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Calculation Guide 1699624488
Calculation Guide 1699624488
1. Basic Understanding
Agitated vessels with an external jacket or an internal coil are increasingly employed in
biotechnology and other process applications. The most common type of jackets consists of an
outer cylinder that surrounds part of the vessel. The heating or cooling medium circulates in the
annular space between the jacket and vessel walls.
Consider a vessel containing an agitated liquid. Heat transfer occurs mainly through forced
convection in the liquid, conduction through the vessel wall, forced convection in the jacket
media, finally combined of natural and forced convection in outer side . The calculation are start
by applying basic energy balance and derive the equation that occurs in both vessel and jacket
side. For vessel side :
Since this is the time dependent calculation which is temperature always change by the time until
reached steady state, the accumulation will not zero. For both vessel and jacket side respectively
:
Page 2 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
𝑑𝑄𝑣𝑒𝑠𝑠𝑒𝑙
𝑑𝑡
= 𝑄𝑖𝑛𝑙𝑒𝑡 𝑡𝑜 𝑣𝑒𝑠𝑠𝑒𝑙 − 𝑄𝑜𝑢𝑡𝑙𝑒𝑡 𝑓𝑟𝑜𝑚 𝑣𝑒𝑠𝑠𝑒𝑙 ± 𝑄𝑡𝑟𝑎𝑛𝑠𝑓𝑒𝑟𝑟𝑒𝑑 𝑓𝑟𝑜𝑚 𝑗𝑎𝑐𝑘𝑒𝑡
𝑑𝑄𝑗𝑎𝑐𝑘𝑒𝑡
= 𝑄𝑖𝑛𝑙𝑒𝑡 𝑡𝑜 𝑗𝑎𝑐𝑘𝑒𝑡 − 𝑄𝑜𝑢𝑡𝑙𝑒𝑡 𝑓𝑟𝑜𝑚 𝑗𝑎𝑐𝑘𝑒𝑡 − 𝑄𝑡𝑟𝑎𝑛𝑠𝑓𝑒𝑟𝑟𝑒𝑑 𝑓𝑟𝑜𝑚 𝑗𝑎𝑐𝑘𝑒𝑡 ± 𝑄𝑙𝑜𝑠𝑠
𝑑𝑡
𝑑𝑄𝑣𝑒𝑠𝑠𝑒𝑙
= 𝐹𝑖𝑛𝑙𝑒𝑡 𝐶𝑝𝑖𝑛𝑙𝑒𝑡 𝑇𝑖𝑛𝑙𝑒𝑡 − 𝐹𝑜𝑢𝑡𝑙𝑒𝑡 𝐶𝑝𝑜𝑢𝑡𝑙𝑒𝑡 𝑇𝑜𝑢𝑡𝑙𝑒𝑡 ± (𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 )𝐽𝑉
𝑑𝑡
𝑑𝑄𝑗𝑎𝑐𝑘𝑒𝑡
= 𝐹𝑖𝑛𝑙𝑒𝑡 𝐶𝑝𝑖𝑛𝑙𝑒𝑡 𝑇𝑖𝑛𝑙𝑒𝑡 − 𝐹𝑜𝑢𝑡𝑙𝑒𝑡 𝐶𝑝𝑜𝑢𝑡𝑙𝑒𝑡 𝑇𝑜𝑢𝑡𝑙𝑒𝑡 ± (𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 )𝐽𝑉 ± (𝑈𝐴Δ𝑇)𝐽𝐴
𝑑𝑡
The subscript JV and JS are stands for jacket to vessel and jacket to ambient surrounding heat
transfer. Let's take considering a vessel side is batch process, hence :
Then obtained :
𝑑𝑇
m Cp = ± (𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 )𝐽𝑉
𝑑𝑡
Please note that heat always travels from the higher temperature to the lower temperature.
Minus/plus sign could vary depend inside temperature of tank. For this tank, hot water are
applied to the jacket, heating the vessel content. Thus, jacket temperature are higher than inside
tank. The heat will travel from jacket to inside tank. Therefore, the sign are positive and inside
tank temperature will increase.
𝑑𝑇 (𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 )𝐽𝑉
=
𝑑𝑡 𝑚 𝐶𝑝
From Eq1, taking integral on both side and put 0 to target time as lower and upper integral limit,
yielded final form :
𝑇_𝑓𝑖𝑛𝑎𝑙 𝑡_𝑡𝑎𝑟𝑔𝑒𝑡
(𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 )𝐽𝑉
න 𝑑𝑇𝑝𝑟𝑜𝑑𝑢𝑐𝑡 = න 𝑑𝑡 .....................[Eq2]
𝜌𝑝𝑟𝑜𝑑𝑢𝑐𝑡 𝑉𝑣𝑒𝑠𝑠𝑒𝑙 𝐶𝑝𝑝𝑟𝑜𝑑𝑢𝑐𝑡
𝑇_𝑖𝑛𝑖𝑡𝑖𝑎𝑙 0
ΔTLMTD is log mean temperatur difference, which is logaritmic average of the temperature
difference between hot and cold fluid for both inside vessel and jacket.
Page 3 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
Δ𝑇1 − Δ𝑇2
Δ𝑇𝐿𝑀𝑇𝐷 =
𝑙𝑛Δ𝑇1 −𝑙𝑛Δ𝑇2
and respectively :
The step above are repeated for jacket side. Since the jacket fluid media always flows for
heating/cooling, thus F_inlet = F_outlet ≠ 0, and derivation are continue giving :
integrating :
𝑇_𝑓𝑖𝑛𝑎𝑙 𝑡_𝑡𝑎𝑟𝑔𝑒𝑡
𝐹𝑚 𝐶𝑝𝑚 Δ𝑇𝑚 − (𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 )𝐽𝑉 − (𝑈𝐴Δ𝑇)𝐽𝐴
න 𝑑𝑇𝑚 = න 𝑑𝑡
𝜌𝑚 𝑉𝑗𝑎𝑐𝑘𝑒𝑡 𝐶𝑝𝑚
𝑇_𝑖𝑛𝑖𝑡𝑖𝑎𝑙 0
.....................[Eq4]
2. Calculation Guide
2.1. UA calculation
According to Eq2 and Eq4 above, both equation required UA parameter which is overall heat
transfer coefficient and heat transfer area. Now we are going to determine them. Overall heat
loss/trasnfer formula :
Δ𝑇𝐿𝑀𝑇𝐷
Q= 𝑈𝐴Δ𝑇𝐿𝑀𝑇𝐷 or simply Q= 𝑅
Based on cylindrical geometry, heat are transferred in two direction, radial direction side
(concentrical) and axial direction side (vertical). Let's taking assumption that heat are travels only
in shell side (radial direction) of the vessel. Then :
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Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
............[Eq7]
The calculation of heat transfer coefficent (h) always dependent on the properties of the fluid
itself and the fluid condition. For the vessel equipped with agitator, the fluid inside the vessel will
move following agitator motion, hence causing the heat spread along the inside vessel. This is
are called forced convection which is heat transfering by motion of the fluid. The inside film heat
transfer coefficient (hi) can be calculated from the following Nusselt number correlation:
𝑁𝑁𝑢 𝑘 ............[Eq8]
ℎ𝑖 =
𝐷𝑇
Also Nusselt's number is dimensionless number, are calculated by Reynold's number and
Prandtl's number:
2
𝜌𝑚 𝑁𝐷𝐴
𝑁𝑅𝑒 = ............[Eq9]
𝜇𝑚
𝐶𝑝𝑚 μ𝑚
𝑁𝑃𝑟 = ............[Eq10]
𝑘𝑚
μ𝑏 𝑑
𝑁𝑁𝑢 = a𝑁𝑅𝑒 𝑏 𝑁𝑃𝑟 𝑐 ............[Eq11]
μ𝑤
where :
hi = heat transfer coefficient inside vessel, W/m2 0C
NNu = Nusselt's number
DA = impeller diameter, m
DT = vessel internal diameter, m
NRe = Reynlod's number
ρm = average fluid density, kg/m3
Page 5 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
N = agitator speed, rpm
NPr = Prandtl's number
Cpm = average fluid specific heat, Jkg/0C
km = average fluid thermal conductivity, W/m 0C
μm = average fluid dynamic viscosity, Pa.s
μb = fluid bulk viscosity, Pa.s
μw = fluid wall viscosity, Pa.s
And a, b, c, and d are the coefficient depending on Reynolds number and type of agitator. Table
bellow shows numerous type agitator and its correction factor that generally used in industry.
Geometry factor
Agitator type Flow region
a b c d
Paddle
Propeller
Page 6 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
Geometry factor
Agitator type Flow region
a b c d
Page 7 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
Geometry factor
Agitator type Flow region
a b c d
Anchor
Helical ribbon
When the agitator are not equipped, the heat only travel due to differences density between hot
fluid and cold fluid. The hold fluid are lighter than cold fluid, thus hot fluid will float and it's place
will be replaced by cold fluid. This phenomena are called natural convection, which heat
transfering without any external forces. Than the Nusselt's number as follows :
1ൗ 2
0.387𝑁𝑅𝑎 6
𝑁𝑁𝑢 = 0.6 + 8ൗ
9ൗ 27 ............[Eq12]
0.559 16
1+
𝑁𝑃𝑟
𝑔 𝛽 𝛥𝑇 𝐷𝑇3 𝜇 𝑘
𝑁𝑅𝑎 = ν=
𝜌
α= ρ𝐶𝑝
𝜈𝛼
Page 8 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
Many jacketed vessels are reactors; the types of exothermic or endothermic effects must be
taken into account. Stirred tank reactors in which an exothermic reaction is performed may
involve the removal of substantial amounts of heat from the reacting mixture. Refluxing of a
boiling solvent is a common method; the heat of vaporization of the solvent is removed by the
reflux condenser, and the condensed solvent is returned to the reactor. Other methods include
cooling the walls of the reactor by means of a jacket with a cooling medium, inserting a cooling
coil, or using an external heat exchanger with a pump around the system. In many applications
using jacketed vessels, successive batches of material are heated (or cooled) to a given
temperature, and therefore the heat transfer involves an unsteady state process. Proper care is
essential in terms of charging, agitation and adequate cooling of the reactants to prevent the
generated heat from subsequently leading to a runaway reaction.
Page 9 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
Nusselt's number for jacket side also applied with same procedural in agitator.
Geometry factor
Jacket type Flow region
a b c d
Conventional jacket
Half-pipe coil
Page 10 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
Geometry factor
Jacket type Flow region
a b c d
Dimple jacket
As most best practice, it is to consider that set the flow region to turbulence. It will enhancing
heat transfer coefficient.
Sometimes vessel are placed inside or outside the building. Hence, we need to consider impact
of environmental to heat losses or transferred. Insulation are applied to cover the tank, especially
contained hot media to protect enveironment side from heat exposed from vessel. Air side (outer
side) heat transfer is due to combined effect of natural convection and forced convection.
For forced convection, Nusselt number are (Churchill & Bernstein correlation) :
5/8 4/5
0.62𝑅𝑒1/2 𝑃𝑟1/3 𝑅𝑒
𝑁𝑢𝑓𝑜𝑟𝑐𝑒𝑑 = 0.3 + 1/4
+ 1+ ............[Eq13]
0.42/3 282000
1+
𝑃𝑟
1ൗ 2
0.387𝑁𝑅𝑎 6
𝑁𝑁𝑢 = 0.6 + 8ൗ ............[Eq12]
9ൗ 27
0.559 16
1+
𝑁𝑃𝑟
Page 11 of 12
Document No. : Date : 10-Nov-23
Revision No. : Prepared by : NFL
Basic Understanding and Calculation Guide for Heat
Tittle :
Transfer on Agitated, Jacketed, and Insulated Vessel
𝑁𝑁𝑢 𝑘
ℎ𝑜 =
𝐷𝑣𝑒𝑠𝑠𝑒𝑙
As we see on [Eq2] and [Eq4] , the calculation involved integral in order to get final temperature
in certain interval time. However, I practical this method are difficult to use since thermal
properties (e.g. density, viscosity, thermal conductivity) are temperature dependent variable that
changes following temperature. Also, since we must to solve both equation simultaneously, it
would complicate the calculation. Numerical method are suggested to use for this kind of
calculation. Runge-Kutta method for solving differential equation will gives good result.
3. Refference
A Kayode Coker, and Ernest E Ludwig. Ludwig’s Applied Process Design for Chemical
and Petrochemical Plants. Amsterdam ; Boston, Elsevier Gulf Professional Pub, 2007.
Kresta, Suzanne M, et al. Advances in Industrial Mixing . John Wiley & Sons, 11 Mar.
2016.
Paul, Edward L, et al. Handbook of Industrial Mixing : Science and Practice . Hoboken,
N.J., Wiley-Interscience, Cop, 2004.
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