DSP: Seminar 2, Binary distillation, McCabe-Thiele method, column with one

MH2O 18 kg/kmol Maa 60.5 kg/kmol Δ vhsteam at 0.4 Mpa 2133.9

Solution:
, column with one and multiple feeds

kJkg-1
 DSP: Seminar 2, Binary distillation, McCabe-Thiele method, column with one fee
Data to Picture
Equlibrium 0 0
0.0055 0.0112 nF= 100 kmol/h nD= 77.77778
0.053 0.133 xF= 0.75 nW= 22.22222
0.125 0.24 q= 1
0.206 0.338 xD/Rmin+1 0.355
0.297 0.437 Rmin= 1.676056
0.51 0.63 R= 3.352113
0.649 0.751
0.803 0.866 xD= 0.95 xD/R+1= 0.218285
0.9594 0.9725 xw= 0.05 Steps 13.5
1 1 P= 101.325 kPa NTS 12.50

45 o line
0 0
1 1
q-line
0.75 0.75
0.75 0.83 1

0.9

0.8
Operating line in rectifying section
0.95 0.95 0.7
0 0.218285
0.6
F
y

0.75 0 0.5
0.75 0.75
0.4
D
0.95 0 0.3
0.95 0.95
0.2
W
0.05 0 0.1
0.05 0.05
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
x
umn with one feed

Δvhwater= 2214 kJkg-1K-1 MH2O 18 Kg/kmol

Δvhaa= 390 kJkg-1K-1 Maa 60.05 Kg/kmol
Psteam 0.4 Mpa
Δ vhsteam 2133.9 kJkg-1 nvm 338.4977

yw 0.13
Δv h v 25555.73 kJ/kmol/K
msteam 4053.87 kg/h

cpwater 4.18 kJ/kg/K

Δv h D 39030.38 kJ/kmol/K
dtH2O 20 K
mH2O 158034.6 kg/h

0.6 0.7 0.8 0.9 1

 DSP: Seminar 2, Binary distillation, McCabe-Thiele method, column with one fee
Data to Picture
Equlibrium 0 0
0.13 0.261 nF= 100 kmol/h nD= 41.17647
0.258 0.456 xF= 0.45 nW= 58.82353
0.411 0.632 q= 1
0.581 0.777 xD/Rmin+1 0.316667
0.78 0.9 Rmin= 1.999998
1 1 R= 3.999997

xD= 0.95 xD/R+1= 0.19

xw= 0.1
P= 101.325 kPa

45 o line
1
0 0
1 1 0.9
q-line
0.8
0.45 0.45
0.5 0.75641 0.7
0.6 1.369231
0.6
0.7 1.982051
y

0.8 2.594872 0.5

Operating line in rectifying section
0.4
0.95 0.95
0 0.19 0.3
F
0.45 0 0.2
0.45 0.45 0.1
D
0.95 0 0
0.95 0.95 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
W x
0.1 0
0.1 0.2
Stage 7.2 kuranglebih
NTS 6.20 Tanpa reboiler
umn with one feed

Δvhwater= 2214
Δvhaa= 390
Psteam 0.4
Δ vhsteam 2133.9

yw 0.13
Δv h v 25555.73
msteam 2465.659

Δv h D

q 1.195
q line slope 6.128205
Colum
nC
intercept -2.307692
Colum
nC
Colum
nC
Colum
nC
Colum
nB

0.6 0.7 0.8 0.9 1

kuranglebih
Tanpa reboiler
kJkg-1K-1 MH2O 18 Kg/kmol
kJkg-1K-1 Maa 60.05 Kg/kmol
Mpa
kJkg-1 nvm 205.8822

kJ/kmol/K
kg/h

cpwater 4.18 kJ/kg/K

Δv h D 39030.38 kJ/kmol/K
dtH2O 20 K
mH2O 96120.34 kg/h
 DSP: Seminar 2, Binary distillation, McCabe-Thiele method, column with multiple
Data to Picture
Equlibrium 0 0
0.0055 0.0112 nF1= 100 kmol/h nD=nF1*xF1+nF2*xF2-(nF1+nF2)*
0.053 0.133 xF1= 0.75 nW= nF1+nF2-nD=
0.125 0.24 q1= 1 nL1= 344.5227
0.206 0.338 nF2= 50 kmol/h nV1= 447.3005
0.297 0.437 xF2= 0.5 nL2= 444.5227
0.51 0.63 q2= 0.5 nV2= 447.3005
0.649 0.751 nL3= 469.5227
0.803 0.866 xD= 0.95 nV3= 422.3005
0.9594 0.9725 xw= 0.05
1 1 P= 101.325 kPa
steps 14.3
45 o line xD/Rmin+1 0.355 N 13.3
0 0 Rmin= 1.676056
1 1 R= 3.352113
q1-line
0.75 0.75 xD/R+1= 0.218285
0.75 0.83
q2-line
0.5 0.5
0.2 0.8
Operating line in section1
0.95 0.95
0 0.218285
F1 F2
0.75 0 0.5 0
0.75 0.75 0.5 0.5
D
0.95 0
0.95 0.95
Operating line in section 3 Operaiting line in section 2
0.05 0.05
0.5 0.55032
W
0.05 0
0.05 0.05
umn with multiple feeds

xF1+nF2*xF2-(nF1+nF2)*xW/(xD-xW)= 102.7778
nF1+nF2-nD= 47.22222
kmol/h

Optimal Feed stage 1 6

Optimal Feed stage 2 10
0 0.0055 0.053 0.125 0.206 0.297 0.51 0.649 0.803 0.9594
0 0.0112 0.133 0.24 0.338 0.437 0.63 0.751 0.866 0.9725

1 x-y diagram, Water-Acetic Acid

0.9

0.8

0.7

0.6
y

0.5
xd/Rmin+1 0.35
Rmin 0.4
1.714286 x'
R= 3.428571

xd/R+1 0.30.214516

0.2

0.1

0 x
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9

1.2

0.8
y

0.6
 1

0.8
y

0.6

0.4

0.2

0
0 0.2 0.4 0.6 0.8 1
x
 1
1

0 0
1 1

Acid
0.75 0
0.75 0.75

0.95 0
0.95 0.95

0.05 0
0.05 0.05

x'

0.8 0.9 1
1 1.2