Quantachrome?ASiQwin?

Automated Gas Sorption Data

Acquisition and Reduction
ⓒ 1994-2017, Quantachrome Instruments
version 5.2

Analysis Report
Operator: SSU Date:2024/04/08 Operator: a
Date:2024/04/10
Sample ID: a Filename: 240408_H1.qps
Sample Desc: Comment: N2- micro/mesopore analysis-
general
Sample Weight: 0.0888 g Instrument: Autosorb iQ Station 1
Outgas Time: 0.0 hrs Outgas Temp.: 0 캜
Analysis gas: Nitrogen Non-ideality: 6.58e-05 1/Torr CellType:
9mm w/o rod
Analysis Time: 10:36 hr:min Bath temp.: 77.35 K
Analysis Mode: Standard VoidVol
Remeasure:off
VoidVol. Mode: He Measure Cold Zone V: 5.79984 cc Warm Zone V:
14.8474 cc
Data Reduction Parameters
Thermal Transpiration: onEff. mol. diameter (D): 3.54 휛 ff. cell
stem diam. (d): 4.0000 mm

t-Method Calc. method: de Boer

BJH/DH method Moving pt. avg.: off Ignoring P-tags below 0.35 P/Po
Adsorbate modelNitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 ?2 Liquid
Density: 0.808 g/cc

Diameter Pore Volume Pore Surf dV(d) dS(d) dV(logd)

dS(logd)
Area
nm cc/g m?g cc/nm/g m?nm/g cc/g
cc/g

3.4164 5.5186e-03 6.4613e+00 1.4430e-02 1.6895e+01

1.1339e-01 1.3276e+02
3.8303 1.1138e-02 1.2329e+01 1.2615e-02 1.3174e+01
1.1113e-01 1.1606e+02
4.3145 1.6633e-02 1.7424e+01 1.0508e-02 9.7419e+00
1.0426e-01 9.6663e+01
4.8957 2.2131e-02 2.1916e+01 8.5970e-03 7.0241e+00
9.6775e-02 7.9069e+01
5.6231 2.4156e-02 2.3357e+01 2.4843e-03 1.7672e+00
3.2110e-02 2.2841e+01
6.5569 2.9193e-02 2.6430e+01 4.7868e-03 2.9201e+00
7.2114e-02 4.3993e+01
7.8115 3.4719e-02 2.9259e+01 3.7932e-03 1.9424e+00
6.8028e-02 3.4835e+01
9.5869 4.0295e-02 3.1586e+01 2.6628e-03 1.1110e+00
5.8546e-02 2.4428e+01
12.3325 4.6368e-02 3.3556e+01 1.7877e-03 5.7984e-01
5.0443e-02 1.6361e+01
17.3255 5.0200e-02 3.4440e+01 5.8154e-04 1.3426e-01
2.2917e-02 5.2910e+00
27.6197 5.8567e-02 3.5652e+01 5.9763e-04 8.6551e-02
3.7179e-02 5.3845e+00
 173.3417 9.6773e-02 3.6534e+01 1.3771e-04 3.1777e-03
4.0009e-02 9.2325e-01

BJH desorption summary

Surface Area = 36.534 m?g

Pore Volume = 0.097 cc/g
Pore Diameter Dv(d) = 3.416 nm