LEARNING ACTIVITY NO.

10

PREPARATION ANS STANDARDIZATION OF HCI

SOLUTION
PROCEDURE:

1. 2 3 4

Add 10.5 mL of HCL Pour the HCL solution into stock bottle
Pour around 50 ml of Add enough distilled water to
distilled water into 250 cautiously and gradually complete the volume to 250
ml volumetric flask. shaking after addition. mL.

1. STANDARDIZATION OF HCI 5.
SOLUTION
Weight accurately 0. 125g of anhyrous
Label and preserve for future use.
sodium carbonate that previously has has
NOTE: Solution should be restandardized
heated at a temperature of about 270 C
prior use.
for one hour in a previously tared
Erlenmeyer flask.

4 5
2 3

Dissolve the sodium carbonate in 20 ml
distilled water and shake until the
solution is complete. Add 2 drops of
methyl orange.
Titrate with HCL solution to faintly pink.
Determine the normality of HCI
Heat again to boiling and titrate further Perform 2 Determination
solution
as necessary until the faint pink color is
no longer affected by continued boiling.
Calculate the normality.
 LEARNING ACTIVITY NO. 11

PREPARATION ANS STANDARDIZATION OF NaOH

SOLUTION
PROCEDURE:

1. 2 3 4 5. 6

Weigh roughly 20 g of Add distilled water to Pour the NaOH solution Rinse the beaker with dd enough distilled water Store the solution in a
NaOH in a previously dissolve the NaOH into a 1 L volumetric flask distilled water and pour to complete the volume to 1 L stock bottle.
tared the rinsing into 1 1L
small beaker L volumetric flask

3 2 STANDARDIZATION OF NaOH 7
1.
SOLUTION
Add 2 drops of Add 40 ml of distilled water Label properly
From the Geisslerburet, run
phenolphthalein
down 20 ml of standard HCI
solution

6
4 5

Determine the normality of HCI

Titrate the NaOH using Mohr buret to Perform 2 determinations
solution
light pink color and point.