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Construction and Building Materials 123 (2016) 444–453

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Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Effects of morphological characteristics of aggregate particles on the


mechanical behavior of bituminous paving mixtures
Francisco Thiago Sacramento Aragão a,⇑, Abraham Ricardo Guerrero Pazos a, Laura Maria Goretti da Motta a,
Yong-Rak Kim b, Luis Alberto Herrmann do Nascimento c
a
Department of Civil Engineering, Federal University of Rio de Janeiro/COPPE, Rio de Janeiro 21941-596, Brazil
b
Department of Civil Engineering, 362N Whittier Research Center, University of Nebraska, Lincoln, NE 68583, United States
c
Cenpes/Petrobras, Asphalt Research Laboratory, Avenida Horácio de Macedo, 950, Rio de Janeiro 21941-915, Brazil

h i g h l i g h t s

 HMA rutting resistance is strongly correlated with coarse aggregate morphology.


 Direct and objective measurements of aggregate shape should be pursued.
 Shape properties characterized at AIMS 2 strongly correlate with rutting resistance.
 Surface texture should be considered in aggregate and HMA specifications.

a r t i c l e i n f o a b s t r a c t

Article history: This study evaluates the influence of morphological properties of aggregates on the mechanical behavior
Received 26 February 2016 of bituminous mixtures. For that, two aggregates with different characteristics, i.e., round river gravel and
Received in revised form 27 May 2016 crushed gneiss, were used in the research. Laboratory tests were conducted to characterize morphological
Accepted 6 July 2016
properties of the aggregates following traditional methodologies and using a modern image analysis sys-
Available online 16 July 2016
tem, AIMS 2. Six asphalt mixtures containing different proportions of gravel and crushed gneiss were
designed according to the Superpave methodology and evaluated in mechanical performance tests. The
Keywords:
results obtained indicated that aggregate morphological characteristics, especially those of coarse parti-
Asphalt mixtures
Aggregates
cles, are strongly correlated with the resistance to rutting of the asphalt mixtures. In addition, AIMS 2 was
Morphological properties shown to provide more direct and scientific measurements of aggregate morphological characteristics
Mechanical behavior that present higher correlations with the mixture performance than traditional methodologies. Finally,
the results also demonstrated that the aggregate surface texture is highly correlated to the performance
of the mixtures and should be carefully considered in aggregate and asphalt mixture specifications.
Ó 2016 Elsevier Ltd. All rights reserved.

1. Introduction The four consensus properties identified by SHRP researchers as


key characteristics directly related to the performance behavior of
In order to improve the performance, durability, safety, and the mixtures were coarse- and fine-aggregate angularity, amount
efficiency of asphalt mixtures, the Strategic Highway Research of flat and elongated particles in coarse aggregates, and sand
Program (SHRP), established in 1987, proposed the Superpave equivalency of fine aggregates. The criteria specified for these
system in 1993. Superpave included a set of significant advance- properties are generally function of the traffic volume expected
ments in the methodologies used to classify asphalt binders and in the area where the flexible pavement will be built. On the other
to design asphalt mixtures. In addition, the Superpave system also hand, the characterization of source properties is considered
defined the so-called consensus and source properties of aggregate optional and the corresponding limiting criteria are specified based
particles. on the experience of the local transportation agencies to account
for the regional geological differences.
Several research efforts have demonstrated reasonable to good
⇑ Corresponding author. correlations between the consensus properties of aggregates spec-
E-mail addresses: fthiago@coc.ufrj.br (F.T.S. Aragão), aguerrero@coc.ufrj.br ified by the SHRP and the overall mechanical behavior of asphalt
(A.R.G. Pazos), laura@coc.ufrj.br (L.M.G. Motta), ykim3@unl.edu (Y.-R. Kim). mixtures [1–7]. However, in the last years, researchers have

http://dx.doi.org/10.1016/j.conbuildmat.2016.07.013
0950-0618/Ó 2016 Elsevier Ltd. All rights reserved.
F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453 445

criticized some of these tests [6,8–13], which are often considered research. Three other mixtures were designed and contained the
to be subjective and/or based on indirect measurements and to following proportions (by weight) of crushed gneiss and gravel,
produce results that are a function of the skills of the operator. respectively: (a) 75% and 25%; (b) 50% and 50%; and (c) 25% and
Some testing procedures, such as the one specified for the determi- 75%. Finally, a sixth mixture composed of crushed gneiss with flat
nation of the coarse aggregate angularity, can also be tedious and and elongated (F&E) characteristics was also designed. This aggre-
time-consuming. gate was obtained in the same quarry as the cubic crushed gneiss,
Considering the relevance of aggregates and the corresponding but processed using a different crushing strategy. Thus, the effect
effects of their properties on the overall behavior of asphalt mix- of aggregate morphological characteristics could be better evalu-
tures and on the costs related to the production and maintenance ated, given that both cubic and elongated crushed gneisses pre-
of flexible pavements, the study of alternative methodologies that sented similar geological and physical properties. Fig. 1 shows
are able to characterize aggregates properties in more objective samples of the three aggregates used in this study.
and representative manners becomes a very important task. In that Tables 1 and 2 present aggregate gradation and volumetric
sense, several researchers have adopted protocols to identify characteristics, respectively, of the six mixtures evaluated in this
aggregate morphological properties based on image analysis study, as well as the limiting criteria for a nominal maximum
techniques, including VDG-40 Videograder, Computer Particle aggregate size of 19 mm and the traffic level between 3 and 10 mil-
Analyzer, Micromeritics OptiSizer PSDA, VideoImaging System lion ESALs, according with AASHTO M 323 [14]. All mixtures
(VIS), Buffalo Wire Works PSSDA, Camsizer, Wipshape, University required the same binder content, i.e., Pb = 4.3% to generate air
of Illinois Aggregate Image Analyzer (UIAIA), Aggregate Imaging voids (Va) between 3.6% and 3.8%.
System (AIMS). Masad et al. [8] compared several of these image Mixtures containing higher amounts of gravel presented lower
analysis systems and identified AIMS as the most promising equip- values of voids in mineral aggregates (VMA), which is in accor-
ment as it allows a comprehensive, objective, and direct analysis of dance with the observation by several researchers [15–18].
shape, angularity, and texture based on two-dimensional and Rounded and less angular aggregates generally present smooth
three-dimensional images of aggregate particles. surfaces, which in combination to the absence of angular edges
This study evaluates the effects of morphological properties of facilitates the compaction of the particles in denser structures
aggregate particles on the overall mechanical behavior of asphalt and reduces the VMA values [15]. The voids filled with asphalt
mixtures. For that, properties of two aggregates with distinct mor- (VFA) were also lower for those mixtures, although within the
phological characteristics, i.e., round river gravel and crushed limits specified by AASHTO M 323 [14].
gneiss, were first characterized based on the specifications of the The percent theoretical maximum specific gravity @ Ninitial
Superpave system. Alternatively, aggregate morphological charac- (%Gmm @ Nini) for the mixtures containing gravel was higher than
teristics were also determined using the second generation of the for the mixtures composed of crushed gneiss only, which may indi-
modern image analysis system AIMS (i.e., Aggregate Imaging Mea- cate a higher sensitivity to the compaction effort during construc-
surement System 2: AIMS 2). To further identify the effects of the tion and a more unstable behavior under traffic loads. The percent
different morphological properties of aggregates on the overall theoretical maximum specific gravity @ Nmaximum (%Gmm @ Nmax)
performance behavior of asphalt mixtures, six mixtures compris- decreased as more gravel was added to the mixture, although all
ing different amounts of gravel and crushed gneiss were designed mixtures met the specified criterion for this parameter. Finally,
based on Superpave mix design specifications, and their perfor- all mixtures presented similar dust to binder ratio (D/B) within
mance behavior was compared to the morphological characteris- the allowed limits.
tics of their aggregate skeleton.
2.2. Characterization of aggregate properties
Specific objectives of this paper are:
Morphological characteristics of aggregate particles based on
 To characterize aggregate particles with distinct morphological
Superpave specifications for consensus properties, i.e., flat and
properties based on Superpave specifications and using the
elongated particles (F&E), coarse aggregate angularity (CAA) and
image analysis system AIMS 2.
fine aggregate angularity (FAA), were first determined. In addition,
 To characterize the mechanical behavior of asphalt mixtures
the test of uncompacted voids described in AASHTO T326 [19] was
containing different amounts of gravel and crushed gneiss. For
also performed because several authors have indicated that this
that, three primary mixture characteristics are evaluated: stiff-
test presents better correlation with the mechanical behavior of
ness, permanent deformation, and cracking.
asphalt mixtures than the typical Superpave CAA test [4,20], which
 To identify correlations between the morphological properties
is based on the amount of fractured faces in the aggregate particles.
of the aggregates evaluated and the mechanical behavior of
Additional characterizations of the aggregates included the deter-
the corresponding asphalt mixtures.
mination of specific gravity, absorption capacity, sand equivalency,
and Los Angeles abrasion.
2. Experimental program Finally, aggregates were tested in the AIMS 2 system before and
after Los Angeles tests to identify their ability to retain the mor-
2.1. Materials and mix design phological characteristics after abrasion. AIMS 2 is a robust image
analysis system that has been used by several researchers to char-
One PG 70-16 S binder obtained from a refinery in Rio de acterize morphological properties of aggregate particles, such as
Janeiro, Brazil, and two types of aggregates, i.e., gravel from the angularity, sphericity, flatness, elongation, and texture. The system
state of Pará, Brazil, and crushed gneiss from Rio de Janeiro were combines a high-resolution camera, lighting, and a microscope to
used in this study. perform the analysis. The AIMS 2 turntable uses removable trays,
Six mixtures with the same aggregate gradation were designed selected by the aggregate size being analyzed, which accommodate
based on Superpave specifications. The first mixture contained the aggregate particles during the tests. An algorithm implemented
crushed gneiss with cubic particles. The second mixture was com- on the operating software of the system allows the automatic elim-
posed of gravel and natural sand. The use of natural sand as the ination of touching particles and their corresponding characteris-
fine part of gradations containing gravel as coarse aggregates has tics are not reported in the results. This is a very important
been a common practice in Brazil and this has been adopted in this feature of the system because touching particles can be
446 F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453

Fig. 1. Aggregates used in this study: (a) cubic crushed gneiss; (b) F&E crushed gneiss; and (c) round river gravel.

Table 1 aggregates obtained from analyses in the AIMS 2 system. Fig. 2


Mixture gradations in this study. shows examples of particles with distinct morphological charac-
Mesh opening % Cumulative passing Limits teristics and the values adopted by AIMS 2 to quantify these
(mm) (by weight)
Minimum Maximum
characteristics.

25.400 100.00 100 100


19.100 99.86 80 100
2.3. Laboratory tests of asphalt mixtures
12.500 78.95 – –
9.500 66.46 60 80 Mixture stiffness was measured in the form of the linear vis-
6.250 58.54 – – coelastic dynamic modulus, obtained from uniaxial tests of cylin-
4.750 54.53 48 65
drical specimens measuring 100 mm in diameter and 150 mm in
2.360 39.55 35 50
1.180 29.71 – – height. Each specimen was cored and cut from Superpave gyratory
0.600 22.02 19 30 compactor (SGC) samples measuring 150 mm in diameter and
0.300 15.02 13 23 170 mm in height. During the tests, the loading levels were care-
0.150 8.29 7 15 fully adjusted until the strain levels were within the range of
0.075 4.01 0 8
0.00005–0.00010. Three linear variable differential transformers
(LVDTs) were mounted onto the surface of the specimens at 120°
radial intervals with a 100-mm gauge length. Averaged vertical
erroneously interpreted as a single particle and compromise the deformations were used to calculate the dynamic modulus, simply
accuracy of the morphological analysis. defined as the ratio of the sinusoidal stress amplitude to the sinu-
AIMS 2 allows two-dimensional characterizations of angularity soidal strain amplitude. As suggested in AASHTO T 342 [21], five
and shape of fine aggregates comprising materials passing the temperatures (10.0; 4.4; 21.1; 37.8; 54.0 °C) and six loading fre-
4.75 mm (No. 4) sieve and retained on the 0.075 mm (No. 200) quencies (0.1; 0.5; 1.0; 5.0; 10.0; 25.0 Hz) were used, and the
sieve. For larger particles with dimensions between 37.5 mm and frequency-temperature superposition concept was applied to
4.75 mm, the system characterizes coarse aggregate angularity, develop master curves representing the dynamic modulus of the
sphericity, flatness, elongation, and texture. The results are pre- mixtures. Three replicates were tested for each mixture.
sented as cumulative distributions or represented by a characteris- The resistance to damage of the six mixtures was evaluated
tic value for each property. Masad et al. [8] have defined categories based on the results of two experiments, i.e., the flow number
for each property based on the morphological characteristics of (FN) and the indirect tensile (IDT) fracture energy tests. The FN test

Table 2
Volumetric characteristics of the mixtures evaluated in this study.

Property Pb (%) Va (%) VMA (%) VFA (%) D/B %Gmm @ Nini %Gmm @ Nmax

Criterion – 4.0 ± 1.0 >13.0 65.0–75.0 0.60–1.20 <89.0 <98.0


F&E gneiss 4.3 3.6 13.2 73.0 1.05 87.5 97.5
Cubic gneiss 4.3 3.8 13.3 71.6 1.02 88.7 97.2
75% gneiss, 25% gravel 4.3 3.6 13.0 71.0 1.03 89.1 97.4
50% gneiss, 50% gravel 4.3 3.8 12.6 69.5 1.04 89.0 97.1
25% gneiss, 75% gravel 4.3 3.7 12.2 69.7 1.05 89.8 97.1
Gravel 4.3 3.8 11.7 67.0 1.06 89.7 97.0
F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453 447

(a) Cubic Crushed Gneiss (b) Gravel


AIMS 2 Angularity = 2.969 AIMS 2 Angularity = 2.071

(c) Cubic Crushed Gneiss (d) Gravel


AIMS 2 Texture = 347 AIMS 2 Texture = 120
Fig. 2. Examples of digital images from AIMS 2: particles with different (a) and (b) angularity; (c) and (d) texture.

was performed to assess the resistance of the mixtures to perma-  ep10 = plastic deformation in the 10th cycle (le); and
nent deformation, while the IDT test was used to evaluate the  FN = flow number (cycle).
resistance of the mixtures to cracking.
For the FN tests, specimens of 100 mm in diameter and 150 mm The traditional laboratory procedures adopted for the charac-
in height were fabricated with a SGC. During the tests, the cylindri- terization of the asphalt mixture fatigue cracking are generally
cal specimens were conditioned to 60 °C and then subjected to a quite time-consuming sometimes requiring several weeks or even
compressive cyclic uniaxial load of 204 kPa. Each cycle was com- months. Thus, alternative and more efficient methodologies have
posed of a pulse of 0.1 s followed by a rest period of 0.9 s. The ver- been pursued by researchers in the last years. One of these alterna-
tical displacement was monitored by LVDTs mounted on the tive procedures is the IDT fracture energy test with the application
surface of the samples and used to calculate the plastic deforma- of monotonic loads. According to Kim et al. [23], the fracture
tion accumulated in each cycle, which was defined as the ratio energy obtained from the area under stress-strains curves is well
between the unrecoverable displacement and the gauge length of correlated with the resistance of asphalt mixtures to fatigue crack-
the LVDTs (100 mm). Three replicates were tested for each ing, both for laboratory-fabricated specimens and for field cores. In
mixture. addition to the good correlation with the mixture performance, the
The FN is associated to the cycle where the rate of plastic defor- IDT fracture energy test is easy to perform and considerably less
mation reaches a minimum value, after which the material experi- time-consuming than traditional fatigue tests that typically require
ences increasing deformation rate with the evolution of the loading several weeks or months of testing for the construction of curves
cycles within the so-called tertiary zone of deformation. Another relating the cycles to failure with the different levels of strain of
parameter obtained from FN tests, i.e., the plastic deformation rate stress applied to the samples.
of the secondary (linear) zone, has also been shown to correlate In this study, the IDT fracture energy test was performed with
well with the resistance of the mixtures to permanent deformation specimens of 100 mm in diameter and 38 mm in height extracted
[22]. The so-called b-parameter has been determined in this paper from SGC samples that measured 150 mm in diameter and
using Eq. (1). In the equation, the 10th cycle was defined as the ini- 115 mm in height. Gauge points were glued over a 25.4 mm gauge
tial point of the secondary zone based on the observation that this length in the center of each specimen on both faces to measure
cycle is typically within that zone for asphalt mixtures. The FN the horizontal and vertical displacements during the tests. A
cycle was chosen as a limit between the secondary and tertiary constant crosshead displacement rate of 50 mm/min. was applied
zones. to the specimens at 20 °C. Three replicates were tested for each
mixture.
epFN  ep10
b¼ ð1Þ Using the horizontal displacements measured, the strain at the
FN  10 center of the specimen was calculated using Eq. (2). In this study,
where the values adopted for c1 , c2 , c3 , and c4 we, respectively, 12.400,
37.700, 0.291, and 0.908 [23,24]. The stress at the center of the
 b = deformation rate in the secondary zone (le/cycle); specimen could also be calculated based on Eq. (3) [25]. Then,
 epFN = plastic deformation in the FN cycle (le); stress-strain curves could be plotted and fracture energy was
448 F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453

defined as the area under the stress-strain curves until the peak The results of the alternative CAA test specified by AASHTO
stress [23]. T326 [19] also indicated higher angularity values for the crushed
gneisses, as expected. However, the difference between extreme
c1 þ tc2
ex¼0 ðtÞ ¼ UðtÞ ð2Þ values, i.e., for cubic crushed gneiss and gravel, was significantly
c3 þ tc4 smaller for the alternative test (11%) than for the Superpave CAA
where test (71%), which shows that the measuring scale for the Superpave
CAA test is much more sensitive to variations in the particle
 ex¼0 ðtÞ = strain at the center of the specimen; angularity.
 U(t) = horizontal displacement (m); Additionally, based on the recommendation by White et al. [4]
 c1 , c2 , c3 , and c4 = coefficients related to the specimen diam- of CAA values above 45%, only the mixture composed solely by
eter and gauge length used; and gravel presented CAA below this limit, which again may indicate
 t. Poisson’s ratio. that this mixture is potentially more susceptible to permanent
deformation than the others evaluated. However, based on the
2PðtÞ results of this test, combinations of crushed gneiss and gravel
rx¼0 ðtÞ ¼ ð3Þ may present satisfactory performance.
ptd
As for F&E characteristics, Table 3 indicates that the F&E
where crushed gneiss was about twice as flat and elongated as the other
aggregates, considering the 5:1 ratio between the larger and the
 rx¼0 ðtÞ. stress at the center of the specimen (Pa); smaller dimensions of the particles, as specified by Superpave.
 P(t) = applied force (N); Some researchers have indicated that 5:1 is not the most appropri-
 t = specimen thickness (m); and ate ratio to determine F&E characteristics of aggregate particles.
 d = specimen diameter (m). Instead, other ratios, such as 2:1 and 3:1, are often recommended
[26]. As shown in Table 2, while only 1.6% of the particles of the
3. Results and discussion F&E crushed gneiss were considered F&E based on the Superpave
5:1 ratio, 51.7% and 20.4% of the particles were characterized as
3.1. Aggregate properties F&E based on the ratios 2:1 and 3:1, respectively.
Sand equivalent results met the Superpave requirements (>45%)
Table 3 presents results of the different combinations of aggre- for all combinations and larger values were obtained for mixtures
gates evaluated in this study based on conventional testing proce- containing gravel. Finally, Table 3 also indicates that the resistance
dures. It can be observed that both crushed gneisses presented to abrasion was inversely proportional to the amount of gravel in
higher specific gravities, but were less absorptive than the gravel. the combinations.
The crushed gneisses also presented higher values for both FAA Following the characterization of aggregate properties by con-
and CAA than the gravel, as expected. All combinations of fine ventional Superpave procedures, aggregate morphological proper-
aggregates presented FAA values above 45%, which is the mini- ties of the six mixtures evaluated in this study were also
mum FAA specified by Superpave for the traffic level (i.e., 10 mil- determined using the AIMS 2 system. As aforementioned, AIMS 2
lion ESAĹs) that mixtures containing the PG 70-16 S binder need presents the results as cumulative distributions. However, the sys-
to support. On the other hand, CAA values for combinations con- tem may also provide a characteristic value for each property
taining gravel were lower than the minimum criteria specified by based on the weighted average of the properties for the different
Superpave for one or more and two or more fractured faces, i.e., sizes analyzed. Table 4 summarizes the characteristic values
85% and 80%, respectively. This may indicate that mixtures com- obtained for several aggregate properties.
prising gravel tend to be more susceptible to permanent The 2D fine aggregate form quantifies the relative shape of fine
deformation. aggregates based on Eq. (4). A perfect circle has 2D fine aggregate

Table 3
Aggregate characteristics based on conventional Superpave methods.

Property (Standard) F&E Crushed Cubic Crushed 75% Gneiss, 25% 50% Gneiss, 50% 25% Gneiss, 75% Gravel Criterion⁄⁄
Gneiss Gneiss Gravel Gravel Gravel

Gsb [27] 2.696 2.695 2.664 2.634 2.605 2.576 –

Gsa [27] 2.759 2.758 2.730 2.702 2.674 2.648 –
Absorption [27], % 0.81 0.82 0.85 0.88 0.92 0.96 –
Flat and elongated particles [28], %
2:1 ratio 51.7 33.4 31.3 29.2 27.1 25.0 –
3:1 ratio 20.4 4.6 4.1 3.7 3.2 2.7 –
5:1 ratio 1.6 0.8 0.8 0.8 0.9 0.9 <10
Fractured faces [29], %
1 or more 100 100 82 65 47 29 >85
2 or more 100 100 79 57 36 14 >80
Coarse aggregate angularity – uncompacted 50.4 49.9 48.7 47.5 46.0 44.5 –
voids [19], %
Fine aggregate angularity –uncompacted 49.2 49.2 48.2 47.6 46.9 46.5 >45
voids [30], %
Sand equivalent [31], % 71 71 73 76 78 80 >45
Los Angeles abrasion [32], % 20.7 19.7 32.2 41.7 52.1 61.1 –

Gsa and Gsb are the apparent and bulk specific gravities of aggregates, respectively.
⁄⁄
Limiting criteria for Superpave consensus properties for a traffic volume between 3 and 10 Million ESALs and depth from surface smaller than 100 mm [14].
F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453 449

Table 4 mixtures with higher resistance to sliding, which improves the


Aggregate characteristics based on AIMS 2 testing procedures. safety level of the roads for users [33–36].
Property Scale F&E Crushed Cubic Crushed Gravel Despite the recognized importance of surface texture, to the
Gneiss Gneiss authors’ best knowledge, there is no well-established methodology
2D form (fine) 0–20 8.25 7.79 to quantify this property, except from visual or tactile indirect
Fine aggregate 0–10.000 3.303 2.789 assessments. In this context, AIMS 2 appears as a promising alter-
angularity native for the quantification of the surface texture of aggregate
Coarse aggregate 0–10.000 2931 2969 2071
angularity
particles [34–36]. In AIMS 2, coarse aggregate surface texture is
F&E 2:1 (coarse) – 24.5 14.9 11.4 characterized by values ranging between 0 and 1000, where 0 rep-
F&E 3:1 (coarse) – 8.4 2.6 1.1 resents a perfectly polished surface. AIMS 2 adopts the wavelet
F&E 5:1 (coarse) – 3.3 0.3 0.4 method to quantify coarse aggregate texture. The wavelet analysis
Texture (coarse) 0–1.000 338 347 120
gives the texture details in the horizontal, vertical, and diagonal
Sphericity (coarse) 0–1 0.72 0.74 0.76
Angularity – texture 0–14.000 4848 4956 2191 directions in three separate images. The texture index at a given
(coarse) decomposition level is the arithmetic mean of the squared values
of the wavelet coefficients for all three directions, as expressed in
Eq. (6). As shown in Table 4, the crushed gneisses were about 3
times rougher than the gravel. Both crushed gneisses presented
form equals to 0, in a scale that ranges between 0 and 20. From
similar surface texture values. This was expected, given that both
Table 4, it can be observed that the crushed gneisses presented
were obtained from the same quarry.
2D form larger than the gravel, which indicates that the latter is
a rounder material. It is important to note that the same fine mate-
1 X3 X N
rial was used for both types of crushed gneisses. Texture ¼ ðDij ðx; yÞÞ2 ð6Þ
3N i¼1 j¼1

XDh
360
RhDh  Rh where
Form 2D ¼ ð4Þ
0
Rh
 D = decomposition function;
where  n = decomposition level;
 N = total number of coefficients in an image;
 Form 2D = 2D form of the fine aggregate;  i = 1, 2, or 3 for detailed images;
 Rh = radius of the particle at an angle h; and  j = wavelet index; and
 Dh = incremental difference in the angle.  x,y = location of the coefficients in transformed domain.

The crushed gneisses were more angular than the gravel, as As indicated in Eq. (7), coarse aggregate sphericity describes the
expected, both for FAA and CAA. In AIMS 2, angularity (for both, 3D shape of the particles in a scale that varies between 0 and 1,
coarse and fine) is quantified based on the change in the gradient where 1 represents a particle with equal dimensions in the 3 direc-
on a particle boundary and is related to the sharpness of its cor- tions of a Cartesian coordinate system. According to Table 4, the
ners, according to Eq. (5): gravel was the aggregate with the largest sphericity, followed by
the cubic and the F&E crushed gneisses.
1 X n¼3
sffiffiffiffiffiffiffiffiffi
Angularity ¼ n jhi  hiþ3 j ð5Þ ds dI
3
 1 i¼1 Sphericity ¼ 3 ð7Þ
2
dL
where
where
 h = angle of orientation of the edge points;
 n = total number of points; and  ds = particle shortest dimension;
 i = denotes the ith point on the edge of the particle.  dI = particle intermediate dimension; and
 dL = particle longest dimension.
The coarse aggregate F&E characteristics were determined for 3
ratios between the dimensions of the particles, i.e., 2:1, 3:1, and Finally, the coarse aggregate angularity-texture (CAAT) index
5:1. The F&E crushed gneiss was obviously the aggregate with represents a combination of texture and angularity characteristics
the most F&E particles for all 3 ratios and was followed by the of the aggregates and is calculated using Eq. (8). In this study, the
cubic crushed gneiss. As for the Superpave F&E test, the 3:1 and crushed gneisses presented CAAT values much larger than the
2:1 ratios distinguished more clearly the F&E characteristics of gravel, as expected.
the F&E crushed gneiss than the 5:1 ratio. While only 3.3% of the
CAAT ¼ 10  ðTextureÞ þ 0:5  ðAngularityÞ ð8Þ
particles were considered F&E when the 5:1 ratio was adopted,
8.4% and 24.5% of the particles were considered F&E for the 3:1 where CAAT = coarse aggregate angularity-texture.
and 2:1 ratios, respectively. Finally, morphological properties of the coarse aggregates eval-
In addition to shape, angularity, and F&E characteristics, surface uated in this study were also characterized after the particles were
texture has been identified as a key morphological property of subjected to the Los Angeles abrasion. For instance, CAA of the
aggregate particles. It affects important mixture characteristics, crushed gneiss particles was reduced by 17.6% after the abrasion
such as workability, adhesive properties, internal friction, among test. On the other hand, gravel particles were more angular after
others. The use of aggregates with rougher surfaces generally the Los Angeles abrasion process. A visual inspection revealed that
results in mixtures with lower workability and that require more gravel particles were fractured as a result of the impact of the
binder, but with higher resistance to shear failure. Several research metallic spheres during the Los Angeles test. This created new par-
efforts have also demonstrated that the use of aggregates that ticles with more angular edges, which affected the angularity mea-
retain their surface texture characteristics after abrasion generates surements. In addition, the fracture of the aggregate particles also
450 F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453

revealed internal surfaces of the particles that were rougher than cubic gneiss and gravel resulted in mixtures with similar stiffness
the original external surfaces. Although indicating that the Los which corresponded to 70% of stiffness of the mixture with F&E
Angeles abrasion may not be the most adequate procedure to eval- gneiss. The gravel-only mixture presented the lowest stiffness that
uate the ability of aggregate particles to retain their morphological was 34% lower than that of the mixture with F&E gneiss.
characteristics, these results also indicate that crushing gravel par- At 10+1 Hz, the cubic gneiss mixture was the stiffest and was
ticles to be used in the composition of asphalt mixtures in the field followed by the mixture with F&E gneiss, which was 8% less stiff.
may be a good strategy to improve some of the aggregate morpho- Both mixtures were stiffer than the other mixtures evaluated.
logical characteristics, such as angularity and texture. The combinations of different aggregates resulted in mixtures with
similar stiffness values, which were around 20% lower than that of
3.2. Asphalt mixture performance behavior the mixture with cubic gneiss. The gravel-only mixture was 44%
less stiff than the mixture with cubic gneiss.
Fig. 3a shows dynamic modulus master curves of the six mix- At 10+6 Hz, the cubic gneiss mixture was also the stiffest. At this
tures evaluated at the reference temperature of 25 °C. The crushed frequency, all mixtures but the one composed solely of cubic gneiss
gneiss-only mixtures presented similar dynamic moduli and were presented similar stiffness values that were between 14% and 22%
generally stiffer than the mixture composed solely of gravel. Mix- lower than that of the mixture composed of cubic gneiss. Finally,
tures composed of combinations of cubic crushed gneiss and gravel mixtures containing F&E gneiss-only or gravel-only were the most
presented similar stiffness characteristics and were stiffer than the susceptible to variations in the loading frequency. The relative
mixture composed of gravel only. stiffness of the F&E gneiss mixture decreased with the increasing
In an attempt to make a clearer comparison among the different loading frequency, whereas the gravel-only mixture presented
mixtures, dynamic modulus values at three distinct frequencies, the lowest relative stiffness at the intermediate frequency
104, 10+1, and 10+6 Hz were plotted in Fig. 3b, c, and d, respec- evaluated.
tively. In each figure, the dynamic moduli were normalized by Table 5 shows FN results at 60 °C. The mixture composed of
the maximum stiffness obtained among the six mixtures at the cubic crushed gneiss was the most resistant to permanent
corresponding frequency evaluated. deformation, with higher FN and lower b-parameter, whereas the
At 104 Hz, the mixture composed of F&E gneiss was 11% stiffer gravel mixture was the most susceptible to permanent deforma-
than the mixture containing cubic gneiss. The combinations of tion. As more cubic crushed gneiss was combined with gravel, a

F&E Gneiss Cubic Gneiss 1.25


Gravel 75% Gneiss 25% Gravel 1.00
Normalized Dynamic

1.E+05
50% Gneiss 50% Gravel 25% Gneiss 75% Gravel 1.00 0.89
Modulus

0.70 0.69 0.72 0.66


Dynamic Modulus (MPa)

0.75

1.E+04 0.50

0.25

1.E+03 0.00

1.E+02
1.E-05 1.E-02 1.E+01 1.E+04 1.E+07

Reduced Frequency (Hz)


(a) (b)

1.25 1.25
0.92 1.00 1.00
Normalized Dynamic

Normalized Dynamic

1.00 0.83 0.82 1.00 0.83 0.86 0.83 0.85 0.78


0.75
Modulus

Modulus

0.75 0.56 0.75

0.50 0.50

0.25 0.25

0.00 0.00

(c) (d)
Fig. 3. Dynamic modulus results at 25 °C: (a) master curves for all mixtures; results at (b) 1E4 Hz; (c) 1E+1 Hz; and (d) 1E+6 Hz.
F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453 451

Table 5 Table 6
FN results. Coefficients of determination between morphological properties of aggregates and
performance of asphalt mixtures.
Mixture Flow number b (le/cycle)
Correlations with FN
F&E gneiss 203 32.3
Cubic gneiss 340 22.0 Test (Standard) R2
75% gneiss, 25% gravel 243 31.8
AIMS 2 – texture 0.84
50% gneiss, 50% gravel 187 37.5
AIMS 2 – CAAT 0.84
25% gneiss, 75% gravel 153 46.7
AIMS 2 – CAA 0.84
Gravel 107 68.9
Superpave – CAA [29] 0.82
Uncompacted voids – CAA [19] 0.76
Superpave – FAA [30] 0.74
considerable enhancement on the resistance to rutting was AIMS 2 – FAA 0.54
AIMS 2 – sphericity 0.30
observed. This resulted from the better aggregate interlock and
Superpave – F&E 5:1 [28] 0.25
higher internal friction among particles with cubic shapes and F&E 2:1 [28] 0.21
rougher surfaces, which improved the ability of the mixtures to F&E 3:1 [28] 0.10
resist damage by the accumulation of permanent deformation.
Correlations with fracture energy
IDT fracture energies at 20 °C are presented in Fig. 4. The mix-
ture with F&E crushed gneiss was the least resistant to fracture. Test (Standard) R2
Mixtures containing combinations of cubic crushed gneiss and Superpave – F&E 5:1 [28] 0.34
gravel could absorb more energy before fracture than the mixture AIMS 2 – texture 0.31
composed solely of gravel. In addition, the resistance to fracture AIMS 2 – CAAT 0.30
AIMS 2 – CAA 0.30
increased as more cubic crushed gneiss was added to the mixtures. AIMS 2 – sphericity 0.30
Superpave – CAA [29] 0.28
3.3. Correlations between morphological properties and mixture Superpave – FAA [30] 0.24
Uncompacted voids for CAA [19] 0.22
performance
AIMS 2 – FAA 0.07
F&E 3:1 [28] 0.06
Before correlating aggregate properties with mixture perfor- F&E 2:1 [28] 0.01
mance, ANOVA (Analysis of Variance) tests were conducted to
determine if there is significant statistical difference between the
FN and IDT fracture energy values from the different combinations key morphological characteristic should be included in aggregate
of aggregates evaluated in this study. An a-value of 0.05 was specifications, given that it affects both functional (e.g., skid resis-
selected to conduct this analysis and resulted in a critical F-value tance) and structural properties of asphalt mixtures and
of 3.11. Considering the F-values of 8.59 and 2.93 obtained for pavements.
the results of the FN and IDT fracture energy tests, respectively, Table 6 also shows that coarse aggregate properties generally
it can be concluded that there is a significant difference among presented higher correlation with the resistance to rutting than
the FN values but not among the IDT fracture energy values. fine aggregate properties, except for the three F&E ratios evaluated,
Table 6 indicates the coefficients of determination (R2) obtained i.e., 5:1, 3:1, and 2:1, which presented relatively low R2 values of
from the comparison between the aggregate morphological prop- 0.25, 0.10, and 0.21, respectively. However, the F&E aggregate
erties and the performance behavior of the corresponding asphalt characteristic is typically more related to construction issues than
mixtures. The three properties that were best correlated with the to problems during the service life because F&E particles tend be
resistance to rutting were obtained from AIMS 2 and presented less resistant to fracture during the compaction of asphalt
R2 equal to 0.84, as seen in Fig. 5. Those properties were texture, mixtures.
coarse aggregate angularity-texture index, and coarse aggregate As for the comparison between aggregate properties and IDT
angularity. fracture energy results, R2 values were much lower than those
In addition to highlight the good correlation of AIMS 2 aggre- obtained in the comparison with FN results. This was expected
gate properties with the mixture resistance to rutting, these results because it is a common sense in the flexible pavement research
also clearly indicate the relevance of texture as a particle charac- community that the resistance to fatigue damage of asphalt mix-
teristic that affects the mixture performance. This implies that this tures is more related to binder than to aggregate properties.

16,000
Fracture Energy (Pa)

14,000 13,380
12,523 12,294
12,000 11,420 11,595 11,511

10,000

8,000

Fig. 4. IDT fracture energy test results for the six mixtures evaluated in this study.
452 F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453

400 400
350 y= 1.6326x0.8739 350
y = 29.71x0.4706
300 R² = 0.8406 300 R² = 0.8183

FN (cycles)
FN (cycles)
250 250
200 200
150 150
100 100
50 50
0 0
100 200 300 400 0 50 100 150
Texture (AIMS scale) CAA

400 400
350 y= 0.0183x1.1297 350 y = 5E-07x2.5299
300 R² = 0.8396 300 R² = 0.8353

FN (cycles)
FN (cycles)

250 250
200 200
150 150
100 100
50 50
0 0
0 2000 4000 6000 0 1000 2000 3000 4000

CAAT CAA-AIMS 2
Fig. 5. Correlation of AIMS 2 texture, CAA, and CAAT with flow number results for the six mixtures evaluated in this study.

Aggregate characteristics determined from tests in the AIMS 2 Superpave CAA, followed by properties of coarse aggregates deter-
system, i.e., texture, coarse aggregate angularity-texture index, mined using AIMS 2, i.e., texture, CAAT, and CAA. Again, the prop-
coarse aggregate angularity, and sphericity, were the ones which erties related with aggregate angularity and texture were the ones
presented the highest R2 values, along with the Superpave F&E that presented the best correlations with the mixture stiffness.
5:1 test.
As also observed from the FN results, fine aggregate properties 4. Summary and conclusions
were not as strongly correlated with the resistance to fracture-
related damage as the coarse aggregate properties. Additionally, This paper evaluated the effects of morphological properties of
texture presented a high correlation with the IDT fracture energy aggregates on the mechanical behavior of asphalt mixtures. Three
in comparison to the other aggregate properties evaluated. This different aggregates, i.e., two crushed gneisses with different
highlights again the importance of texture as a critical aggregate shapes and one gravel, were used in the composition of six
characteristic to be considered in existing specifications. Superpave asphalt mixtures. Several aggregate properties were
Finally, a comparison between the aggregate properties and the characterized based on Superpave procedures for typical aggregate
dynamic modulus (|E⁄|) of the mixtures at 10 Hz was also made, as consensus properties. Additionally, morphological aggregate
shown in Table 7. R2 values were considerably high, as it was also characteristics were also determined in a modern image analysis
observed in the analysis of correlation between the particle prop- system, the AIMS 2. The morphological properties were evaluated
erties and the mixture FN. The best correlation was found with before and after Los Angeles abrasion tests to assess the ability of
the different aggregates to retain their characteristics after the
abrasion process. The mechanical behavior of the mixtures was
Table 7
also evaluated based on several test results of dynamic modulus,
Coefficients of Determination between Morphological Properties of Aggregates and
Dynamic Modulus of Asphalt Mixtures. flow number, and IDT fracture energy.

Correlations with Stiffness (|E⁄| @ 10 Hz) Based on the results, the following conclusions could be drawn:
Test (Standard) R2
Superpave – CAA [29] 0.78  Aggregate morphological characteristics were shown to be
AIMS 2 – texture 0.73 strongly correlated with the resistance to rutting of the asphalt
AIMS 2 – CAAT 0.72 mixtures evaluated. Weaker correlations were found with the
AIMS 2 – CAA 0.70
resistance to fracture of the mixtures. The observation implies
Uncompacted voids – CAA [19] 0.69
Superpave – FAA [30] 0.64
that the resistance to rutting of asphalt mixtures is dominated
AIMS 2 – FAA 0.59 by aggregate characteristics, whereas fatigue may be more
AIMS 2 – sphericity 0.44 related to binder properties. Test results also showed that the
F&E 2:1 [28] 0.38 mixture stiffness can be influenced by the aggregate morpho-
F&E 3:1 [28] 0.27
logical properties, especially at intermediate to low loading
Superpave – F&E 5:1 [28] 0.04
frequencies.
F.T.S. Aragão et al. / Construction and Building Materials 123 (2016) 444–453 453

 Among the properties evaluated, coarse aggregate characteris- [14] AASHTO M323, Standard Specification for Superpave Volumetric Mix Design,
American Association of State Highway and Transportation Officials, 2013.
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 Test-analysis results also indicated that the surface texture of [19] AASHTO T326, Uncompacted Void Content of Coarse Aggregate (As influenced
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Acknowledgements
Simple Performance Test for Superpave Mix Design. NCHRP Report 465,
National Cooperative Highway Program. Transportation Research Board,
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