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User Manual
21-10890-1
List of Safety Symbols
Safety Symbol Meaning
Caution - General
(Reference ISO 7000-0434B, 2004-01)
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Quest Heated Puck
User Manual
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Table of Contents
1. INTRODUCTION ............................................................................ 5
2. SAFETY .......................................................................................... 6
3. SPECIFICATIONS & PART NUMBERS ........................................ 8
3.1 SPECIFICATIONS ............................................................................ 8
3.2 PART NUMBERS ............................................................................. 8
3.3 SPARE PARTS................................................................................ 8
4. UNPACKING AND CHECKLIST .................................................... 9
5. RECOMMENDED SAMPLING PROCEDURES .......................... 10
5.1 VOLATILES COVER ....................................................................... 10
5.2 BACKGROUND SPECTRUM ............................................................ 10
5.3 BEST PRACTICE FOR RECORDING AN FTIR SPECTRUM WITH THE HEATED
PUCK .......................................................................................... 10
5.4 TEMPERATURE OVERSHOOT......................................................... 11
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Introduction
Important Information! This symbol indicates it is important to
read all associated information in the accessory manual before
operating the device.
The heated puck has been designed for use with the QuestTM ATR
accessory. Its primary function being, heating a test sample placed on the
optical aperture from ambient to a maximum of 110°C for elevated sample
temperature assessments. The puck temperature is controlled via the USB
Temperature Controller and supplied PC software.
Please consult manuals for additional supplied products that the Heated
Puck is intended to be used with (revision numbers 2I-523-214 - USB
Temperature Controller and 2I-10800 – Quest ATR accessory).
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Safety
WARNING! Hot Surface - nearby surface may get hot.
These surfaces should not be touched while in operation
or without appropriate PPE.
Do not use this equipment with any accessory it has not been specifically
designed or configured for use with. Contact your local authorized Specac
dealer or sales team for further information regarding the compatibility of
the controller and puck with other devices and 3rd party accessories.
No user serviceable parts. Specac Ltd and their authorised agents only are
permitted to carry out repairs.
Only clean with a soft, lightly dampened cloth. Do not use harsh and/or
abrasive cleaners on any Specac product. Consult Specac or their
authorised agent if in any doubt.
Always check before use that the safety protection provided by the
accessory has not been compromised or impaired. The controller should
be made inoperative and be secured against unintended operation if in any
doubt.
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The protection is likely to be impaired if for example the controller:
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Specifications & Part Numbers
1.1 Specifications
ATR Crystal: Extended Diamond or ZnSe (uncoated)
Sample volume: ~700 μL
Sample Types: Small Solids and Liquid
Operating Temperature: Ambient to 110 °C
Max Ramp Rate: ca. 10 °C min-1
Detector type: 4 Wire Pt RTD
Detector Sensitivity: ~1/3 DIN
Storage conditions: -20 to +60 °C
1.2 Part Numbers
Quest, Heated Puck and USB temperature Controller Bundle
GS10894 Extended Diamond
GS10895 Uncoated ZnSe
Heated Puck & USB temperature Controller (Requires Quest for use)
GS10890 Extended Diamond
GS10891 Uncoated ZnSe
Heated Puck (Requires Quest & USB temperature Controller for use)
GS10892 Extended Diamond
GS10893 Uncoated ZnSe
1.3 Spare Parts
GS10503 Volatile Cover
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Unpacking and Checklist
On receipt of your product, please check that the following have been
supplied.
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Recommended Sampling Procedures
For cleaning and sample handling instructions please consult the Quest
Manual.
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and then wait 5-15 minutes for the system to equilibrate before recording a
background sample.
➢ For a liquid, fill sample well to the top, fit the volatiles cap (if required).
➢ For a solid, load your sample into the well and apply a load to ensure
good contact.
Then wait a further 5 minutes for your sample to equilibrate before
recording your spectrum.
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Worldwide Distribution
France Switzerland
Eurolabo - Paris. Portmann InstrumentsAG
Tel.01 42 08 01 28 Biel-Benken
Fax 01 42 08 13 65 Tel: 061 726 6555
email: Eurolabo@aol.com Fax: 061 726 6550
email: info@portmann-instruments.ch
Germany Website:www.portmann-instruments.ch
L.O.T. - Oriel GmbH & Co,
KG - Darmstadt USA
Tel: 06151 88060 SPECAC INC.
Fax: 06151 880689 414 Commerce Drive
email:info@LOT-Oriel.de Suite 175,
Website: www.LOT-Oriel.com/de Fort Washington,
PA 19034, USA
Japan Tel: 215 793 4044
Systems Engineering Inc. -Tokyo Fax: 215 793 4011
Tel: 03 3946 4993
Fax: 03 3946 4983 United Kingdom
email:systems-eng@systems-eng.co.jp Specac Ltd. - London
Website: www.systems-eng.co.jp Science and Innovation Centre,
Halo Business Park,
Spain Cray Avenue,
Teknokroma S.Coop C. Ltda Barcelona Orpington,
Tel: 93 674 8800 Kent BR5 3FQ
Fax: 93 675 2405 Tel: +44 (0) 1689 873134
email: comercial@teknokroma.es Registered No. 1008689 England
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Brilliant Spectroscopy™
www.specac.com
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