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Laarge-Scale Produc
P ction of
o Highh-Perfformance
F
Fiber-MMetal-Lamiinates by Prrepreg-Presss-Techhnologgy
Christian Lauter,
L Corin Reuter, Shuaang Wu, Thoomas Troesteer
I. INTRO
ODUCTION
L
Abstract—Lightweight connstruction becaame more andd more IGHTWEIGH HT design iss an importannt contributioon to
mportant over thhe last decadess in several applications, e.g. in the
im
reduce CO2 eemissions andd fuel consumpption as well as to
auutomotive or aiircraft sector. This
T is the ressult of econommic and
ecological constrraints on the oone hand and increasing safeety and impprove safety aand performannce of vehiclees [1], [2]. U Using
coomfort requirem ments on the othher hand. In thhe field of lighttweight lighhtweight technnologies, the reealization of ccomponents w with a
deesign, different approaches aree used due to specific requirrements low
wer mass and with stable or o even betterr characteristics is
towwards the techhnical systems. The use of endless carbonn fiber posssible. In the aautomotive seector a decreaase of the vehhicles
reiinforced plasticcs (CFRP) offerrs the largest weight
w saving pootential masss of 100 kg leeads to a reducction of CO2 eemissions of about a
Open Science Index, Materials and Metallurgical Engineering Vol:10, No:5, 2016 waset.org/Publication/10004518
International Scholarly and Scientific Research & Innovation 10(5) 2016 964 ISNI:0000000091950263
World Academy of Science, Engineering and Technology
International Journal of Materials and Metallurgical Engineering
Vol:10, No:5, 2016
The prepreg ppress technoloogy can be divvided into fourr steps thicckness of t = 2 mm was useed. The prepreegs were stanndard
(F
Fig. 2). The innput for this pprocess is conntinuously prooduced semmi-finished prooducts from SG GL. The epoxxy resin from SGL
prrepregs, that aare shipped oon coils, and formed sheet metal (Tyype E201) embbeds carbon fibers in a ssymmetric 9 llayer
strructures. In the first sttep, the preppregs are sttacked scrim (90/02/90//0)S. The preepregs were manufacturedd by
coorresponding to t the expecteed loads in thhe final compponent. preppreg press techhnology. For tthe bonding w with epoxy resin as
Affter a compacction of the llayer structuree in a calendeer, the an aadhesive, the prepreg was ddirectly presseed on the mettallic
prrepreg stack iss cut to the ggeometry of thhe final compponent, surfface.
e.gg. by an ultrassound cutter. IIn the second step, a robot with a T
The manufactuuring process was divided into several steps. s
sppecial gripper system handdles the uncuured tacky prrepreg. Firsst, prepregs, sheet
s metal aand release fiilm were cut and
Toogether with a formed sheeet metal struccture, the preppreg is layeered. Second, the press process was realiized. For this step
inserted into a heated moldd in step threee. The laminnate is diffferent defined parameters w were used. Thhe test plates w were
prressed on the metallic surfface by a hyddraulic press device postt-cured in a fuurnace for 30 m minutes at a temperature off 180
wiith a pressure of about 0.1 tto 0.5 N/mm2. At a temperatture of °C, which simulaates the catapphoretic paintiing process. N Next,
1440 to 180 °C, tthe prepreg is pre-cured forr a time of 90 to 120 threee-point bendiing samples w were cut from the test platess and
seeconds dependding on the lam minate thickneess. Afterwardds, the testeed with a threee-point bendinng setup.
finnal hybrid strructure can bbe removed ffrom the molld and D
During the experimenttal investigaations, diffe ferent
staacked. The ffinal curing oof the epoxy resin occurss in a commbinations off temperaturee, pressure aand time for the
doownstream cattaphoretic painnting process that is simulaated by consolidation proocess were ussed. The aim was to identiify a
a ffurnace heatinng of 30 minuttes at 180 °C. suittable process window to m minimize the ccycle times off the
preppreg press proocess.
Inn Fig. 3, the results of three-point bbending testss for
diffferent process parameters arre illustrated. As A a consolidaation
presssure 0.3 MPaa was used. It can be seen tthat the values for
the maximum beending stress aachieve a platteau of aboutt 750
MPa for pre-curinng times abovve 60 secondss and temperattures
above 160 °C. Thhe values decreease at temperratures higher than
abouut 190 °C.
S
Summarizing, optimal process parameterrs for the preepreg
presss process werre found: the ttemperature foor low cycle ttimes
shouuld be about 180 °C, the ppressure shoulld be betweenn 0.3
andd 0.4 MPa andd the time shouuld be above 90 seconds. T These
valuues depend onn influence facctors such as thhe layer thicknness,
the materials or thhe textile semii-finished com mponent.
F
For the hybrid three-point beending samplees, a characterristic
failuure behavior could be fouund (Fig. 4). The sheet m metal
plasstically deformms under influuence of the teest force, whilee the
CFR RP componennt fails by delamination annd fiber breakkage.
For a force transm mission not frrom the metall side but from m the
Fig. 2 Process steps for the m
manufacturing off hybrid automootive sidee of the CFRP, the failuure is characcterized evenn by
sstructural parts, for example a bb-pillar, by preppreg press technnology delaamination andd fiber breakagge – in this ccase, as a resuult of
International Scholarly and Scientific Research & Innovation 10(5) 2016 965 ISNI:0000000091950263
World Academy of Science, Engineering and Technology
International Journal of Materials and Metallurgical Engineering
Vol:10, No:5, 2016
coompression forrces in the CFRP structure. adhesive was useed (Dow Betam mate 1620) [12]. The maxim mum
forcces for the ddifferent pre-curing tempeeratures are on o a
sim
milar level at abbout 7.5 kN. T
The use of a sstructural adheesive
leadds to slightly higher forcess of about 8.2 kN. The tensile
enerrgy absorptioon reveals thaat the failuree behavior off the
epoxy resin as ann adhesive is qquite brittle. T
This results inn low
valuues for the ennergy absorpttion of aroundd 2.5 J, whilee the
imppact resistant mmodified Dow w Betamate 1620 reaches 33.7 J.
Summmarizing thee bonding perfformance of the Dow Betam mate
is aabove the leveel of the epoxxy resin. Thiss is not surpriising
becaause the adheesive war optiimized for thiis applicationn. On
the other side it can
c be noted, that the use of o the epoxy rresin
offeers an optimizzed bonding solution for hybrid structtures,
wheen costs and mechanical
m prooperties are takken into accouunt.
Open Science Index, Materials and Metallurgical Engineering Vol:10, No:5, 2016 waset.org/Publication/10004518
8 4
4 2
Fiig. 4 Failure behhaviour of hybriid three-point bending sampless (force
transmmission from thhe side of the shheet metal)
2 1
The performaance of a mullti-material or hybrid structuures is
strrongly influennce by a permmanent and sollid bonding. F For the
coombination of sheet metaal blanks annd CFRP diffferent 0 0
International Scholarly and Scientific Research & Innovation 10(5) 2016 966 ISNI:0000000091950263
World Academy of Science, Engineering and Technology
International Journal of Materials and Metallurgical Engineering
Vol:10, No:5, 2016
International Scholarly and Scientific Research & Innovation 10(5) 2016 967 ISNI:0000000091950263
World Academy of Science, Engineering and Technology
International Journal of Materials and Metallurgical Engineering
Vol:10, No:5, 2016
900
800
700
Stress σ [ N/mm 2]
600
500
400
300
200
Fig. 12 Foour-point bendinng test of a FML
L specimen
100
1200 0,03
3
0
0 002
0,0 0,004 0,006 0,008 0,01 0,012 0,014 0,,016
Sttrain ε [mm/mm]
1000 0,02
25
1.4301-FML, t = 150
0 °C 1.4301-FML, t = 180 °C
800 2
0,02
Stress σ [ N/mm 2]
Strain ε [mm/mm]
Fig. 9 Stress-sstrain-curves froom tensile tests of different FM
MLs
600 0,015
1200 0,03
400 0,01
1000 0,025
200 05
0,00
800 0,02
Stress σ [ N/mm2]
Strain ε [mm/mm]
600 0,015 0 0
400 0,01
200 0,005
0 0
Tensile strength
h Fracture straiin
F 13 Results from
Fig. f four-pointt bending tests oof different FML
Ls
(caalculations of sttress and strain according to DIIN EN ISO 14125)
Strain ε [mm/mm]
600 0,015
400 0,01
200 0,005
0 0 (a) (b)
Figg. 14 Microsections of the midddle plies of the DC01-CFRP-F FML
maanufactured withh the following pre-curing paraameters: (a) 1500 °C,
300 s and (b)) 180 °C, 90 s
Tensile strenggth Fracture straain
International Scholarly and Scientific Research & Innovation 10(5) 2016 968 ISNI:0000000091950263
World Academy of Science, Engineering and Technology
International Journal of Materials and Metallurgical Engineering
Vol:10, No:5, 2016
off the area oof applicatioons of FML L. Currently, main of sheet metal and
a local CFRP rreinforcements,” Key Eng. Materr., vol.
appplications off FML can bbe found in straight or sllightly 504–506, pp. 2995–300, 2012.
[16] “DIN EN ISO 527-1: Kunststofffe. Bestimmung der Zugeigenschhaften.
cuurved componeents for the airrcraft industryy. Teil 1: Allgemeiine Grundsätze,” 1996.
The manufaccturing of FM MLs by prepreeg press technnology [17] “DIN EN ISO 527-4: Kunststofffe. Bestimmung der Zugeigenschhaften.
ennables the prodduction of commplex pillar structures, whiich are Teil 4: Prüfbeedingungen für isotrop und aniisotrop faserversstärkte
Kunststoffverbuundwerkstoffe,” 1997.
ussed in a widee range of industrial applications. Aside, this
[18] “DIN EN ISO 527-5: Kunststofffe. Bestimmung der Zugeigenschhaften.
tecchnology alloows a significaant reduction of cycle timess from Teil 5: Prüüfbedingungen für unidirektiional faserversstärkte
soometimes seveeral hours to unnder 5 minutes. Kunststoffverbuundwerkstoffe,” 1997.
The availablle paper shoows basic invvestigations oof the [19] “DIN EN 25662: Luft- und Raumfahrt. Koohlenstoffaserversstärkte
Kunststoffe. U Unidirektionale L Laminate. Biegeeprüfung parallel zur
m
manufacturing oof FMLs by this t technologgy. Therefore,, plane Faserrichtung,” 1997.
hyybrid test plattes were mannufactured witth different pprocess
paarameters. Froom these plates standard teest specimenss were
cuut out. The reesults from thhe conducted tensile, threee- and
foour-point bendding tests dem monstrated the potentials oof this
innnovative apprroach. The proocess enables a manufacturring of
materials withh a good and reprodducible mechhanical
m
peerformance annd a high qualiity within cyclle times of lesss than
5m minutes.
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