy con-
Reclaimed Asphalt Pavement
Cold Recycled Mixture
sumption and emissions during in plant production and laying, in addition to the actual possibility of
Bitumen achieving durable pavement layers. A CRM totally made of RAP is proposed in this research, the main goal
Emulsion of which was to evaluate the different physical and mechanical characteristics derived by the large use of
Base layer recycled materials. According to the final mix-design, CRM does not show significant differences in terms
of physical properties, when compared to a Hot Mix Asphalt (HMA) for base layers. Moreover, even if the
experimental mixture shows lower mechanical values, these are acceptable and higher than the limits
imposed by the most common Italian technical specifications for Cold Mix Asphalts containing up to
30% RAP.
Ó 2017 Elsevier Ltd. All rights reserved.
1. Introduction and scope practitioners to adopt more sustainable technologies and design
approaches.
In recent years, a constant decrease of costs related to the con- In this context, the pavement construction industry still repre-
struction and maintenance of civil infrastructures has been sents one of the largest consumers of natural resources and raw
recorded. This is due to the increasing interest of public opinion materials [2] and its negative environmental and economic effects
in the concept of sustainable development and to the growing are enhanced by the production of quantities of wastes during the
political awareness of environmental issues [1] that leads maintenance and the rehabilitation of stressed roads [3,4].
The limited availability of virgin aggregates, the rise in prices of
materials and the additional costs related to the disposal of wastes,
have promoted the use of recycling technologies for the rehabilita-
⇑ Corresponding author.
tion and construction of asphalt pavements[5,6,7].
E-mail addresses: cesare.sangiorgi4@unibo.it (C. Sangiorgi), piergiorg.tataranni2@
The recycled materials used in the road construction industry
unibo.it (P. Tataranni), andrea.simone@unibo.it (A. Simone), valeria.vignali@unibo.it
(V. Vignali), claudio.lantieri2@unibo.it (C. Lantieri), giulio.dondi@unibo.it (G. Dondi). are generally classified as:
http://dx.doi.org/10.1016/j.conbuildmat.2017.02.004
0950-0618/Ó 2017 Elsevier Ltd. All rights reserved.
C. Sangiorgi et al. / Construction and Building Materials 138 (2017) 232–239 233
Industrial by-products, such as steel slags, blast furnace slags, constant mass. Tests were always carried out on fully cured
fly ashes and similar; specimens.
Road by-products, mainly Reclaimed Asphalt Pavement (RAP) In this first step of the experimental program, the workability
materials; and volumetric properties of the mixtures were assessed by means
Construction and Demolition by-products, such as crushed con- of the compaction curves obtained at the end of the gyratory com-
crete, mortars, tiles, bricks and similar [8,9,10]. paction. The volumetric characterization was then supported by
the analysis of the air voids content of each specimen (EN
In the last ten years, an ever-increasing number of these mate- 12697-8).
rials has been tested in addition, partial or total substitution of The static mechanical characterization included the Indirect
constituents commonly used in paving applications. Tensile Strength (ITS) both in dry (at 25 °C) and wet conditions
Thus different innovative and eco-friendly materials are (EN 12697-12). According to the EN 12693-23 standard, the
now available on the market and a number of second-hand specimen was loaded by a constant velocity of 50 mm/min until
materials are studied, being the step of physical and failure.
mechanical characterization necessary to assess their real benefits The consecutive dynamic mechanical characterization was
[11,12,13]. based on the determination of the Stiffness Modulus applying indi-
RAP, being readily available, is by far the most known and rect power to cylindrical specimens (EN 12697-26). The stiffness
common recycled material used within asphalt mixtures, also modulus was determined through a pulse loading with a 124 ms
because it partially covers the need of virgin aggregates and rise-time, to generate a horizontal deformation of 7 ± 2 lm in the
new asphalt binder [14]. In the last years, different techniques core of the sample. Before testing, all the specimens were first con-
and approaches have been extensively studied and applied to ditioned for six hours at three reference temperatures: 5, 20 and
incorporate increasing amounts of RAP in the production of 40 °C.
ACs. Among them Cold Mix Asphalt (CMA) recycling is now pop-
ular due to its versatile properties and proven environmental 2.2. Trial field phase
advantages [15]. From an economic and environmental point of
view, the possibility to produce bituminous mixtures without Once defined the mix design and the physical and mechanical
the addition of heat, results in a significant reduction in energy properties of the two different mixtures, these were laid to devise
consumption and emissions during the in plant production and a full-scale trial field. In situ test and samples collection were
laying processes [16,17,18]. More recent studies [19,20,21] also planned in four dates, corresponding to 0, 60, 180 and 365 days
assessed the possibility of incorporating up to 100% of RAP in of cumulative heavy traffic. A specific quantity of material was
fully recycled mixtures. taken from the paving screed during the laying process and three
The present research starts form the idea that 100% RAP can be samples for each mixture were prepared with gyratory compaction
advantageously used in cold recycling technique for the production (ASTM D6925). Each specimen had a dry mass of 4500 g and a
of bituminous mixtures for eco-friendly and durable pavements. diameter of 150 mm, made with a constant compaction pressure
The aim is to evaluate the positive properties conferred to the mix- of 600 kPa, external angle of 1.25° and 180 revolutions. The work-
ture by using high amount of recycled materials together with bin- ability and volumetric characteristics of the mixtures were anal-
der emulsion and cement. Starting from the laboratory mix-design ysed by means of the compaction curves and the determination
a full scale trial field was constructed, in order to evaluate the of the air voids content of each specimen (EN 12697-8). The volu-
development of the mechanical and physical properties of the pro- metric analysis was also supported by the ITS test (EN 12697-23)
posed CRM when compared to a high-modulus HMA for base at 25 °C. The evolution of the mechanical characteristic of the
layers. two different mixtures for base layer was evaluated by means of
the ITSM test (EN 12697-26) at 20 °C carried out on cores. The
2. Experimental program, test methods and materials physical properties of the two mixes were also analysed and com-
pared to those obtained during the laboratory step, in order to
The experimental program was divided in two different and define the potential differences given by the in plant production
consecutive phases. The first one is a laboratory study in which and in situ compaction with roller.
the mix designs and the physical and mechanical properties of
the two different mixtures were defined. One, labelled CRM, made 2.3. Materials
out of 100% RAP material, the second one, labelled HMA, was a
high-modulus asphalt concrete mixture for base layer. Two different mixtures for base layers were studied: a tradi-
In the second phase, the mixtures were laid in a full-scale test tional HMA and a CRM.
section open to heavy quarry traffic. In situ tests and samples col- Three materials were used for the recycled mixture: Reclaimed
lection were planned at regular intervals, for the evaluation of the Asphalt Pavement (RAP), Cement (C) and Bituminous Emulsion
development of the mechanical characteristics of each mixture (EM). A small amount of water was added to the mixture to control
under. the workability and to achieve the maximum dry density during
compaction.
2.1. Laboratory phase RAP was collected and milled from a motorway asphalt
concrete pavement. Later, the material was divided in to three
Nine specimens were prepared for each of the mixture with different fractions: coarse RAP 20/40 (20–40 mm), coarse RAP
gyratory compaction (ASTM D6925). Each specimen had a dry 10/20 (10–20 mm) and fine RAP 0/10 (0–10 mm). Table 1
mass of 4500 g and a diameter of 150 mm, made with a constant summarizes the properties of the aged bitumen recovered from
compaction pressure of 600 kPa, external angle of 1.25° and 180 the RAP.
revolutions. As for binder materials, a typical Portland Cement 32.5 and a
Laboratory curing of CRM specimens has been carried out in bituminous emulsion (61% bitumen content) with a 55 pen grade
a single way. After the production, specimens were placed in SBS modified bitumen (Table 2) were adopted.
oven for 3 days at 40 °C. In order to attain a full curing condi- For HMA mixture, a traditional 50/70 pen grade bitumen was
tion, the specimens were then kept at 20 °C until maintained a used according to a dosage of 4.3% by the weight of aggregates.
234 C. Sangiorgi et al. / Construction and Building Materials 138 (2017) 232–239
Table 1
Properties of the aged asphalt binder from RAP.
Table 2
Properties of the bitumen emulsion.
Table 3
Designation and composition of CRM.
Material Density (g/cm3) Mixture Fig. 2. CRM gyratory compaction curves (left); HMA gyratory compaction curves
(right).
RAP 20-40 2.62 14.0%
RAP 10-20 2.62 25.0%
RAP 0-10 2.63 55.0%
Filler 2.66 4.0%
and maximum density achieved at the end of compaction process.
Cement 2.95 2.0%
The relative differences for the final density of the two mixtures
Bitumen Emulsion (EM) 1.04 (at 25 °C) 4.0%
are less than 1%. As for the air voids content, there are not evident
Additional Water 0.99 (at 25 °C) 0.9%
variation between the CRM and HMA specimens. Both mixtures are
C. Sangiorgi et al. / Construction and Building Materials 138 (2017) 232–239 235
Fig. 5. Indirect Tensile Stiffness Modulus results: total and average values at 5, 20 Fig. 7. Compaction curve models for CRM and HMA after laboratory and trial field
and 40 °C. compaction.
4.1. Volumetric analysis: Compaction curve, air voids content and ITS Fig. 7 and Table 5 show the compaction curve models for CRM
and HMA for both laboratory (lab) and trial field (t.f.) phases.
A specific quantity of material was taken from the paving According to the results, all the compaction curves show the
screed during the laying process and three samples for each same trend. As verified during the laboratory phase, there are not
mixture were prepared by gyratory compaction (ASTM D6925), substantial differences between the compaction curves of the
with the same setting and procedures adopted in the laboratory CRM and HMA produced in plant. Both the mixtures achieve a good
phase. and almost equivalent final density at 180 gyrations (92.5% for
Fig. 6. Trial field paving operations: laying of CRM (left) and compaction with rollers (right).
C. Sangiorgi et al. / Construction and Building Materials 138 (2017) 232–239 237
Table 5 Those data confirm the value of the mix design and the good
Gyratory compaction curves models for CRM and HMA after laboratory and trial field paving processes of in plant production, laying and compaction.
compaction.
If the displacement to the maximum load is taken into account,
Mixture a b average values are higher for HMA (1.22 mm) when compared to
Model CRM lab 3.309 75.998 the recycled mixture (1.08 mm).
Model HMA lab 3.261 76.714
Model CRM t.f. 3.341 74.759
4.2. Development of stiffness modulus
Model HMA t.f. 3.476 75.231
Model equation: y ¼ a lnðxÞ þ b. As already mentioned, it was evaluated the development of the
stiffness of the two mixtures under traffic load, by taking cores
CRM and 93.3% for HMA). The same relative difference in terms of according to a specific timetable. Four date were chosen, corre-
density is maintained constant during the whole gyratory com- sponding to 0, 60, 180 and 365 days of cumulative passes of trucks.
paction process. After the laying and the roller compaction, three For each repetition, three cores for both mixtures were first condi-
cores were taken from each section. The air voids content was cal- tioned for six hours at 20 °C and then tested in accordance to EN
culated according to EN 12697-8 standard. Table 6 shows the 12697-26 standard in the indirect tensile configuration.
results. Fig. 9 shows the results for cores while data are compared with
Air voids content is in line with the compaction curve results: those obtained during the laboratory phase in Table 7.
even if there are not significant dissimilarity between the two mix- From the results analysis it is clear that both the mixtures fol-
tures, HMA has a lower air voids content. These values are in com- low a similar trend in terms of stiffness development. There is a
pliance with those generally obtained after compaction for base gradual increase in stiffness from day 0 to 60 followed by a pro-
layers in Asphalt Concrete. If compared to the volumetric analysis gressive reduction until day 365. The initial rise of the stiffness
made during the laboratory phase, it can be observed that the air moduli is probably due to the road pavement settlement given
voids content is lightly lower for the core samples. ITS test was also by the traffic load. After the 60th day, a gradual decrease in stiff-
carried out on the same cores, according to EN 12697-23 standard. ness values is recorded: it probably marks the beginning of the loss
Fig. 8 shows ITS values and the comparison between the values of mechanical properties of the material due to the effect of the
obtained in the laboratory and trial field phase.
The histogram shows a rise in ITS for core samples when com-
pared to laboratory specimens (+90%). In this case the ITS values
for CRM are very high considering this type of asphalt concrete
and similar to those usually identified for common bituminous
mixtures.
Table 6
Air voids content for CRM and HMA cores.
Fig. 8. ITS resistance for CRM and HMA after laboratory and trial field compaction.
238 C. Sangiorgi et al. / Construction and Building Materials 138 (2017) 232–239
Table 7
ITSM test results at 20 °C from laboratory and trial field phase.
traffic. For CRM mixture it is recorded a reduction in stiffness of The gyratory curves obtained after the compaction of the
33% from day 60 to day 365, while for HMA the same decrease is material taken from the paving screed, confirm the results
of 22%. However, even if values are lower when compared to the achieved in the laboratory phase. There are not evident
reference mixture, the stiffness modulus calculated for CRM is differences regarding the volumetric properties of the two
acceptable considering the high RAP content, the heavy traffic mixtures. The analysis of air voids content of the core
and the under-designed road section. Furthermore, in addition to samples proves the good workability and compactability
the results obtained after ITS tests, data from Table 7 confirm that properties of CRM.
CRM mix design is effectively reproducible in cold mix plant. The From ITS and ITSM test, it is confirmed the difference in terms of
values of stiffness for every core sample taken right after the pav- resistance and stiffness between the experimental and the
ing process, are always higher than those recorded for the speci- reference mixture. In this case, the mechanical properties of
mens processed in laboratory. CRM are considerably higher than those registered during the
laboratory characterization. The trends of development of
5. Discussion and conclusions the stiffness moduli for CRM and HMA are the same for the
whole period of analysis. The high presence of RAP does not
The aim of the present work was to evaluate the physical and determine an excessive reduction in stiffness after 365 days of
mechanical properties of a Cold Recycled Mixture made with cumulative passes of dumpers and trucks.
100% RAP material together with bituminous emulsion and Port-
land cement. The experimental program was divided in a labora- According to this result, it can be first stated that there is corre-
tory and a trial field phase, in which the properties of the spondence between the data obtained during the preliminary lab-
material have been always compared with those registered for a oratory characterization and those registered from in situ tests.
high-modulus Hot Mix Asphalt for base layer, taken as a reference. Thus highlights the validity of the mix design, and the quality of
According to the experimental results presented in this study, the constituents of the mixture. Furthermore, data also indicates
the following conclusion can be drawn for the laboratory phase: that all the processes, from in plant production to the stated paving
operations, have proved to be correct and completely feasible. The
The presence of 100% RAP inside the mix does not seem to wor- mechanical and physical properties of the experimental mixture
sen the compactability of the bituminous mixture. As shown by are strictly related to the mix design and to the quality of RAP,
the compaction curve, according this specific mix design, the being the step of characterization of this material of crucial impor-
high presence of RAP together with bituminous emulsion and tance. Further work is clearly necessary to study the durability and
cement do not limit the workability of the mixture if compared the fatigue performance of CRM mixtures in order to back the con-
to the reference HMA. There is not a significant difference in clusions here presented.
terms of final density and air voids content between the two
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