Professional Documents
Culture Documents
Non Destructive Testing
Non Destructive Testing
Die penetrate test (liquid penetrate inspection), Principle, scope. Equipment &
techniques, Tests stations, Advantages, types of penetrants and developers,
Zyglo test, Illustrative examples and interpretation of defects. 5
Magnetic particle Inspection – scope and working principle, Ferro Magnetic
and Non-ferromagnetic materials, equipment & testing. Advantages,
limitations Interpretation of results, DC & AC magnetization, Skin Effect, use
of dye & wet powders for magna glow testing, different methods to generate
magnetic fields, Applications. 5
Liquid Penetrant Testing (PT)
• This is a method which can be employed for the detection of open-to-
surface discontinuities in any industrial product which is made from a
non-porous material.
• In this method a liquid penetrant is applied to the surface of the
product for a certain predetermined time after which the excess
penetrant is removed from the surface.
• The surface is then dried and a developer is applied to it.
• The penetrant which remains in the discontinuity is absorbed by the
developer to indicate the presence as well as the location, size and
nature of the discontinuity.
General procedure for liquid penetrant
inspection
• Cleaning the surface to be examined
• There should be no material such as plating, or coatings of oxide or loose dirt particles on surface. This is to
prevent false indications and to expose hidden discontinuities to the penetrant.
• Solid contaminant such as carbon, engine varnish, paints and similar materials should be removed by vapour
blast, chemical dip or other acceptable methods.
• Methods such as shot blasting, emery cloth, wire brushing or metal scrapping should not be used, especially
for soft materials, since these cleaning methods will cover up defects by cold working the surface.
• Contamination can occur due to the presence of lubricants, protective oils, metal dust polymerization,
oxidation, carbonaceous deposits, protective paints, etc. Various solvents have been developed by different
companies to remove them.
• Contamination due to inorganic corrosion products, heat treatment scale, operationally formed refractory
oxides, etc. is conveniently removed by abrasive blasting with glass beads, etc. combined with a chemical
cleaning.
• Whichever method is employed the use of trichloroethylene vapor degreasing as a final stage is strongly
recommended.
General procedure for liquid penetrant
inspection
• Drying the surface
• If, for any reason, separations are filled with liquid, they will prevent entry of
penetrant, hence drying is an essential operation.
• It should be realized that although the surface may seem dry, separations may
still be filled with liquid.
• The lesson is that improper drying may be worse than no cleaning, because the
remaining solvent may present a barrier to the penetrant too.
• If penetrant liquid does reach into the separation, it will be diluted by the
solvent, and this also makes the treatment less effective.
General procedure for liquid penetrant
inspection
• Application of penetrant
• The penetrant is applied with the help of a brush or by spray or by dipping the
test piece into a bath of penetrant.
• After this a certain residence time or 'dwell time' is allowed for the penetrant
to seep into discontinuities.
• The residence time varies with the temperature, the type of penetrant, the
nature of the discontinuity and the material of the test specimen. It usually
varies between 5 and 30 minutes. In special cases it may be as long as one
hour.
General procedure for liquid penetrant
inspection
• Removal of superfluous penetrant
• The excess penetrant on the surface should be removed to obtain optimum
contrast and to prevent misleading indications.
• The appropriate remover is usually recommended by the manufacturer of the
penetrant. Some penetrants are water washable while others need application
of an emulsifier before they can be removed with water. The removal method
is to use a sponge or water spray. There are special penetrant removers which
are essentially solvents.
• It is most important that removal of the penetrant is restricted to the surface
and that no penetrant is washed out of the flaws which can easily happen when
the cleaning is too rigorous.
General procedure for liquid penetrant
inspection
• Removal of superfluous penetrant
• When the surface is smooth washing can be less intensive than for rough
surfaces; in the latter case there is a definite risk that penetrant may be washed
out of small imperfections.
• A general criterion for the removal operation is that it must be fast and should
be prolonged long enough to make the surface almost clean.
• It is better to leave small traces of penetrant on the surface than to carry out
excessive cleaning.
• When removing fluorescent penetrants, the effect of the treatment should
preferably be watched under black light.
General procedure for liquid penetrant
inspection
• Drying the surface
• The surface can be dried with a dry cloth or an air blower.
• Drying is generally needed to prepare the surface for the application of a
powder developer, which would otherwise clot at wet places.
• It also decreases the adverse effect of insufficiently removed traces of
penetrant.
• Here again excess should be avoided. Penetrant liquid left in flaws should not
be allowed to dry, and this can happen when hot air is used for drying.
General procedure for liquid penetrant
inspection
• Application of developer
• Developers are usually of two types namely dry and wet developer.
• Dry developer consists of a dry, light colored powdery material.
• It is applied to the surface after removal of excess penetrant and drying of the
part.
• It can be applied either by immersing the parts in a tank containing powder, or
by brushing it on with a paint brush (usually not a desirable technique) or by
blowing the powder onto the surface of the part.
General procedure for liquid penetrant
inspection
• Application of developer
• Wet developer consists of a powdered material suspended in a suitable liquid
such as water or a volatile solvent.
• It is applied to the parts immediately following the water washing operation.
Developers should be such that they provide a white coating that contrasts
with the colored dye penetrant, and draw the penetrant from the discontinuities
to the surface of the developer film, thus revealing defects.
• The dry developers are applied generally with fluorescent penetrants. They are
applied just prior to the visual inspection process.
• The wet developers are also used in connection with fluorescent penetrants.
They are applied after the washing operation and before the drying operation.
General procedure for liquid penetrant
inspection
• Application of developer
• The solvent based developers are generally used with the visible dye-
penetrants. They are applied after cleaning off extra penetrant.
• A short time should be allowed for development of indications after the
developer has been applied. This time should be approximately one half that
allowed for penetration.
• Developer coating is removed after inspection by water stream, spray nozzle,
brush, etc.
• The powder concentration of the liquid developer should be carefully
controlled to obtain the required thin and uniform layer over the surface.
General procedure for liquid penetrant
inspection
• Observation and interpretation of indications
• An indication in the developer will become visible after a certain lapse of
time. Because all penetrant inspection methods rely upon the seeing of an
indication by the inspector, the lighting provided for this visual examination is
extremely important.
• For best results, inspection for fluorescent indications should be done in a
darkened area using black light.
• For the interpretation of indications, it is very important to observe their
characteristics at the very moment they appear. As soon as the flaws have bled
out the indications may run to larger spots, depending on size and depth, and
at this stage it is difficult to derive characteristic information from a flaw.
General procedure for liquid penetrant
inspection
• Observation and interpretation of indications
• A brief guide to the penetrant indications is given here.
• A crack usually shows up as a continuous line of penetrant indication.
• A cold shut on the surface of a casting also appears as a continuous line, generally a
relatively narrow one.
• A forging lap may also cause a continuous line of penetrant indication.
• Rounded areas of penetrant indication signify gas holes or pit holes in castings.
• Deep crater cracks in welds frequently show up as rounded indications.
• Penetrant indications in the form of small dots result from a porous condition. These may
denote small pin holes or excessively coarse grains in castings or may be caused by a
shrinkage cavity.
General procedure for liquid penetrant
inspection
• Observation and interpretation of indications
• A brief guide to the penetrant indications is given here.
• With fluorescent penetrants, the whole surface may glow feebly. With dye penetrants, the
background may be pink instead of white. Depth of defects will be indicated by richness
of color and speed of bleed out.
• The time required for an indication to develop is inversely proportional to the volume of
the discontinuity.
Penetrant Materials
• Penetrant materials come in two basic types. These types are listed below:
• Type 1 - Fluorescent Penetrants
• Type 2 - Visible Penetrants
• Fluorescent penetrants contain a dye or several dyes that fluoresce when exposed to
ultraviolet radiation.
• Visible penetrants contain a red dye that provides high contrast against the white developer
background.
• Fluorescent penetrant systems are more sensitive than visible penetrant systems because the
eye is drawn to the glow of the fluorescing indication.
• However, visible penetrants do not require a darkened area and an ultraviolet light in order
to make an inspection. Visible penetrants are also less vulnerable to contamination from
things such as cleaning fluid that can significantly reduce the strength of a fluorescent
indication.
Penetrant Materials
• Penetrants are then classified by the method used to remove the excess
penetrant from the part. The four methods are listed below:
• Method A - Water Washable
• Method B - Post-Emulsifiable, Lipophilic
• Method C - Solvent Removable
• Method D - Post-Emulsifiable, Hydrophilic
Penetrant Materials
• Water washable (Method A) penetrants can be removed from the part by rinsing
with water alone. These penetrants contain an emulsifying agent (detergent) that
makes it possible to wash the penetrant from the part surface with water alone.
Water washable penetrants are sometimes referred to as self-emulsifying systems.
• Post-emulsifiable penetrants come in two varieties, lipophilic and hydrophilic.
• In post-emulsifiers, lipophilic systems (Method B), the penetrant is oil soluble and
interacts with the oil-based emulsifier to make removal possible.
• Post-emulsifiable, hydrophilic systems (Method D), use an emulsifier that is a
water soluble detergent which lifts the excess penetrant from the surface of the part
with a water wash. Solvent removable penetrants require the use of a solvent to
remove the penetrant from the part.
Penetrant Materials
• Penetrants are then classified based on the strength or detectability of
the indication that is produced for a number of very small and tight
fatigue cracks. The five sensitivity levels are shown below:
• Level ½ - Ultra Low Sensitivity
• Level 1 - Low Sensitivity
• Level 2 - Medium Sensitivity
• Level 3 - High Sensitivity
• Level 4 - Ultra-High Sensitivity
Penetrant Materials
• The major US government and industry specifications currently rely on the US Air
Force Materials Laboratory at Wright-Patterson Air Force Base to classify penetrants
into one of the five sensitivity levels.
• This procedure uses titanium and Inconel specimens with small surface cracks
produced in low cycle fatigue bending to classify penetrant systems. The brightness
of the indication produced is measured using a photometer. The sensitivity levels
and the test procedure used can be found in Military Specification MIL-I-25135 and
Aerospace Material Specification 2644, Penetrant Inspection Materials.
• An interesting note about the sensitivity levels is that only four levels were
originally planned. However, when some penetrants were judged to have
sensitivities significantly less than most others in the level 1 category, the ½ level
was created.
Emulsifiers
• When removal of the penetrant from a defect due to over-washing of
the part is a concern, a post-emulsifiable penetrant system can be used.
Post-emulsifiable penetrants require a separate emulsifier to break the
penetrant down and make it water-washable. Most penetrant
inspection specifications classify penetrant systems into four methods
of excess penetrant removal. These are listed below:
• Method A: Water-Washable
• Method B: Post-Emulsifiable, Lipophilic
• Method C: Solvent Removable
• Method D: Post-Emulsifiable, Hydrophilic
Emulsifiers
• Method C relies on a solvent cleaner to remove the penetrant from the
part being inspected.
• Method A has emulsifiers built into the penetrant liquid that makes it
possible to remove the excess penetrant with a simple water wash.
• Method B and D penetrants require an additional processing step
where a separate emulsification agent is applied to make the excess
penetrant more removable with a water wash.
Developers
• The role of the developer is to pull the trapped penetrant material out of defects
and spread it out on the surface of the part so it can be seen by an inspector.
• The fine developer particles both reflect and refract the incident ultraviolet
light, allowing more of it to interact with the penetrant, causing more efficient
fluorescence.
• The developer also allows more light to be emitted through the same
mechanism. This is why indications are brighter than the penetrant itself under
UV light.
• Another function that some developers perform is to create a white background
so there is a greater degree of contrast between the indication and the
surrounding background.
Developer Forms
• The AMS 2644 and Mil-I-25135 classify developers into six standard
forms. These forms are listed below:
• Form a - Dry Powder
• Form b - Water Soluble
• Form c - Water Suspendable
• Form d - Nonaqueous Type 1 Fluorescent (Solvent Based)
• Form e - Nonaqueous Type 2 Visible Dye (Solvent Based)
• Form f - Special Applications
Developer Forms
• Dry Powder
• Dry powder developer is generally considered to be the least sensitive but it is
inexpensive to use and easy to apply.
• Dry developers are white, fluffy powders that can be applied to a thoroughly dry
surface in a number of ways.
• The developer can be applied by dipping parts in a container of developer, or by
using a puffer to dust parts with the developer.
• Parts can also be placed in a dust cabinet where the developer is blown around
and allowed to settle on the part.
• Electrostatic powder spray guns are also available to apply the developer. The
goal is to allow the developer to come in contact with the whole inspection area.
Developer Forms
• Water Soluble
• As the name implies, water soluble developers consist of a group of chemicals that are
dissolved in water and form a developer layer when the water is evaporated away.
• The best method for applying water soluble developers is by spraying it on the part.
• The part can be wet or dry.
• Dipping, pouring, or brushing the solution on to the surface is sometimes used but these
methods are less desirable.
• Aqueous developers contain wetting agents that cause the solution to function much like
dilute hydrophilic emulsifier and can lead to additional removal of entrapped penetrant.
• Drying is achieved by placing the wet but well drained part in a recirculating, warm air
dryer with the temperature held between 70 and 75°F. If the parts are not dried quickly,
the indications will be blurred and indistinct.
• Properly developed parts will have an even, pale white coating over the entire surface.
Developer Forms
• Water Suspendable
• Water suspendable developers consist of insoluble developer particles
suspended in water.
• Water suspendable developers require frequent stirring or agitation to keep the
particles from settling out of suspension.
• Water suspendable developers are applied to parts in the same manner as water
soluble developers.
• Parts coated with a water suspendable developer must be forced dried just as
parts coated with a water soluble developer are forced dried.
• The surface of a part coated with a water suspendable developer will have a
slightly translucent white coating.
Developer Forms
• Nonaqueous
• Nonaqueous developers suspend the developer in a volatile solvent and are
typically applied with a spray gun.
• Nonaqueous developers are commonly distributed in aerosol spray cans for
portability.
• The solvent tends to pull penetrant from the indications by solvent action.
Since the solvent is highly volatile, forced drying is not required.
• A nonaqueous developer should be applied to a thoroughly dried part to form a
slightly translucent white coating.
Developer Forms
• Special Applications
• Plastic or lacquer developers are special developers that are primarily used
when a permanent record of the inspection is required.
Nature of the Defect
• The nature of the defect can have a large affect on sensitivity of a liquid penetrant
inspection. Sensitivity is defined as the smallest defect that can be detected with a
high degree of reliability.
• Typically, the crack length at the sample surface is used to define size of the defect.
• A survey of any probability-of-detection curve for penetrant inspection will quickly
lead one to the conclusion that crack length has a definite affect on sensitivity.
However, the crack length alone does not determine whether a flaw will be seen or
go undetected.
• The volume of the defect is likely to be the more important feature. The flaw must
be of sufficient volume so that enough penetrant will bleed back out to a size that is
detectable by the eye or that will satisfy the dimensional thresholds of fluorescence.
• It is an
example of
fluorescent
penetrant
inspection
probability of
detection
(POD) curve
from the
Nondestructi
ve Evaluation
(NDE)
Capabilities
Data Book.
Penetrant inspections are more effective at
finding
• small round defects than small linear defects. Small round defects
are generally easier to detect for several reasons.
• First, they are typically volumetric defects that can trap significant amounts of
penetrant.
• Second, round defects fill with penetrant faster than linear defects.
• One research effort found that elliptical flaw with length to width ratio of 100,
will take the penetrant nearly 10 times longer to fill than a cylindrical flaw
with the same volume.
• deeper flaws than shallow flaws. Deeper flaws will trap more
penetrant than shallow flaws, and they are less prone to over washing.
Penetrant inspections are more effective at
finding
• flaws with a narrow opening at the surface than wide open
flaws. Flaws with narrow surface openings are less prone to over
washing.
• flaws on smooth surfaces than on rough surfaces. The surface
roughness of the part primarily affects the removability of a penetrant.
Rough surfaces tend to trap more penetrant in the various tool marks,
scratches, and pits that make up the surface. Removing the penetrant
from the surface of the part is more difficult and a higher level of
background fluorescence or over washing may occur.
Inspecting Welds with Liquid Penetrants
• Inspecting Welds with Liquid Penetrants
Zyglo test
Advantages
• The method has high sensitivity to small surface discontinuities.
• The method has few material limitations, i.e. metallic and nonmetallic, magnetic
and nonmagnetic, and conductive and nonconductive materials may be inspected.
• Large areas and large volumes of parts/materials can be inspected rapidly and at
low cost.
• Parts with complex geometric shapes are routinely inspected.
• Indications are produced directly on the surface of the part and constitute a visual
representation of the flaw.
• Aerosol spray cans make penetrant materials very portable.
• Penetrant materials and associated equipment are relatively inexpensive.
Disadvantages
• Only surface breaking defects can be detected.
• Only materials with a relatively nonporous surface can be inspected.
• Precleaning is critical since contaminants can mask defects.
• Metal smearing from machining, grinding, and grit or vapor blasting must be
removed prior to LPI.
• The inspector must have direct access to the surface being inspected.
• Surface finish and roughness can affect inspection sensitivity.
• Multiple process operations must be performed and controlled.
• Post cleaning of acceptable parts or materials is required.
• Chemical handling and proper disposal is required.
Magnetic particle Inspection
• Magnetic particle Inspection – scope and working principle, Ferro
Magnetic and Non-ferromagnetic materials, equipment & testing.
Advantages, limitations Interpretation of results, DC & AC
magnetization, Skin Effect, use of dye & wet powders for magna glow
testing, different methods to generate magnetic fields, Applications.
Magnetic particle Inspection
• Magnetic particle inspection (MPI) is a nondestructive testing method
used for defect detection
• MPI uses magnetic fields and small magnetic particles (i.e. iron
filings) to detect flaws in components.
• The only requirement from an inspectability standpoint is that the
component being inspected must be made of a ferromagnetic material
such as iron, nickel, cobalt, or some of their alloys.
Basic Principles
• It can be considered as a combination of two nondestructive
testing methods: magnetic flux leakage testing and visual testing.
• The first step in a magnetic particle inspection is to magnetize the
component that is to be inspected.
• If any defects on or near the surface are present, the defects will
create a leakage field.
• After the component has been magnetized, iron particles, either in
a dry or wet suspended form, are applied to the surface of the
magnetized part.
• The particles will be attracted and cluster at the flux leakage
fields, thus forming a visible indication that the inspector can
detect.
Diamagnetic, Paramagnetic, and
Ferromagnetic Materials
• When a material is placed within a magnetic field, the magnetic forces
of the material's electrons will be affected. This effect is known as
Faraday's Law of Magnetic Induction.
• However, materials can react quite differently to the presence of an
external magnetic field. This reaction is dependent on a number of
factors, such as the atomic and molecular structure of the material, and
the net magnetic field associated with the atoms.
• The magnetic moments associated with atoms have three origins.
These are the electron motion, the change in motion caused by an
external magnetic field, and the spin of the electrons.
Diamagnetic, Paramagnetic, and
Ferromagnetic Materials
• In most atoms, electrons occur in pairs. Electrons in a pair spin in
opposite directions.
• So, when electrons are paired together, their opposite spins cause their
magnetic fields to cancel each other.
• Therefore, no net magnetic field exists.
• Alternately, materials with some unpaired electrons will have a net
magnetic field and will react more to an external field.
• Most materials can be classified as diamagnetic, paramagnetic or
ferromagnetic.
Diamagnetic, Paramagnetic, and
Ferromagnetic Materials
• Diamagnetic materials have a weak, negative susceptibility to magnetic
fields. Diamagnetic materials are slightly repelled by a magnetic field and the
material does not retain the magnetic properties when the external field is
removed.
• Paramagnetic materials have a small, positive susceptibility to magnetic
fields. These materials are slightly attracted by a magnetic field and the
material does not retain the magnetic properties when the external field is
removed.
• Ferromagnetic materials have a large, positive susceptibility to an external
magnetic field. They exhibit a strong attraction to magnetic fields and are able
to retain their magnetic properties after the external field has been removed.
Quantifying Magnetic Properties
• The units for magnetic field strength H is ampere/meter. A magnetic
field strength of 1 ampere/meter is produced at the center of a single
circular conductor with a one-meter diameter carrying a steady current
of 1 ampere.
• The number of magnetic lines of force cutting through a plane of a
given area at a right angle is known as the magnetic flux density, B.
• The flux density or magnetic induction has the tesla as its unit. One
tesla is equal to 1 Newton/(A/m).
Quantifying Magnetic Properties
• The total number of lines of magnetic force in a material is called magnetic
flux, f. The strength of the flux is determined by the number of magnetic
domains that are aligned within a material. The total flux is simply the flux
density applied over an area. Flux carries the unit of a weber, which is simply a
tesla- meter2.
• The magnetization is a measure of the extent to which an object is magnetized.