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AATCC TM197-2011e2(2018)e

Test Method for Vertical Wicking of Textiles


Developed in 2011 by AATCC Commit- 3.3 vertical wicking rate, n.—the are not a measure of comfort which is be-
tee RA63; editorially revised and reaf- speed at which liquid travels along or yond the scope of this method.
firmed 2012; reaffirmed 2013, 2018; through a textile. 5.7 The relationship between results
editorially revised 2016, 2019. 3.4 wicking, n.—in textiles, the move- obtained by vertical and horizontal wick-
ment of a liquid, by capillary action, ing tests is not known.
along or through a material.
Foreword 3.5 wicking distance, n.—the linear 6. Apparatus, Reagents, Materials
measurement that the liquid travels along
Historically, the textile industry has 6. 1 Distilled or deionized water at 21
utilized many different test procedures or through a textile from a starting point
to a stopping point. ± 2°C (70 ± 4°F).
for determining the wicking characteris- 6. 2 Marking pens, with fine point, per-
tics of textile fabrics, i.e., the movement 3.6 wicking time, n.—the measurable
period during which liquid travels along manent and soluble ink (see 13.2).
of water or liquid through fabrics. Within 6. 3 Stopwatch or digital timer.
the last decade, the industry has devel- or through a textile.
6. 4 Tape or ruler, mm graduations.
oped new technologies that have changed 6. 5 Surface tensiometer, if using liquid
water movement and absorbency re- 4. Safety Precautions other than water (see 9.1).
sponses of textiles leading to the use of 6.6 Erlenmeyer flask or elongated pan
NOTE: These safety precautions are
the labeling term “moisture manage- (see Figs. 2 and 3).
for information purposes only. The pre-
ment” to describe these phenomena. 6.7 Pipette and bulb.
cautions are ancillary to the testing proce-
Many interested groups (textile manufac- 6.8 Scissor jack (optional).
dures and are not intended to be all inclu-
turers, chemical suppliers, and retailers, 6.9 Straight pins or a holder that per-
sive. It is the user’s responsibility to use
as well as independent testing laborato- mits the suspension of a specimen into a
safe and proper techniques in handling
ries) participated in the efforts to stan- flask or other device (see Figs. 2 and 3
materials in this test method. Manufac-
dardize test methods to measure the verti- and 13.3).
turers MUST be consulted for specific
cal wicking properties of fabrics with 6.10 Small paper clip or clamp (op-
details such as material safety data sheets
moisture management attributes. tional).
and other manufacturer’s recommenda-
Unofficial techniques for determining 6.11 Template, 165 (or longer) × 25 mm.
tions. All OSHA standards and rules
the absorbency and wicking properties of 6.12 Disposable gloves, such as latex
must also be consulted and followed.
textile fabrics were published in the 2004 or nitrile.
AATCC/ASTM International’s Techni- 4.1 Good laboratory practices should
be followed. Wear safety glasses in all 6.13 Double-sided tape.
cal Supplement: A Compilation of Proce-
dures and Guidelines for Textile Products laboratory areas.
7. Specimens
and the 2008 AATCC/ASTM Interna-
tional’s Moisture Management Technical 5. Uses and Limitations 7.1 Determine whether the fabric has a
Supplement: Applicable to Apparel, Lin- hydrophobic or hydrophilic side. Upon
ens and Soft Goods (see 13.1). This test 5.1 The movement of liquid through a
agreement between interested parties, de-
method is based on one of the testing pro- fabric may be influenced by fiber con- termine whether both fabric sides are to
cedures for wicking published in this tent, fabric construction, mechanical or be tested. If only one fabric side is to be
Technical Supplement. chemical processing or a combination of tested, mark the selected side. If testing is
these. to be performed after laundering, use a
1. Purpose and Scope 5.2 This test method is used to evaluate marking pen with permanent ink to de-
the wicking ability of vertically aligned note the fabric side chosen for testing.
1.1 This test method is used to evaluate test specimens, exposed to distilled or 7.2 Minimize handling of the test spec-
the ability of vertically aligned fabric deionized water, where wicking is influ- imens or use gloves as oils from the skin
specimens to transport liquid along and/ enced by gravity. may affect moisture movement.
or through them, and is applicable to wo- 5.3 Liquids other than distilled or 7.3 All specimens should be cut at least
ven, knitted, or nonwoven fabrics. deionized water (tinted water, dye solu- 100 ± 5 mm from the selvage. If testing
tions, etc.) may be used in this test. If a garments, take specimens from different
2. Principle liquid other than water is chosen, its sur- garment panels away from seams, pock-
face tension should be measured and re- ets, plackets or other assembly features.
2.1 The rate (distance per unit of time)
ported as solutions of different surface Take each specimen such that different
liquid travels along and/or through a fab-
tensions may yield different results. sets of (fabric) length and width yarns are
ric specimen is visually observed, manu-
ally timed and recorded at specified inter- 5.4 Dark fabric colors or prints and de- present.
vals. signs may be difficult to test. The use of a 7.4 Cut three specimens at least 165 ±
soluble ink of a contrasting color may 3 × 25 ± 3 mm with the long dimension
help in making the marks more clearly parallel to the fabric direction(s) chosen
3. Terminology
visible. to be tested. For length direction testing,
3.1 fabric, n.—in textiles, a planar 5.5 The procedure measures the time align the long direction of the template
structure made from yarns or fibers and distance water will move up from the with the warp yarns (wales); for width di-
(ASTM D123 and see 13.4). cut edge of a specimen, but does not du- rection testing, align the long direction of
3.2 vertical wicking, n.—in a textile plicate an end-product’s exposure during the template along the filling yarns
held vertically, the upward movement of wear. (courses). Cut an extra specimen to deter-
liquid from a cut edge. 5.6. The results obtained by this test mine water level in the flask or beaker

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM197-2011e2(2018)e 405
Copyright © 2020 American Association of Textile Chemists and Colorists
before starting the testing (see 9.2.4). amount of water required may be added
7.5 If testing the durability of finishes to a flask as instructed in 9.2.4 for deter-
or evaluating wicking properties after mining and marking a water level fill line
laundering, take specimens as described on the outside of a flask. After a speci-
in 7.4 from fabric swatches that have men is suspended in the flask, a pipette
been laundered according to conditions can be used to raise the water level to the
chosen from the AATCC LP1. appropriate height.
9.2.8 Use a clean flask with fresh water
for testing subsequent samples.
8.Conditioning
9.2.9 Start stopwatch or timer as soon
8.1 Prior to testing, condition the speci- as the water reaches the 5 ± 1 mm line
mens as directed in ASTM D1776, Stan- and the soluble ink begins to migrate up-
dard Practice for Conditioning and Test- 150 mm wards. Monitor the rise of the water.
ing Textiles (see 13.4). Condition Record the time, to the nearest second,
specimens for at least 4 h in an atmo- that it takes for the soluble ink at the
sphere of 21 ± 2°C (70 ± 4°F), 65 ± 5% marked 20 ± 1 mm line to start to mi-
RH by laying each test specimen sepa- grate. Continue monitoring the rise of the
rately on a screen or perforated shelf of a water and record to the nearest second the
conditioning rack. time and distance that the test was termi-
8.2 Perform all tests in the standard at- nated.
mosphere for testing. 9.2.10 The test should be terminated if
20 the water does not wick to either the 20 ±
mm 1 mm line in 5.0 ± 0.1 min or if the total
9. Procedure time of the water to wick to the 150 ± 1
5 mm
9.1. If necessary, the surface tension of 25 mm mm line exceeds 30.0 ± 0.1 min. In either
the chosen liquid (including tinted water case, measure the distance the water has
or dye solution) should be measured as migrated and the time that the test was
Fig. 1—Vertical wicking stopped. Record the time and distance
directed in ASTM D1331-89, Standard specimen and marking.
Test Methods for Surface and Interfacial and the reason for termination of the test.
Tensions of Solutions of Surface-Active 9.2.11 Remove the specimen from the
Agents (see 13.4) and reported. flask.
9.2 Option A—Measure time at a Straight pin line 9.2.12 Repeat steps 9.2.2 through
given distance. 9.2.11 for the remaining specimens.
9.2.1 Using a marking pen with soluble 9.3 Option B—Measure distance at a
ink, mark a line across the end of each given time.
specimen at a distance of 5 ± 1 mm from 9.3.1 Place a ruler vertically against the
the end on the fabric side to be tested. back of the elongated pan (see Fig. 3) in-
The 5 mm line denotes the level to which Second test line side the box so that the ruler touches the
a specimen is to be lowered into the water
(150 mm) bottom. Fill the elongated pan with dis-
in the flask or beaker which is the test tilled or deionized water to a depth of 38
start time. ± 2 mm (1.5 ± 0.1 in.) water.
9.2.2 Using a marking pen with soluble 9.3.2 Remove the ruler from the back
ink, measure from the 5 ± 1 mm line, and of the pan. Secure the ruler with tape on
mark lines across the width of the speci- the outside of the pan so that the top of
men at distances of 20 ± 1 and 150 ± 1
First test line the water surface is at the “0” mm mark
(20 mm)
mm (see Fig. 1). To facilitate the mea- on the ruler.
Water level line 9.3.3 Use double-sided tape to secure a
surement of wicking distances, intervals (5 mm)
of 10 ± 1 mm may be marked along the specimen to the top of the box so that the
specimen length between the 20 ± 1 mm bottom edge just touches the top surface
and 150 ± 1 mm lines. of the water (same as the “0” mm mark
9.2.3 Alternative wicking distances Fig. 2—Vertical alignment on the ruler) and start the stopwatch or
may be used depending on the desired test configuration. timer immediately.
end use of the fabric. When comparing 9.3.4 Some light weight woven, knit-
results, the same wicking distance bench-
of soluble ink marks on the specimen.
marks should be used.
9.2.4 To determine the amount of water 9.2.5 Some light weight woven, knit-
for the test, use the extra specimen and ted, or hydrophobic fabrics may float on
position it at the opening of an Erlen- the water, in which case, a small paper
meyer flask (which may be placed on a clip or clamp may be attached to the end
scissor jack) by the insertion of a straight of the specimen that is to be submerged.
pin or other device near the end of the If a paper clip or clamp is used, it should
specimen (see Fig. 2). Allow the speci- be noted in the report (see 11.1.1).
men to hang into the flask. Add water up 9.2.6 Fill the flask with distilled or
to the level at which the specimen’s 5 ± 1 deionized water to the line marked as in-
mm line is reached and then mark the re- structed in 9.2.4. Insert the specimen into
quired water level on the outside of the the flask, or raise the scissor jack to posi-
flask. Special care should be taken to in- tion the specimen so that the water is at
sure that the lip and the neck of the flask the 5 ± 1 mm line.
remain dry to prevent premature bleeding 9.2.7 Alternatively, the approximate Fig. 3—Multiple specimen elongated pan.

406 AATCC TM197-2011e2(2018)e AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists
ted, or hydrophobic fabrics may float on mm line from the distance that the water tion. Table I shows the means and confi-
the water, in which case, a small paper has reached in 30.0 ± 0.1 min. or, dence intervals for each fabric in the
clip or clamp may be attached to the end (Option B) from the distance the water length direction. Table II shows the
of the specimen that is to be submerged. has wicked in 10.0 ± 0.1 min. means and confidence intervals for each
If a paper clip or clamp is used, it should fabric in the width direction.
be noted in the report (see 11.1.1). 12.1.3 Interlaboratory Study for Op-
11. Report and Interpretation
9.3.5 Monitor the rise of the water. At tion B. Tests for wicking of textiles using
2.0 ± 0.1 min, use a ruler to measure the 11.1 Report the direction(s) and side(s) vertical orientation were conducted in
distance that the water has wicked. of the sample tested. 2010, with one laboratory, two operators,
Record the distance in millimeters. At 11.1.1 Report the wicking times, wick- and four samples. The four samples used
10.0 ± 0.1 min, use a ruler to measure the ing distances, average wicking times, cal- in the study were (a) cotton pique, (b)
distance that the water has wicked. culated wicking rates, whether short pe- polyester jersey, (c) polyester mesh, and
Record the distance in millimeters. riod or long period, and whether a paper (d) polyester/spandex rib.
9.3.6 Alternative wicking times may clip or clamp was attached to the bottom 12.1.4 The analysis of variance tech-
be used depending on the desired end use of the test specimens. nique was applied to the different data
of the fabric. When comparing results, 11.1.2 If the test was terminated by sets (length and width directions). The
the same wicking time benchmarks reaching the marked distance(s) or the analyses are being retained for reference
should be used. maximum time was exceeded, report the at the AATCC Technical Center. In the
9.3.7 The test should be terminated if distance wicked and the time the test was analyses of variance, the operators as a
the water does not wick any distance in terminated. source of variation were not found to be
10.0 ± 0.1 min or if the total time of the 11.2 Report if a solution other than dis- significant. Table III shows the means
water to wick to the end of the specimen tilled or deionized water at 21 ± 2°C (70 and confidence intervals for each fabric
exceeds 30.0 ± 0.1 min. In either case, ± 4°F) was used and its surface tension in the length direction. Table IV shows
measure the distance the water has mi- and temperature. the means and confidence intervals for
grated and the time that the test was 11.3 Report if testing was performed each fabric in the width direction.
stopped. Record the time and distance after laundering, the laundering condi- 12.1.5 Between-laboratory precision
and the reason for termination of the test. tions used and the number of launderings has not been established for this test
9.3.8 Remove the specimen from the completed. method. Until such precision informa-
flask. 11.4 The 20 mm mark, or the 5.0 min tion is available, users of the method
9.3.9 Repeat steps 9.3.1-9.3.8 for the time, may provide data on initial wicking should use standard statistical techniques
remaining specimens. and the 150 mm mark, or the 30.0 min. in making any comparison of test results
time, may provide data on extended for between-laboratory averages.
10. Calculation wicking. The two levels of vertical wick- 12.2 Bias. The true value of vertical
ing ability may be used as indicators to wicking rates of textile fabrics can be de-
10.1 Calculate the vertical wicking differentiate performance. fined only in terms of a test method.
rates. Two different rates, a short period There is no independent method for de-
rate and a long period rate, are obtained termining the true value. In estimating
12. Precision and Bias
for each sample. this property, the test method has no
10.1.1 Vertical wicking rate is calcu- 12.1 Precision. known bias.
lated by dividing the wicking distance by 12.1.1 Interlaboratory Study for Op-
the wicking time as shown in formula 1. tion A. Tests for wicking of textiles using
vertical orientation were conducted in 13. Notes
W = d/t (Eq. 1)
2009, with one laboratory, three opera- 13.1 Available from AATCC, P.O. Box
where: tors, and five samples. The five samples 12215, Research Triangle Park NC 27709; tel:
W = wicking rate, mm/s used in the study were (a) 100% cotton +1.919.549.8141; fax: +1.919.549.8933; e-mail:
d = wicking distance, mm jersey knit, (b) 100% cotton interlock ordering@aatcc.org; web site: www.aatcc.org.
t = wicking time, s knit, (c) 100% polyester woven, (d) 13.2 A suitable marking pen contains ink
100% cotton twill weave, and (e) 50/50 that is water soluble, available commercially
10.1.2 The short period rate is calcu- cotton/polyester blend woven. such as Paper Mate® Flair® Fiber Tip Pen from
lated: 12.1.2 The analysis of variance tech- Sanford Corporation, 2707 Butterfield Rd., Oak
(Option A) from the time it takes to nique was applied to the eight different Brook IL 60523; tel: +1.630.481.2200; fax: +1.
reach the 20 ± 1 mm line or, from the dis- data sets. The analyses are being retained 866.666.8735; web site: www.papermate.com.
tance the water has wicked in 5.0 ± 0.1 for reference at the AATCC Technical 13.3 A suitable device that will function as
min. or, Center. In the analyses of variance, the a specimen holder is a ring stand with a hori-
(Option B) from the distance the water zontal bar. An optional device to automati-
operators as a source of variation were cally lower the specimen into solution is a
has wicked in 2.0 ± 0.1 min. not found to be significant in all cases ex- pneumatic cylinder incorporated into the spec-
10.1.3 The long period rate is calcu- cept for testing in the width direction, imen holder.
lated: when the measurement was made at the 13.4 Available from ASTM International,
(Option A) from the time it takes to long period, in testing either in the flask 100 Barr Harbor Dr., W. Conshohocken PA
reach the 150 ± 1 mm line or, for those or in the elongated pan. The fabrics were 19428; tel: +1.610. 832.9500; fax: +1.610.832.
specimens that have not reached the 150 found to be a significant source of varia- 9555; web site: www.astm.org.

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM197-2011e2(2018)e 407
Copyright © 2020 American Association of Textile Chemists and Colorists
Table I—Summary of Statistics (OPTION A)—Length Direction (rate in mm/s)
Jersey Interlock Polyester Woven Cotton Woven Poly/Cotton Woven
ELONGATED PAN METHOD SHORT PERIOD
Mean 1.6 0.2 2.6 1.4 0.3
Standard Deviation 0.5 0.1 0.9 0.4 0.1
Count 18 18 18 18 18
Confidence Level (95.0%) 0.3 0.0 0.4 0.2 0.1
FLASK METHOD SHORT PERIOD
Mean 1.4 0.4 2.6 1.3 0.3
Standard Deviation 0.4 0.1 0.7 0.6 0.0
Count 18 18 18 18 18
Confidence Level (95.0%) 0.2 0.1 0.4 0.3 0.0
ELONGATED PAN METHOD LONG PERIOD
Mean 0.1 0.0 0.1 0.1 0.1
Standard Deviation 0.0 0.0 0.0 0.0 0.0
Count 18 18 18 18 18
Confidence Level (95.0%) 0.0 0.0 0.0 0.0 0.0
FLASK METHOD LONG PERIOD
Mean 0.1 0.0 0.1 0.1 0.1
Standard Deviation 0.0 0.0 0.0 0.0 0.0
Count 18 18 18 18 18
Confidence Level (95.0%) 0.0 0.0 0.0 0.0 0.0

Table II—Summary of Statistics (OPTION A)—Width Direction (rate in mm/s)


Jersey Interlock Polyester Woven Cotton Woven Poly/Cotton Woven
ELONGATED PAN METHOD SHORT PERIOD
Mean 1.9 0.9 2.3 1.0 0.3
Standard Deviation 0.7 0.2 0.7 0.3 0.1
Count 18 18 18 18 18
Confidence Level (95.0%) 0.3 0.1 0.4 0.1 0.1
FLASK METHOD SHORT PERIOD
Mean 1.8 1.0 2.2 1.2 0.2
Standard Deviation 0.6 0.4 0.7 0.7 0.1
Count 18 18 18 18 18
Confidence Level (95.0%) 0.3 0.2 0.4 0.3 0.1
ELONGATED PAN METHOD LONG PERIOD
Mean 0.1 0.1 0.1 0.1 0.0
Standard Deviation 0.0 0.0 0.0 0.0 0.0
Count 18 18 18 18 18
Confidence Level(95.0%) 0.0 0.0 0.0 0.0 0.0
FLASK METHOD LONG PERIOD
Mean 0.1 0.1 0.1 0.1 0.0
Standard Deviation 0.0 0.0 0.0 0.0 0.0
Count 18 18 18 18 18
Confidence Level (95.0%) 0.0 0.0 0.0 0.0 0.0

Table III—Summary of Statistics (OPTION B)—Length Direction (rate in mm/s)


Cotton Pique Polyester Jersey Polyester Mesh Polyester/Spandex Rib
SHORT PERIOD
Mean 0.44 0.45 0.61 0.50
Standard Deviation 0.02 0.07 0.03 0.03
Count 20 20 20 20
Confidence Level (95.0%) 0.02 0.07 0.02 0.02
LONG PERIOD
Mean 0.14 0.18 0.20 0.18
Standard Deviation 0.003 0.01 0.01 0.01
Count 20 20 20 20
Confidence Level (95.0%) 0.003 0.01 0.01 0.01

Table IV—Summary of Statistics (OPTION B)—Width Direction (rate in mm/s)


Cotton Pique Polyester Jersey Polyester Mesh Polyester/Spandex Rib
SHORT PERIOD
Mean 0.42 0.46 0.58 0.57
Standard Deviation 0.03 0.07 0.03 0.05
Count 20 20 20 20
Confidence Level (95.0%) 0.02 0.07 0.03 0.04
LONG PERIOD
Mean 0.13 0.18 0.19 0.20
Standard Deviation 0.01 0.01 0.01 0.01
Count 20 20 20 20
Confidence Level (95.0%) 0.01 0.01 0.01 0.01

408 AATCC TM197-2011e2(2018)e AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists
AATCC TM198-2011e3(2020)

Test Method for Horizontal Wicking of Textiles


Foreword (ASTM D123 and see 14.3). deionized water (tinted water, dye solu-
3.2 horizontal wicking, n.—in tex- tions, etc.) may be used to evaluate the
Historically, the textile industry has tiles, the movement of liquid across the wicking of textiles. If a liquid other than
utilized many different test procedures horizontal plane of a textile from a site water is chosen, its surface tension
for determining the wicking characteris- where a specific volume has been ap- should be measured and reported as solu-
tics of textile fabrics, i.e., the movement plied. tions of different surface tensions may
of water or liquid through fabrics. Within 3.3 horizontal wicking rate, n.—the yield different results.
the last decade, the industry has devel- change in the area of the liquid with re- 5.4 Dark fabric colors or prints and de-
oped new technologies that have changed spect to time as the liquid travels through signs may be difficult to test. The use of a
water movement and absorbency re- a textile. soluble ink of a contrasting color may
sponses of textiles leading to the use of 3.4 wicking, n.—in textiles, the move- help in making the liquid more clearly
the labeling term “moisture manage- ment of a liquid, by capillary action, visible.
ment” to describe these phenomena. along or through a material.
While, traditionally, wicking tests mea- 5.5 The results obtained by this test are
3.5 wicking distance, n.—the linear not a measure of comfort which is be-
sured the movement of liquids through measurement that the liquid travels along
the vertical plane of fabrics (commonly yond the scope of this method.
or through a textile from a starting point 5.6 The relationship between vertical
referred to as vertical wicking), (see to a stopping point.
AATCC TM197, Test Method for Verti- and horizontal wicking test results is not
3.6 wicking time, n.—the measurable known. Caution should be used when
cal Wicking of Textiles), the improve- period during which liquid travels along
ments in the last decade have also led to comparing results using different align-
or through a textile. ments.
an interest in measuring the movement of
liquids across the horizontal plane of fab- 4. Safety Precautions
ric surfaces (horizontal wicking). Many 6. Apparatus, Reagents, Materials
interested groups (textile manufacturers, NOTE: These safety precautions are
chemical suppliers, and retailers, as well for information purposes only. The pre- 6.1 Distilled or deionized water at 21 ±
as independent testing laboratories) par- cautions are ancillary to the testing proce- 2°C (70 ± 4°F).
ticipated in the efforts to standardize test dures and are not intended to be all inclu- 6.2 Marking pens, with fine point, per-
methods to measure the vertical and hori- sive. It is the user’s responsibility to use manent and soluble ink (see 14.2).
zontal wicking properties of fabrics with safe and proper techniques in handling 6.3 Stopwatch or digital timer.
moisture management attributes. materials in this test method. Manufac- 6.4 Tape or ruler, mm graduations.
Unofficial techniques for determining turers MUST be consulted for specific 6.5 Surface tensiometer, if using liquid
the absorbency and wicking properties of details such as material safety data sheets other than water (see 10.1).
textile fabrics were published in the 2004 and other manufacturer’s recommenda- 6.6 Beaker or Petri dish.
AATCC/ASTM International’s Techni- tions. All OSHA standards and rules 6.7 Burette, 10 (± 0.05 mL) mL with
cal Supplement: A Compilation of Proce- must also be consulted and followed. 0.5 mL numbered graduations that allows
dures and Guidelines for Textile Products 4.1 Good laboratory practices should a delivery rate of 15-25 drops per millili-
and the 2008 AATCC/ASTM Interna- be followed. Wear safety glasses in all ter, or handheld electronic pipette.
tional’s Moisture Management Technical laboratory areas. 6.8 Embroidery hoop, 152 ± 5 mm (6.0
Supplement: Applicable to Apparel, Lin- ± 0.2 in.) diameter (see 14.1).
ens and Soft Goods (see 14.1). This test 5. Uses and Limitations
method is based on the testing procedures 6.9 Laboratory sealing film (optional).
for wicking published in those Technical 5.1 This method is primarily applica- 6.10 Ring stand and clamp.
Supplements. ble to fabrics that absorb the full volume 6.11 Template, 100 ± 3 mm diameter.
of the test liquid, without pooling on the
1. Purpose and Scope surface or allowing dripping. If the full 7. Sampling
volume of the test liquid is not available
1.1 This test method is used to evaluate to measure the wicking rate, inconsistent 7.1 Determine whether the fabric has a
the ability of horizontally aligned fabric results should be expected. Hence, the re- hydrophobic or hydrophilic side. Upon
specimens to transport liquid along and/ sults obtained on fabrics that fully absorb agreement between interested parties, de-
or through them, and is applicable to wo- the test liquid cannot be compared with termine whether both fabric sides are to
ven, knitted, or nonwoven fabrics. those obtained on fabrics that do not. In be tested. If only one fabric side is to be
addition, the movement of liquid within a tested, mark the selected side. If testing is
2. Principle fabric may be influenced by fiber con- to be performed after laundering, use a
tent, fabric construction, mechanical or marking pen with permanent ink to de-
2.1 The rate (area per unit of time) liq- chemical processing or a combination of note the fabric side chosen for testing.
uid travels through a fabric specimen is these. 7.2 All specimens should be cut at least
visually observed, manually timed and 5.2 This method evaluates the wicking 100 ± 5 mm from the selvage. If testing
recorded at specified intervals. ability of horizontally aligned test speci- garments, take specimens from different
mens to distilled or deionized water. In garment panels away from seams, pock-
3. Terminology this test, wicking may be influenced by ets, plackets or other assembly features.
the properties of the test liquid, but not by Each specimen shall be taken so that dif-
3.1 fabric, n.—in textiles, a planar gravity. ferent sets of length and width yarns are
structure made from yarns or fibers 5.3 Liquids other than distilled or present.

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM198-2011e3(2020) 409
Copyright © 2020 American Association of Textile Chemists and Colorists
8. Specimens Agents (see 14.3) and reported. determined in 10.3.1, and dispense 1.0 ±
10.2 Use a template and a fine-point 0.1 mL of water from the 10 ± 1 mm
8.1 Cut five specimens, 200 × 200 ± 5 marking pen with soluble ink to mark a height onto the center of the 100 ± 3 mm
mm, aligned with the fabric selvage or 100 ± 3 mm diameter circle in the middle marked circle. A handheld electronic pi-
longitudinal alignment of the garment of each specimen. Mark the circle on the pette may be used instead of a burette but
panels. For testing horizontal wicking of side of the fabric to be tested. The place- the same height of 10 ± 1 mm from the
garment samples, it may not be necessary ment of the water volume for the test is to fabric surface should be maintained. Im-
to cut out individual specimens. be in the center of the circle (see Fig. 1). mediately after opening the stopcock or
8.2 Cut an extra specimen from either pressing the dispense button, start the
10.3 Fill a 10.0 mL burette with dis-
fabric or garment samples to determine timer. The test should be terminated
tilled or deionized water and lower the
placement of the drop in the center of the when the water reaches the 100 ± 3 mm
water level to the top graduation level,
marked circle before starting the testing circle. Record the distance the liquid has
sighting to the bottom of the meniscus.
(see 10.2). spread in the length and width direction
8.3 If testing the durability of finishes 10.3.1 Insert a trial specimen into an
embroidery hoop, ensuring that its sur- of the fabric and the time elapsed.
or evaluating wicking properties after 10.6 The test should be terminated if
laundering, take specimens as described face is taut, without creases or wrinkles.
Place the embroidery hoop horizontally the water stops migrating and does not
in 8.1 from fabric swatches that have reach the 100 ± 3 mm circle in 5 ± 0.1
been laundered according to conditions on the top of the beaker or Petri dish.
Lower the burette so that the tip is 10 ± 1 min. Record the time that the test was ter-
chosen from the AATCC LP1. minated.
mm above the fabric surface. Slowly
open the burette stopcock to verify that 10.7 Repeat steps 10.4-10.6 for each
9. Conditioning 1.0 ± 0.1 mL volume of water can be dis- remaining specimen.
9.1 Condition specimens for at least 4 pensed into the center of the marked cir-
h in an atmosphere of 21 ± 2°C (70 ± cle. Determine (and record) the approxi- 11. Calculation
4°F), 65 ± 5% RH prior to testing accord- mate position of the stopcock opening
that ensures a consistent delivery of the 11.1 Record the time to the nearest sec-
ing to ASTM D1776, Standard Practice ond for each specimen.
for Conditioning and Testing Textiles (see test liquid, i.e., the position that permits
delivery of the specified number of drops 11.2 Calculate the horizontal wicking
14.3). rate for each specimen and the average
9.2 Perform all tests in the standard at- of the test liquid in 10 ± 2 s. Discard the
trial specimen. wicking rate for each sample. Use for-
mosphere for testing. mula 1 below for the calculation of hori-
10.4 Insert test specimen into the em-
broidery hoop with the chosen fabric side zontal wicking rate:
10. Procedure
to be tested facing up for exposure to the
water. The use of laboratory sealing film W = π(1/4)(d1)(d2)/t (Eq. 1)
10.1 If necessary, the surface tension of
the chosen liquid (including tinted water on the embroidery hoop ring surfaces where:
or dye solution) should be measured as may be utilized to prevent slippage of W = wicking rate, mm2/s
directed in ASTM D1331-89, Standard light weight fabric and help maintain a d1 = wicking distance in length direc-
Test Methods for Surface and Interfacial taut fabric surface. tion, mm and d2 = wicking dis-
Tensions of Solutions of Surface-Active 10.5 Open the stopcock, to the position tance in width direction, mm
t = wicking time, s

11.3 The wicking rate can be calcu-


lated from either the time it takes to reach
the edge of the circle or the distance trav-
eled in the 5.0 ± 0.1 min time period.

12. Report and Interpretation


12.1 Report the wicking time, the
wicking distance in the length and width
Burette – Tip of burette 10 mm above direction, and the average wicking rate
specimen surface for each sample. Report any dripping or
pooling of test liquid.
12.2 Report if a solution other than dis-
tilled or deionized water at 21 ± 2°C (70
Embroidery hoop with ± 4°F) was used and its surface tension
200 × 200 mm specimen and temperature.
12.3 Report if testing was performed
after laundering, the laundering condi-
tions used and the number of launderings
Beaker – 2L to accommodate
completed.
152 mm diameter embroidery hoop 12.4 Shorter horizontal wicking times
indicate faster wicking (see 5.1 and 5.5).

13. Precision and Bias


13.1 Precision.
13.1.1 Interlaboratory Study. Tests for
wicking of textiles using horizontal ori-
Fig. 1—Horizontal alignment test configuration. entations were conducted in 2009, with

410 AATCC TM198-2011e3(2020) AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists
one laboratory, three operators, and five ANOVA indicated that the effect due to Table II—Statistical Results
samples. The five samples used in the the fabric was significant, the results, (rate in mm2/s)1
study were: (a) 100% cotton jersey knit, shown in Table II, for each of the three
100% 100% 100%
(b) 100% cotton interlock knit, (c) 100% fabrics are separate. The analysis is being Cotton Cotton Cotton
cotton twill weave, (d) 50/50 cotton/poly- retained for reference at the AATCC Jersey Interlock Woven
ester blend woven, and (e) 100% polyes- Technical Center.
Average 53 23 78
ter woven. However, two of the woven 13.1.3 Between-laboratory precision Std Dev 13 6.0 50
samples (d and e) were found to be not has not been established for this test 95% CI 5.0 2.0 18
suitable for the measurement of horizon- method. Until such precision informa-
tal wicking, as water pooled on the sur- tion is available, users of the method 1
All values in this table are expressed with exactly two
face and did not spread during the test. should use standard statistical techniques significant figures.
Therefore, the single lab precision state- in making any comparison of test results
ment shown is based on only three fab- for between-laboratory averages.
rics: two knits and one woven. 13.2 Bias. The true value of horizontal
13.1.2 The data is shown in Table I. wicking rates of textile fabrics can be de- termining the true value. In estimating
The analysis of variance technique was fined only in terms of a test method. this property, the test method has no
applied to the data set. Because the There is no independent method for de- known bias.

14. Notes

Table I—Data (rate in mm2/s)1 14.1 Available from AATCC, P.O. Box
12215, Research Triangle Park NC 27709; tel:
Operator 1 Operator 1 Operator 2 Operator 2 Operator 3 Operator 3 +1.919.549.8141; fax: +1.919.549.8933; e-mail:
Day 1 Day 2 Day 1 Day 2 Day 1 Day 2 ordering@aatcc.org; web site: www.aatcc.org.
100% 14.2 A suitable marking pen contains ink
Cotton Jersey 40 60 37 39 44 68 that is water soluble, available commercially
34 57 84 70 56 62 such as Paper Mate® Flair® Fiber Tip Pen
41 32 51 60 59 61 from Sanford Corporation, 2707 Butterfield
64 47 68 48 41 60 Rd., Oak Brook IL 60523; tel: +1.630.481.
60 58 55 30 62 46 2200; fax: +1.866.666.8735; web site: www.
papermate.com.
100%
Cotton Interlock 29 25 24 40 23 22 14.3 Available from ASTM International,
28 22 25 16 19 19 100 Barr Harbor Dr., W. Conshohocken PA
27 17 35 29 19 22 19428; tel: +1.610. 832.9500; fax: +1.610.832.
16 19 31 20 21 19 9555; web site: www.astm.org.
37 14 18 18 27 20
100% 15. History
Cotton Woven 120 49 33 120 43 31
47 90 130 110 46 140 15.1 Reaffirmed 2020
47 45 130 170 38 35 15.2 Reaffirmed 2018, 2013. Editorially re-
76 66 160 220 44 29 vised and reaffirmed 2012. Editorially revised
98 51 43 71 27 43 2019, 2016.
15.3 Developed in 2011 by AATCC Com-
1
All values in this table are expressed with exactly two significant figures. mittee RA63.

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM198-2011e3(2020) 411
Copyright © 2020 American Association of Textile Chemists and Colorists
AATCC TM199-2013e(2018)e

Test Method for Drying Time of Textiles: Moisture Analyzer


Developed in 2011 by AATCC Commit- textile construction, fiber content, apparel chemical processing or a combination of
tee RA63; reaffirmed 2018; revised construction, finishes, the atmosphere in these aspects.
2012, 2013; editorially revised 2017, which the test is performed, and the vol- 5.2 Other factors that may influence
2019. ume challenge of the liquid. drying include the temperature and hu-
3.2 drying time, n.—the time it takes midity conditions of the test and the
for a specified amount of liquid to evapo- amount of liquid to be dried. This test
Foreword rate from a textile under controlled test- method is performed in non-standard tex-
Historically, the textile industry has ing conditions. tile testing conditions. Since this test can
utilized many different test procedures NOTE: In this test method the amount be performed at various temperature set-
for determining the drying characteristics of water is determined in a preparatory tings of the moisture analyzer, test tem-
of textile fabrics, whether those charac- step so that the specimen is wet-out to a peratures can be selected to simulate the
teristics are drying rate, time or some given level. The testing conditions are temperature of a human body at rest, dur-
other drying parameter. Within the last controlled by the analyzer. ing exercise, or when exposed to outdoor
decade, the industry has developed new 3.3 endpoint, n.—the point of termina- temperatures.
technologies that have resulted in an im- tion of a drying test that is either to the 5.3 This method is based on the appli-
provement in these characteristics, as one original dry weight of a specimen or cation of a controlled amount of water to
of many attributes associated with the use some other agreed value such as dry test specimens, measurement of the dry-
of the term “moisture management.” weight +4.0% moisture content. ing rate of that application, and calcula-
Many interested groups (textile manufac- 3.4 moisture retention, adj.—for this tion of the moisture retention based on
turers, chemical suppliers, retailers, as test method, the percent moisture reten- that application.
well as independent testing laboratories) tion of the specimen after being sub- 5.4 This method is limited to fabrics
participated in the effort to develop and merged in deionized water for 1 min, and with at least one side that exhibits an ab-
publish standard test methods to measure hanging vertically for 5 min in a con- sorbency time within 30 ± 2 s (see
the drying characteristics of fabrics. Un- trolled environment (see 9.3.2 and for- AATCC TM79, Test Method for Absor-
official techniques for determining the mula 1). bency of Textiles). It is not applicable to
drying properties of textile fabrics were 3.5 test side, n.—the side, either the fabrics that exhibit an absorbency of
published in the 2008 AATCC/ASTM In- face or back of a specimen, which is up- more than 30 s, as in such fabrics water
ternational’s Moisture Management Tech- permost when placed on the moisture bal- would begin evaporating from the surface
nical Supplement: Applicable to Apparel, ance analyzer support platform; the side of the fabric as the temperature is being
Linens and Soft Goods. This test method onto which the test volume of water is ap- raised, thereby skewing the results.
formalizes an additional technique that plied. 5.5 One possible use of this method is
has been used by several companies. 3.6 weight loss, n.—the difference be- to compare the moisture retention charac-
tween the saturated weight of a specimen teristics of untreated versus treated fab-
1. Purpose and Scope and the weight after drying. rics, or to compare the moisture retention
3.7 wet pick-up, n.—in textile pro- characteristics of a textile material with
1.1 This test method is intended to cessing, the amount of liquid, and mate- or without an additive.
evaluate the drying time of knit, woven rial carried by the liquid, applied to a tex- 5.6 The results obtained by this test are
or nonwoven fabrics at an elevated tem- tile. not a measure of comfort which is be-
perature using a gravimetric moisture an- yond the scope of this method.
alyzer. By performing the test at non- 4. Safety Precautions 5.7 The relationship between drying
standard textile testing conditions, it is time measured by this test and absor-
possible to simulate drying at body tem- NOTE: These safety precautions are
bency has not been defined. Although
perature or to perform testing at tempera- for information purposes only. The pre-
TM79 is used in the preparatory steps to
tures that simulate conditions of use. cautions are ancillary to the testing proce-
determine which side of a fabric should
dures and are not intended to be all inclu-
be used in testing, this test does not mea-
sive. It is the users’ responsibility to use
2. Principle sure absorbency.
safe and proper techniques in handling
2.1 Water is applied to the test speci- materials in this test method. Manufac-
men and then dried at a pre-selected tem- turers MUST be consulted for specific 6. Apparatus and Materials
perature (37° ± 2°C [99 ± 4°F]); if an al- details such as material safety data sheets 6.1 Moisture analyzer with a ceramic
ternative temperature is used it should be and other manufacturers’ recommenda- heating element and accurate to at least
reported, in an automated moisture ana- tions. All OSHA standards and rules 0.001 g (see 14.1).
lyzer. The time required for a test speci- must also be consulted and followed.
6.2 Deionized water.
men to reach a designated endpoint is 4.1 Good laboratory practices should
measured and recorded as the drying be followed. Wear safety glasses in all 6.3 Vertical specimen stand. The stand
time. laboratory areas. should have a horizontal hanger of suit-
able size to hang the specimen using
binder clips. (see Fig. 2).
3. Terminology 5. Uses and Limitations 6.4 Tweezers.
3.1 drying rate, n.—the change in vol- 5.1 The drying of a fabric may be in- 6.5 400 mL beaker.
ume per unit time of a liquid that evapo- fluenced by fiber content, fabric con- 6.6 Wire screen—standard 0.25 × 0.25
rates from a textile. struction (e.g., thickness or raised sur- in. mesh (see 14.2).
NOTE: Drying rate is dependent upon face, such as fleece), mechanical or 6.7 Specimen support platform (see

412 AATCC TM199-2013e(2018)e AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists
Fig. 3).
6.8 Electronic motorized pipette with
2.5 mL tip, and a dispensing speed of 4
mL/min (see 14.1).
6.9 Computer with software for data
capture (optional).

7. Specimens
7.1 Cut ten 70 ± 1 mm round speci-
mens diagonally across the width of a
sample, to ensure that different sets of
length and width yarns are in each speci- Fig. 3—Specimen support platform.
men or from different sites from a prod-
uct are taken. If the sample being tested is
not large enough to cut ten 70 ± 1 mm di-
ameter specimens across the width, it is
acceptable to test a smaller specimen
size, but must be reported with the test re-
sults. Two of the specimens are to be
used for the preliminary steps, and eight
are for the testing (see Section 9).

8. Conditioning
8.1 Place the specimens on a flat
smooth, horizontal surface without tension
before testing. Condition them to moisture
equilibrium in a standard atmosphere for
Fig. 2—Vertical specimen stand.
testing according to ASTM D1776, Stan- Fig. 4—Placement of specimen
dard Practice for Conditioning and Testing on support platform.
Textiles, Table I, Textiles, General (see
14.3). the specimen in water, as shown in Fig. 1.
9.3.1 Using tweezers, remove the spec-
9. Preparation imen after 1 min and hang on the vertical
stand, as shown in Fig. 2.
9.1 Turn on the moisture analyzer to 37 9.3.2 After 5 min, remove the speci-
± 2°C (99 ± 4°F) and allow it to warm up men with tweezers. Weigh and record the
for at least 30 min. specimen weight (W2). Use formula 1 to
9.2 Using TM79, place a drop of water determine the moisture retention.
on the face of an extra fabric specimen to
judge absorbency; on the back of another Moisture Retention (%) =
extra specimen, repeat to determine W2 – W1
which is the most absorbent side to use -------------------- * 100 (Eq. 1)
for testing. If there is no difference, either W1
side can be used for testing by this where: Fig. 5—Placement of
method. If both sides of the specimen W1 = dry weight, in g wire screen on top of specimen.
have absorbency times greater than 30 s, W2 = saturated weight, in g
see 5.4.
9.3 Weigh and record the original Use formula 2 to determine the amount
9.5 Follow the manufacturer’s instruc-
weight (W1) of the specimen. Submerge of water to add to the fabric:
tion for setting the program operation.
x *W The test endpoint should be agreed upon
y = --------------1- (Eq. 2) by interested parties.
100
where: 10. Procedure
y = amount of water to add, in mL
x = moisture retention (see result of 10.1 Open the sample chamber and
formula 1) place the support platform and wire
W1 = dry weight, in g screen in the sample chamber (as shown
in Fig. 3).
NOTE: This equation assumes the den- 10.2 Tare the moisture analyzer. Place
sity of water is 1 g/mL at 25°C (77°F). the specimen with the selected test side
9.4 Set the electronic motorized pipette up on the support platform (see Fig. 4).
to pickup and dispense the calculated 10.3 Using an electronic motorized pi-
amount of water determined in 9.3. This pette, apply the specified amount of
amount will be used for all specimens deionized water in a uniform manner
from a sample without regard to variation over the surface of the specimen.
in weight of individual specimens from 10.4 Place the wire screen on top of the
Fig. 1—Submersion of specimen in water. the same sample. specimen (see Fig. 5) and start the ana-

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM199-2013e(2018)e 413
Copyright © 2020 American Association of Textile Chemists and Colorists
lyzer and software (if applicable). The age drying time and standard deviation, and (e) 100% polyester interlock knit.
moisture analyzer or the software will au- amount of water applied, temperature, 13.2 Table I Statistical Summary. Data
tomatically terminate the test when the and the end point. includes mean drying time, standard de-
selected endpoint is reached. 12.2 If the specimens tested were not viation and the 95% confidence level for
10.5 Repeat 10.1-10.4 for remaining 70 ± 1 mm in diameter, report the speci- both operators.
specimens. men diameter used. 13.3 Between-laboratory precision has
10.6 Record the drying time to the not been established for this test method.
nearest minute for each specimen. Until such precision information is avail-
13. Precision and Bias
able, users of the method should use stan-
11. Calculations and Evaluation dard statistical techniques in making any
13.1 Precision. Tests for drying time of
11.1 Calculate the average drying textiles using a moisture analyzer were comparison of test results for between-
time and the standard deviation for the conducted in 2010, with one laboratory, laboratory averages.
sample. two operators, and five samples. The five 13.4 Bias. The true value of the drying
samples used in this study were (a) 100% time of textile fabrics can be defined only
12. Report cotton interlock knit, (b) 100% polyester in terms of a test method. There is no in-
twill weave, (c) 100% cotton jersey knit, dependent method for determining the
12.1 Report moisture retention, aver- (d) 65/35 polyester/cotton blend woven, true value. In estimating this property, the
test method has no known bias.

Table I—Statistical Summary Data 14. Notes


Operator 1 Operator 2 14.1 These items may be obtained from any
Drying Time Mean Drying Mean Drying lab equipment supplier.
by Fabric Time, min Std Dev 95% CI Time, min Std Dev 95% CI 14.2 This item may be obtained from any
A 147 4.7 3 158 5.2 4 hardware or home improvement store.
B 115 4.2 3 121 4.5 3 14.3 Available from ASTM International,
C 73 2.5 2 78 2.6 2 100 Barr Harbor Dr., W. Conshohocken PA
D 28 1.7 1 28 1.3 1 19428; tel: +1.610. 832.9500; fax: +1.610.832.
E 85 1.8 1 93 3.5 2 9555; web site: www.astm.org.

414 AATCC TM199-2013e(2018)e AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists

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