Distilasi dengan metode reflux dan

Mc-Cabe Thiele

Kelompok 1 :

1. ALZENA ARAMINTA A.J 1831410060

2. HAYU NINDIKA R.P 1831410008
3. ILLA FATMA 1831410153
 PROBLEM SOLVING

11.4-1
Rectification column is fed 100kg mol/h of mixture
of 50 mol % benzene and 50 mol % toluene at 101.32
kPa abs pressure. The feed is liquid at the boiling point.
The distilate is to contain 90 mol % of benzene and the
bottoms 10 mol % of benzene. The reflux ration is
4.52:1. calculate the kg mol/h distilate, kg mol/h bottoms
and the number of theoretical trays needed using the
McCabe-Thiele method
O  
Diketahui : Benzene-Toluene
OF : 100 kg mol/h
OP : 101.32 kPa
O : 0.9
O : 0.1
O : 0.5
O R : 4.52

Ditanya
a. Distilate (kg mol/h) ?
b. W (kg mol/h) ?
c. Jumlah tray teoritis yang dibutuhkan menggunakan McCabe-
Thiele Method?
O Neraca
  massa overall di subtitusikan (11.4-3)

F =D+W
100 = D + W
W = 100 – D

a) Distilate
F. = D. + W. (11.4-4)
100 x 0.5 = D x 0.9 + (100 – D) x 0.1
50 = 0.9D + 10 – 0.1D
40 = 0.8D
D = 50 kg mol/h
b) Bottoms
W = 100 – D
W = 100 – 50
W = 50 kg mol/h
c)
O Number
  of theoretical trays

O Garis operasi enriching (11.4-8)

+
+
= + 0.16

O Data equilibrium diperoleh dari tabel 11.1-1

- Karena maka boiling point umpan
- T = 92 C = 365.15 K
- q = 1 (Saturated liquid)
- Intercept
x=0
y = = = 0.16
0.16 (intecep)
 Jumlah langkah teoritis = 5 + ()
= 5.9
Jadi jumlah langkah teoritis adalah 5.9 yang terdiri dari
4.9 tray dan 1 reboiler
 PROBLEM SOLVING

11.4-3
O  
O For the rectification given in Problem 11.4-1,
where an equimolar liquid feed of benzene and toluene
is being distiled to give a distillate of composition 0.9
and a bottoms of composition = 0.1 . Calculate the
following using graphical methods.
O  
Diketahui
O : 0.9
O : 0.1
O : 0.5
O Karena suhu umpan masuk pada titik didihnya maka
q=1

Ditanya :
a) Reflux minimum ratio ()
b) Jumlah minimum tray pada R total
 Garis operasi untuk
a)  
O

Dari grafik didapatkan

x' = 0.5
y' = 0.71
- Substitusi ke pers. 11.4-24

=
=
=
0.4 = 0.19
= 0.91
b) Jumlah tray = 5
- 4 Tray teoritis
- 1 reboiler
TERIMA KASIH
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