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KTA-Tator, Inc.
Adhesion
Common Pitfalls When Testing Coating Adhesion
Reporting
Learning Outcomes
Completion of this webinar will enable the
participant to:
Explain the purpose of testing the adhesion properties of coatings
Describe the two types of adhesion testing mechanisms
List four standard test methods used to test the adhesion of
coating systems
Learning Outcomes,
continued
adhesion testers
compliance
Common in-process
inspection of TSC
Determine
maintenance strategy
for existing coating
systems
Adhesion data is not
typically a predictor of
coating performance
Cohesion Strength
in a specification
Method
D 3359-09
D 6677-07
Knife Adhesion
D 4541-09
D 7234-05
perpendicular pull)
are different
Adhesion testing is destructive to the coating film
Equipment
Steel ruler or guide
Utility knife
Brush
Adhesive tape
Magnifier
ASTM Test Method
Cross-cut Tester
(alternative to knife
and guide)
3A
2A
1A
0A
<5%
2B
1635%
1B
3665%
0B
By Knife
Description
10
Pitfalls to Avoid
ASTM D3359 is for coatings on metallic surfaces
Dull knife blades can produce erroneous results
Maintain proper spacing between incisions when
Permacel 99 as suitable
Permacel 99 discontinued in 2009
No immediate replacement
Intertape Polymer Group LA26 will
be investigated (backing, adhesive,
thickness & adhesion to steel
similar)
Section 5.3 indicates 1 (25 mm)
width and adhesion strength as
agreed is acceptable
Exercise caution when comparing
data using different tapes/batches
of tape
Reporting
Substrate type and coating system; method of
cure
Environmental conditions (temperature and RH)
No. of tests performed
Manufacturer and type of tape employed (when
used)
Mean and range of ratings
Location of Break (between coats, within a coat,
between substrate surface and primer, etc.)
Fixed Alignment
Type II
Self-Aligning
Type III
Self-Aligning
Type VI
Self-Aligning
Type IV
Self-Aligning
Type V
Selecting an Adhesive
High solids epoxy
adhesives
Cyanoacrylate
adhesive
Ensure compatibility
with coating
UV curable adhesive
available with Type IV
tester (requires special
loading fixtures with
transparent base)
Range
106/1
0-500 psi
106/2
(shown)
0-1000 psi
106/3
106/4
106/4A
106/5
0-30 psi
0-500 psi
F-2
0-1,000 psi
F-4
0-2,000 psi
F-8
0-4,000 psi
F-16
0-8,000 psi
F-8/12
0-4,000/0-10,000 psi
Round base with pigtail hose
Silicone rubber gasket (lifted upward)
Round threaded top plate
valve
button
Push in and hold the
Run button, while
On/off
slowly opening the Rate
Valve until pressure
increases at ~2
psi/second
Do not exceed 6 psi/
second
Run
Peak
Reset
**
3. Loading Rate
The pressure loading rate should be 30 psi/second;
the test should be completed in 5-30 seconds
Pitfalls to Avoid
Determine which tester to use. Different testers
Reporting
General Nature of Test
Substrate type and coating system (thickness, type, surface
orientation)
Field or laboratory testing
Air temperature and relative humidity
Testing apparatus employed; loading fixture type/dimensions
Adhesive type employed
No. of tests performed
Load applied (pull-off values, in psi, KPa or MPa)
Mean and range of pull-off values
Location of break (between coats, within a coat, between substrate
surface and primer, etc.)
Note scoring, if employed (and any other deviations from procedure)
THE END