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Microstructures
Fe3C (cementite)
-Eutectoid (B): austenite) R S
Fe3C 1000
+
+Fe3C
800
B 727°C = Teutectoid
R S
600
+Fe3C
400
0 1 2 3 4 5 6 6.7
(Fe) 0.77 4.30 Co, wt% C
120m
Ceutectoid
Hardness on metallographic
samples (Vicker’s)
Scanning Electron Microscope (SEM) &
Energy Dispersive X-ray Analyzer (EDAX)
• Fractography
• Wear debris
analysis
• Morphology /
Topography
• Elemental
analysis
Element Weight%
• Individual grains C 2.19
• Large depth of O 51.31
Mg 0.69
field Al 10.72
Si 23.68
• Nature of failure: K 0.36
• inter-granular Ca 8.53
Ti 0.37
Fe 1.53
Pd 0.61
Scanning Electron Microscope (SEM) &
Energy Dispersive X-ray Analyzer (EDAX)
MICROSTRUCTURES
OF
STEELS
Microstructure of Steel
Constituents structure Properties Microscope
apperance
Ferrite - Iron soft and ductile white
bcc
Pearlite alternate layers of Hard and ductile; dark
+ Fe3C ; gives toughness
Austenite - Iron Soft and ductile white
fcc
Ferrite Microstructure
Austenite
This is the structure of iron at high
temperatures (over 912 deg C).
Has a face-centre cubic (FCC) crystal
structure. This material is important in
that it is the structure from which other
structures are formed when the material
cools from elevated temperatures.
Often known as iron. Not present at
room temperatures.
Austenite Structure
Cementite
A compound of iron and carbon, iron
carbide (Fe3C).
Martensite Microstructure
50 m
Martensite Microstructure
Bainite
Hardness of Martensite as a
40 function of Carbon content
20 % Carbon →
Properties of 0.8% C steel
0.2 0.4 0.6
Constituent Hardness (Rc) Tensile strength
(MN / m2)
Coarse pearlite 16 710
Fine pearlite 30 990
Bainite 45 1470
Martensite 65 -
Martensite tempered 55 1990
at 250oC
EFFECTS OF ALLOYING
ELEMENTS
Effects of Alloying Elements
Typical Principle Effects
ranges (%)
Al <2 Aids nitriding, grain refining,
removes O in steel melting
S, P <0.5 Adds machinability, reduces
weldability, ductility and
toughness
Cr 0.3-4 Increases corrosion resistance,
hardenability, high-T strength;
form hard wear resistant carbide
Effects of Alloying Elements
Typical Principle Effects
ranges (%)
Ni 0.3-5 Austenite former, increase
hardenability and toughness
Cu 0.2-0.5 Aid atmospheric corrosion
resistance
Mn 0.3-2 Austenite former, increase
hardenability; combine with S to
reduce its adverse effects
Ceutectoid (wt%C)
0.8
0.6 Ni
Cr
0.4
TEutectoid (°C)
1200 Ti Si Si
Mo W Mn
0.2 W
1000 Ti Mo
Cr 0
800 0 4 8 12
Mn wt. % of alloying elements
600 Ni
0 4 8 12
wt. % of alloying elements
24
MORE MICROSTRUCTURES
Carbon Steel
Banded structure
Bainite
Structure
Martensite structure
Austenite Structure
Graphitisation
Sensitized microstructure
Sensitisation
Creep
Damage
Oxide filled crack
Internal Surface Oxide scale
Oxide Scale
Thermal Fatigue cracks
Copper particles in Internal deposit
IPW DMW Joint
Corrosion pits
Corrosion pit
Weld Pores
Remaining Life Assessment
(RLA)
VISUAL INSPECTION HARDNESS MEASUREMENT
-Dimension Portable Hardness Testers
-Documentation -Rebound technique
-Ultrasound technique
NDT TECHNIQUES
-Ultrasonic Test MECHANICAL
-DPT MEASUREMENT
-MPI, etc RLA -Portable ball indentation
-Small punch testing
CONICAL DIAMOND (CD) & SMALL BALL (SB); TRUNCATED (T); TRIANGULAR (TA)
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