JOURNAL OF EXPERIMENT

Title of Experiment : Determination of the Distribution Coefficient

Day/Date of Experiment : Monday/ 3th April 2021
Name/ID : Andi Nurul Fauziah/1913442001
Class/group : ICP of Chemistry Education/IV
Members : 1. Nur Akifah Pardan
2. Siti Fathima
3. Izzatul Ummah
Assistant : Yuliana

A. OBJECTIVE OF EXPERIMENT
Determine the distribution coefficient of I2 in a water-chloroform system

B. APPARATUS AND CHEMICALS

1. Apparatus
a. Beaker glass 250 mL 2 pieces
b. Burette 50 ml 2 pieces
c. Clamp 2 pieces
d. Stative 3 pieces
e. Erlenmeyer 250 ml 4 pieces
f. Digital stopwatch 1 piece
g. Separatory funnel 250 mL 1 piece
h. Graduated cylinder 50 mL 1 piece
i. Graduated cylinder 10 mL 1 piece
j. Big funnel 1 piece
k. Small funnel 1 piece
l. Spray bottle 1 piece
m. Smooth cloth 1 piece
n. Rough cloth 1 piece
 2. Chemicals
a. Iodine solution in chloroform I2 in CHCl3
b. Sodium thiosulfate 0.02 M solution Na2S2O3
c. Aquadest H2O
d. Tissue
e. Label

C. WORK PROCEDURES

I2 in CHCl3
K I 0 .1 N

Put 135 mL of I2 135 mL I2 in Put 100 mL of H2O 100 mL H2O was

in CHCl3 into CHCl3 into into graduated added into
graduated separating funnel cylinder separating funnel
cylinder

2.5 mL of each layer The top layer is The bottom layer Shaken until 15
was inserted into the separated too is separated first minutes
erlenmeyer flask

Na2S2O3

Put Na2S2O3 Na2S2O3 was added The bottom layer The top layer is
into the beaker to the burette is titrated titrated too
glass
 The volume of
Na2S2O3 was
recorded

Makassar, 26th March 2021

Assistant Apprentice

Yuliana Andi Nurul Fauziah

ID. 1713142006 ID. 1913442001