P :ge tlo

5 Date

ESTIMATIoN OF Mn0a In KAOLUSITE

A To estimate pecentage MoO
Sample
Qiven Pyolusite usinq
appooximatel 1N Solukien oq oxali acand
a standard Solutien Potaium Pernayang
47
Solvtion

HpnanlusBusete, Prpette, Standard dask, conical Hask

Reauine fungel, Test bube, Beaket
Beagents Pobassiumpemangaabe, Oxalfc aci, Dil. H,S04
,Magnesum oxite
inleA weighk 4 ney powderd Sample
Known
9s heabe Known x ce Oxalis A
Solubien in esence 8lube Sulphuic actd
Oxali ocio uce Mn Sample
o mangonese Salb

Mn0a +HaGOy tHS04 MnSo tAC +RH0

Aelif'ed KMrO oxdizes eXcen_oxasic ad asAllas

2KHoOut 3H,S04 so4t2, s04t3440 t+50).

SHaCot S(o) lOco +5H0
Teaciers Signature
 DATE

EpNO. PAGE

acue ) Standardization KMOO4 Salukion

waette aitkh Suked KHeD4 Solution

ai 9ap e in
nsepg tiak tkere o

budette S ven given IN oxal~ ac

mode
ptpede ul a RSdmL Standhtd Hask,
ak witA Sisti lled wakeh ad
Shakn ell

L Estiaatien
About O-bgs 4oudersd Sarmfle is wehe
autakls and kaansferte 0 o a Conical plask
éxacetu ASnL iven N xalia acze
Solutien is MpeMe and
dl
dl Solyic ac meakaing Cuades are
added
Conlcelask.Mou e
cenical lask is coveud il a alas
emel. 1ts gentiy boiled enl
ack pankices emainsan become
clean bavwn Solutien s obkaied

Obseupkion
cweighe 9 Puobsite éxanser W-0:64Y qms-
Skandasdizatien KMaQ Sd
Sol Eakn n tA bwdelt e 0iN KHnOu Sel
S. lako n
lask Snl oOxalic actä Sol
Lndi cakon :KMnd4
CRange doz faem aloreas bo palefia
MLESTNE
 DATE J-
Exp. No. b PAGE

|Taial itial Reaa Hhd RaasHinqVal KHaou

No. mL) m

48
0 24-6 21 6
24-8 24.8

Agreng value V, g KMo A4:434 mL

C) Estimalion MnOa
Sol. takon in tdo burete 0LN4 k*o0a-
Ssl. in the Hask Snl expesinenkal sol
1dicaosUsed KMA
Er Point Lolouadess o ale piok

TaialTiol Aea final Realin Vol kMaOs_

No. (L) mL) ML

13S 13-S
13.S
13 13.2

Hggeeivalue Va 0 N KMnOu 13:4 mL

MILESTONE
 DATE / 1
Exp. No. S . PAGE

Calculakienss

aSoL d . Oxalie Aci =V,ml g 0LN kMnd24 734m

Exces Oxalc Acid Va ml _0.fN_KMa04 13.ml

Vol 0-LN' KMN eativdat to oxalia acid a t d

VV= (24:434-1s.4)
:33Mmt
Vol :1iN KMnO, eaphvalents axalic aci xenced
ba eaHre 0ve 10(V,-v2)
10(l33u)
I13-3mL

1o00ml
IoDaml N KMO4 43-am Hod Ew.E)

lo(v-Vml 0N KMaO41O x(V-v)x u3-z Ko

to00

13.34x 43-44X0-L

0.y924 qms Mo0a

Perxcenk Mo02
Peacek - 0 given Pulolusike 0:ugAxloo e%
0 644

Aesot Pexcentage Mnoa a qien samleI65066

MILESTONE