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Experiment 4 & 5 SKL PDF
Experiment 4 & 5 SKL PDF
QUESTIONS
Activity 1:
1) Describe the steps used in the preparation of 250mL 0.1 M sodium hydroxide solution. (Use
diagram in your explanation.)
Calculation :
1.00 g
RESULTS
A B C D E Unknown
concentration
After KCNS was added
A B C D E Unknown
concentration
QUESTIONS
1) Calculate the volume that needs to be pipetted from stock solution for each new
concentration
REFERENCES
1) https://en.wikipedia.org/wiki/Iron(III)_chloride
2) https://www.extension.iastate.edu/wine/preparing-standard-sodium-hydroxide-solution
EXPERIMENT 5: TITRATION
RESULTS
2. Before you fill the burette, you should rinse it several times with the solution that will
eventually be in it. Why?
Rinsing the burette several times with the solution that will eventually be in it is to make sure
the concentration of the solution inside will be exactly what you expect it to be. Rinsing with
solution actually serves a simple but very practical purpose.
4. What is other precaution should you take while doing titration experiments?
One of precaution that we should take while doing titration is pay very close attention to the
color of the indicator as one extra drop of titrant could possibly shoot the solution past the
equivalence point. To avoid further error, make sure the burette being used is not a faulty one
as accidental leaks often lead to overshooting the equivalence point.
CONCLUSION.
We run this experiment is to determine the molarity HCl which is strong base by titrating with the
certain volume of strong base, we use NaOH. The data gathered by titrating the unknown solution
with a standardized solution provides the equilibrium point, and how many moles of the titrant were
needed to reach this equilibrium point. By using the stoichiometric ratios of the two solutions in the
titration and the equation C = n/v, one can calculate the concentration of the NaOH solution.