Page NO..

Expt. No.

Epeuiment-4

Ain O
allo a50 mL
apas oh MLo 31andand 2o1
02aliC acid1
b inq theSame eal, n d out h o m o l a f y
and stngh_c_given KMnO 3.o1
Matexiats tequuned
iqht boz, A1achopal weigha, qlas Dd
watth qlass, we
5 0ml beake ash bettlo 5Oml moakuin4 ilask,
butettepipetlu ttat ceoical 4lask, 4unðel

Chemicals equitad
nalicacd cHYStals, dil: S04 K MnO4 Sol"_

Ihe.oeLy
Tiatio 0Naie aid AD
a odc it1ation
KMAChEinq a 830naanidfefnq aqent oidisies
ZA aid uorm +3 10ty Atate Aidutes îtkeu
m t7 to+a Atato
Lmolas ma CLS1ailing pxaic acid o H,o=laG9
AJO06-
COOH
Molasity (M) =Avol(m 1)

OxIbo0. = wE 0..18q _0 S 0.8q

AO 26 5 0

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Expt. No.
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Pto co d w

D
PAapanation o oxaic acid
eiqh a cleandy oatch gla k ucidits
wigh accuwtatels 8 08q o01alic aid eiqhi.
Cystals O0tha waich qlas and
3 Lianste cateully th weiqhod ovalic socond H weighi1
into a acid ousta
beakes and d?gsoiuo it uinq dittiuud
LOateuin tho wasb bottle
uTHanfa ths enti Aol into a 5 0 m
Lask-atd mcasuinq
S Aud ensugb_distiued o a e
into tho measinq
uptoust b elow tho etchad 4lask
masAk GD b eck
Add the la
e duO{ diriiud watou with a
ppetic uhhl tho táuoey lavo) o
ruch tho
menitcu ut
maik_O0 tho eaNHing as

Fpau a a50ml a M/uo oaic acid Sa by

O.Sa C 0xali add eustals
diescluing
2 p cte_cut iCmC t Soi io titsta tion lask
3Add 10ml e cone H &Oin
iation
9) Heot tha rnixtuu to o-Go C to flask
fasten Aate Oh
5Add KMnou 30l n butett X note ntialaadin
6AddKMnîn o2alic acd kol l a Liqht pink
Colou appeaus ote tho inal adinq o4 butcta
|Ropeat th Atep ti you qetd Conco.Hdant

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Expt. No. Page No.

Ob&evatfon
weight wach gla 0.05
weiqht_o 0alit acid caystals = O.&
Veum e OXalica t i d %ol piop axd 5Oml
malauih a ozalie auid solE M
40

olume_ Dnaic add sol? taken

each ttHatiop s 1O ml

SNa initial soadinq- na oadinq yOLOL KMn0-

b ette (v O buotto(V,) ako V-V)

21 10. 20.2 JO.y

3) 0 6 3 1O.4

Paecautions i
ay 9ap om butate&
9Ramous the unnel beja notinq tho aadinga
3No duop o lquid should haiq aL tho tip e bulete
Neve buuutte o pirctteoith bloken noglo
5Neveu oiget to hoat ho minute to 50'c -60°
beLo tinatioD

Result 6-0062
nolaHihy ogiven kMnOy 3ol_

T523tt
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tart
 Cheoi.acactation

Ructien KMO 13 SO
> K, So, 1MOSO +3H,0+5C)
Go'C
Czidatien H CO t fo 2 CO2 1 , 0 x5

SOt2MoSSo,

KMnC, , SO+51, C,02

+loCO,2 +8 ,O

eq u a i o n

MrO + 8H 4 5 M 2t
+ HH0 x2
2C0 t/2e

16H 2 MOn t loCo 8H

 Calclation
Ex
a) Molaty KMoO Sol
Sol

moles KMOu uacts

Fio m balanu d
fiom eq,
wilh 5 moles Onalic acid

M,V M2V2 =) M, V)
M, V
M, molastrty aiven KMOO Sul
VVoumo iun MnO Sot 10. m
molQs o kMo0u in balan ad eq a

M
M molo1ity oOnalic oci d sot Yao M
Vo uume oh oMalic aid s 1 10 m
rmolus o 0malic acid ibalanod e 5

M,x 0. =) M,
2 O.00962M
xIo

b Stonqt o KMnOu Sol

Stongth molaity X molast us

mola ma o KM00u
193
0tongth M,x 15 8
0.00462 X158

1.6 2.q/L