Professional Documents
Culture Documents
1. Fekadu Mazengia……………………………….0701693
2. Tadilo Belete ……………………………….0702316
June 2018
Declaration
We would like to declare that we have successfully completed a four month internship
program at Gondar Pepsi-Cola factory. We have stayed from February 05/2018 to June 2018.
This paper includes all requirements of an internship program. We want to assured that this
report exactly belongs to us. We have done a project during the internship program and is
included as part of this report. We were fully engaged to write this report and also to perform
our project. Except we have taken from reference materials all the descriptions,
recommendations are our own. Finally, we are intended to tell you this document is a good
indicator of how much effort we made to go steps forward in the practical world by
integrating it with the theoretical knowledge.
I
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
Acknowledgment
First of all thanks to God for keeping all things to be happened in good manner. We would
like thanks to Bahir Dar University for giving this chance to get practical skills & Gondar
Pepsi Cola plant for accepting us to get costless knowledge. There are many people around
that have supported us all the way through and to make things easier. We tank our advisor
Mr.Bassazin Ayalew for visiting and advising us in doing of our project and report. We
thanks for managers and employees of Gondar Pepsi cola company specially the company
supervisor Mr. Nuredin who is supervisor of production for his incredible level of advice,
many suggestions and constant support at every step of this report. This report could not
finalize without his regular valuable suggestion and encouragement. And, we have a great
honor for other employees for their genuine intention to teach us under great motivation.
II
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
Executive summary
MOHA soft drink industry S.C is one of the leading competitive companies in Ethiopia
which is found in most Ethiopian region. It has many branches. Among them Gondar Pepsi
Cola plant the one, which is found in Amhara region. Currently Gondar Pepsi cola plant
manufactures Pepsi and Mirinda only. It uses oldest technology, different machines,
materials, human skills and methods to manufacture its products qualitatively and
quantitatively. This report consists of the brief history and profile of our hosting company
including the main raw material used to produce its main products and also the main
customers that use its main products and supplier, consequently its organizational structure
and detail work flow of beverages production activities in each section and the overall
systems of the organization. The report also describes the current practice and activities that
take place in the production Department and other main supportive departments. Project work
on wastewater characterization is done and the document is included in this report. The main
benefits of internship are also included on this report.
The wastewater effluent has different concentration for various samples. During production
period the wastewater has temperature of 280c, PH of 10.93, TDS of 1100 ppm, turbidity of
45.05 NTU and TSS of 60mg/l this is mostly generated from bottle washer. During sanitation
wastewater effluent has average temperature of 330c, PH of 10.87 and TDS of 900, turbidity
of 54.65 NTU and TSS of 75 mg/l.
This document consists of the characterization of wastewater effluent in Gondar Pepsi Cola
Company. The nature of wastewater effluent in GPCP includes physical (temperature, color,
odor, turbidity), chemical (PH, TSS, TDS, COD and BOD), and biological characteristics
which depend on the wastewater discharge section. All those parameters are measured to
characterize the effluent wastewater in GPCP. Caustic soda consumption for washing process
has highest contribution to this wastewater characteristic. These values are compared with
standard and except PH other effluent parameters are acceptable. We recommended for the
company to apply a simple treatment process before discharging the wastewater.
III
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
Table of Contents
Declaration................................................................................................................................................................I
Acknowledgment.....................................................................................................................................................II
Executive summary.................................................................................................................................................III
Table of Contents....................................................................................................................................................IV
List of figures...........................................................................................................................................................VI
List of tables...........................................................................................................................................................VII
List of acronyms....................................................................................................................................................VIII
CHAPTER ONE...........................................................................................................................................................1
1. INFORMATION ON GONDAR PEPSI COLA PLANT.................................................................................................1
1.1 Background of the Hosting Company................................................................................................................1
1.2 Objective of the Company..............................................................................................................................2
1.3 Mission and Vision of the Company...............................................................................................................2
1.3.1 Vision of the Company............................................................................................................................2
1.3.2 Mission of Company................................................................................................................................2
1.3.3 Future Program of the Company............................................................................................................3
1.4 Main Products of Gondar Pepsi-Cola Company.............................................................................................3
1.4.1 The Main Customers/End Users of Its Products.....................................................................................3
1.7 Organization structure...................................................................................................................................4
1.7.1 Responsibilities of the department.........................................................................................................5
CHAPTER TWO..........................................................................................................................................................8
2. PRODUCTION PROCESS OF GONDAR PEPSI COLA PLANT....................................................................................8
2.1 Main Raw Materials and Their Properties.....................................................................................................8
2.2 General Process Flow Sheet of Gondar Pepsi-Cola........................................................................................8
2.3 Main Rooms of Gondar Pepsi Cola Plant.....................................................................................................10
2.3.1 Water Treatment Section......................................................................................................................10
2.3.2 Boiler Room...........................................................................................................................................15
2.3.3 Air Compressor Room...........................................................................................................................17
2.3.4 Syrup Room...........................................................................................................................................18
2.3.5 Bottle Washer........................................................................................................................................21
2.2.6 Filling room............................................................................................................................................23
2.3.7 CIP Method............................................................................................................................................27
2.3.8 Quality Control Section.........................................................................................................................27
CHAPTER THREE.....................................................................................................................................................32
PROJECT WORK......................................................................................................................................................32
3. 1 Introduction.................................................................................................................................................32
IV
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
V
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
List of figures
Figure 1 organization structure of the company.......................................................................................................4
Figure 2 general production flow sheet of Gondar Pepsi cola plant........................................................................9
Figure 3 sand filter tank.........................................................................................................................................12
Figure 4 Cartridge Filter.........................................................................................................................................13
Figure 5 polishers...................................................................................................................................................14
Figure 6 block diagram in water treatment room...................................................................................................15
Figure 7 fire tube boiler..........................................................................................................................................16
Figure 8 Air compressor.........................................................................................................................................18
Figure 9 finished syrup reservoir...........................................................................................................................19
Figure 10 solid ingredient of Mirinda....................................................................................................................20
Figure 11 bottle washer..........................................................................................................................................22
Figure 12 water and syrup reservoir for mixing.....................................................................................................24
Figure 13 carbon cooler.........................................................................................................................................24
Figure 14 date coder...............................................................................................................................................26
Figure 15 Drainage System of Gondar Pepsi Cola Plant Wastewater Effluent.....................................................44
VI
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
List of tables
Table 1 standard for finished syrup........................................................................................................................21
Table 2 faults on filler and possible causes............................................................................................................25
Table 3 CIP steps for production change...............................................................................................................27
Table 4 Food safety and quality department..........................................................................................................29
Table 5 Summary of Typical Characteristics of Untreated Wastewater................................................................35
Table 6 Wastewater discharges to land or water regulation..................................................................................35
Table 7 values of wastewater characterizations parameters.................................................................................39
Table 8 measurements conducted for TSS determination......................................................................................41
Table 9 comparison of measurements with the standard.......................................................................................43
VII
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
List of acronyms
AC Activated Carbon
DS Dissolved Solids
DE Diatomaceous Earth
IT Information Technology
LAB Laboratory
Mgr Manager
MOS Micro-Organisms
P reading Phenolphthalein
VIII
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
Sup Supervisor
TS Total solids
TN Total Nitrogen
UV Ultra Violet
IX
BIT, FCFE
Internship report and project on MOHA soft drinks/Gondar 2010 E.C
CHAPTER ONE
1. INFORMATION ON GONDAR PEPSI COLA PLANT
1.1 Background of the Hosting Company
Pepsi cola traces its origins to 1898 by Caleb Brad ham, a pharmacist in New Bern, North
caroling, created a curative drink for dyspepsia called Pepsi cola – Pepsi cola later referred to
simply as Pepsi was a mixture of carbonated water, cane sugar syrup and an extract from
tropical Kola nuts. To sell this product, Brad ham formed the Pepsi cola company in 1903.in
addition to selling the drink at drug store counters brad ham bottled Pepsi for sale on store
shelved. At this time bottling was a new innovation in food packaging.
Nefas Silk Pepsi Cola is the first Pepsi Cola plant in Ethiopia and was established in 1966 as
a share company with an initial capital of 1 million Birr. The capacity of the bottling line at
that time was 20,000 bottles per hour (BPH). In 1986, the plant was renovated and expanded
to a capacity of 50,000 bph with twin fillers. Total renovation and expansion investment cost
was Birr 6,647,944.00.
Dessie Plant, Dessie soda industry was established in 1952 by and individual owner In1979.
The plant discontinued other soda products and started producing Pepsi Cola, Miranda brand
and carbonated Tosa Water.
Gondar Plant was established in 1961 as ‘Saba Tej’ Share Company, but nationalized in 1975
replacing the old line as stated predicating Pepsi cola, Miranda and Team brands in January
1978. Gondar Pepsi Cola Plant, before nationalization was owned by private individual
produced wilk-fite water. The Ethiopian beverage corporation made a new feasibility study
on Pepsi cola product which got the blessing of the government to erect the currently
operating plant in 1986.
The current Gondar Pepsi-Cola Plant was established in 1986 by the Government owned
Ethiopian Beverages Corporation under license from Pepsi Cola Company. The capacity of
the bottling line at that time was 5000 per hour (bph). The sales area of the plant is north and
south Gondar and west and central Tigray. GPCP’s activity is being managed by General
Manager and under him there four department managers and one supervisor. In all these
departments there are 10 supervisors, who are management team members. The plant
executes its production and sales activities with a total number of 230 permanent and 61
contract employees. The plant is striving for the development and implementation of food
safety management system based on HACCP, to improve its overall food safety performance
and achieve certification to the standard. To achieve this goal, the HACCP study team.
Which consist of seven members from different departments with different disciplines and
skills, has developed this HACCP plan for best food safety achievements.
Warehouse sup
Vehicles maintenance
sup
Fleet sup
Branch manager
CHAPTER TWO
2. PRODUCTION PROCESS OF GONDAR PEPSI COLA PLANT
2.1 MAIN RAW MATERIALS AND THEIR PROPERTIES
Water: - as the main component of a soft drink, usually accounts for between 85−95%
of the product and acts as a carrier for the other ingredients. This water used should be
treated water.
Sweeter - are a critical ingredient of Pepsi cola products and there use must be properly
controlled which greatly affect the sensory experience.
Concentrate - receipt and handling must be properly managed ensure good quality
beverage.
Carbon dioxide - imparts a pungent slightly acidic taste to the finished product as well
as creating greater eye appeal.CO2 to extent used as preservatives.
Food grade raw materials- These raw materials have direct contact with the product
and they are not toxic for the product. From these: - Sugar, Water, Carbon dioxide,
Flavorant, Common salt, Acidulates and Colorant
Non –Food raw materials- Those raw materials are not direct contact with the product
and they are toxic for the product mostly they are used for water treatment and bottle
washing purpose .From these:-Activated carbon, Coagulants like Aluminum sulfate
Caustic soda Lime, Lubricant ,Chlorine, Calcium hypo chlorate and Crown cork
10. Generator
11. Workshop
Sugar
Water treatment
Simple syrup
Boiler room (steam)
preparation
Concentrate
Finished syrup
preparation
Bottle washing
Co2
reser
Bottle Inspection
voir
and date coding
Storage
Lime: - lime is used for alkalinity reduction. It is also used to increase the pH of the
water. The total alkalinity of the treated water should be below 50 ppm. Lime reduces
alkalinity by converting carbon dioxide to bicarbonate alkalinity, and bicarbonate
alkalinity to the insoluble forms calcium carbonate and magnesium hydroxide, which
precipitate out of the water.
Calcium chloride: - reacts with the lime to reduce the water alkalinity. Sodium
alkalinity is present when the total alkalinity is greater than the hardness of the water.
Calcium chloride which forms calcium carbonate from the sodium bicarbonate as the
calcium bicarbonate is formed. In some cases, water contains sodium alkalinity. If
sodium alkalinity is present, it will be necessary to add small amounts of calcium
chloride to get the treated water total alkalinity below the maximum limit of 50 ppm.
i. Coagulation Tank
Coagulation (Reaction) tank is the first tank in the water treatment room. The desired
chemical reaction takes place and water is sanitized. Coagulation is a chemically water
treatment process by changes smaller particles in to heavier that is they can quickly settle out.
The aluminum sulfate, lime and chlorine join the raw water as it flows in to the mixing zone
of the tank. The coagulant, usually Aluminum sulfate with the assistance of the chlorine and
lime, forms heavy flock which entraps particles of debris, dirty organic matter and other
undesirable material in the water, and settles slowly toward the bottom of the tank. The flock
forming the lime is causing the alkalinity components (calcium carbonate and magnesium
hydroxide) to precipitate out of the water. The precipitated alkalinity also settles slowly
toward the bottom of the tank. The treated water flows upward toward the treated water draw
off pipe, the flock because of its own weight, is left behind continuously trapping particles of
debris as it settles. The treated water flows toward the treated water draw off pipe and out of
the tank (toward the sand filter and reminder of the system, while still reserving the benefits
of chlorine. The chlorine in the coagulation tank, in addition to oxidizing organics and in
organics and reacting with ferrous sulfate, is destroying microorganisms so that sanitary
water is assured. The treated water then flows through a sand filter for straining (and removal
of flock particles), a carbon filter to remove chlorine,(and color, odors, tastes and
organics)and final polishing. Terminal ultraviolet disinfection follows the polisher.
The purpose of sand filter tank is to remove only physical matters and unwanted materials
from the raw water like floating materials present in the ground water. The sand removal
filter tank consists of three layers. At the bottom of the tank there are sands which also called
gravels and they are relatively larger in size. On the medium part of the tank there are also
sands which are lesser in size than gravels and also they cover a few heights above the gravel.
Finally the upper part of the tank is filled with fine sand filters followed by anthracite at top
up that enhances filtration of foreign matter or suspended particles coming with raw water
which may occur during storage at concrete tank. Then the raw water passed through the sand
filter will be stored in three different raw water storage tanks each sized 80m3.
The treated water that comes from coagulation tank enters in to the sand filter. In this tank
there is small sand that is used to settle the lime. This used to remove the unwanted chemicals
except chlorine from water. In the sand filter we can checked the lime dosage in the treated
water, by using the formula: A= 2P-M
Where: A -is which tells us whether the lime treatment is correct or not
P-is phenolphthalein indicator
M -is will tell us if all bicarbonate was removed whether we have free lime present.
• When A is positive, that is 2P is >M this implies that free lime is present in the
treated water.
• When A is negative, that is M is> P this implies that bicarbonate is present in the
treated water.
For proper lime treatment A value should be in between 2 and 7.
iii. Carbon filter tank
The treated water that comes from the intermediate tank is entered in to the carbon purifier.
This is used to remove chlorine by using activated carbon that present in the water. The
presence of chlorine can be changed the color and test of the final product (Pepsi, Miranda,
7up Miranda apple, Miranda orange and Miranda tonic). The chlorine dosage in the carbon
purifier must be in between 6and8.
If the color can be c hanged the water has chlorine, therefore the treated water can be
corrected by removed chlorine before enter in to the polisher. Because if the water that has
chorine is passed in to the process can be changed the color and test of the product.
Regeneration of activated carbon is takes place by the incoming steam from boiler room.
iv. Cartridge Filter (Polisher, 1micro Sized)
This is used to remove suspended activated carbon that comes from the carbon purifier and
other unwanted particle that may be passed through the carbon purifier before transferred to
UV. The filter bag used for filtration is called polisher
The white colored polisher is the new/to be used by replacing the old one that used for one
month period inside the Cartridge filter. Cartridge filter contains five polishers inside it as in
the above arrangement for one month.
Figure 5 polishers
Water storage tanks → Water treatment by Coagulation tank → Sand filtration → Carbon
(Activated) purifier → Polishing → UV → Treated water (fot syrup preparation, filling…..)
These reactions are continuous until the active site of sodium in zeolite complex compound is
all occupied by Mg and Ca. The structure contains a relatively large central open area which
allows large ions or other molecules to move through or reside within its frame. As a result,
sodium zeolite can function as a chemical sieve. During the reactions since alkali metals are
more active than alkaline earth metals; Mg and Ca are displaced from their carbonate
compound by Na to form Na2CO3. Na2CO3 does not have an effect on the hardness of water.
In the second softener: In this softener sodium zeolite is regenerated by adding brine solution
Softened water obtained from the softener is transferred in to different rooms; such as boiler
room, washer room and cooling room, chiller.
Lime
CaCl2
Al2 (So4)3
Coagulation tank
Raw water
Sand Filter
Treated
Cartridge filter
water UV
Carbon purifier
(Light oil) is that it is cheaper than fuel. A boiler or steam generator is a device which is used
to create steam by applying heat energy to water. This generated steam has different
functions in different sectors of the company.
Such as;
o for heating caustic soda in washing room
o To dissolve sugar in syrup room.
o Sanitation
There are three types of boilers namely, fire tube, water tube and electrical tube boiler. The
plant uses fire tube boiler to produce steam. Fire tube boiler flame is move inside the tube and
water is on the outside of the tube meaning on the shell side, while water tube boiler water
moves inside the tube and flame on the outside of tube.
A boiler machine requires different raw materials to produce steam. These raw materials
possess combustion process. During combustion the heat energy is produced. This heat
energy is applying to the water inside the boiler tanker, then the water heated more and more
it changes to steam which is required product.
The boiler machine requires sensor solenoids which controls the amount of water present
inside its tanker. This simply indicates that when the amount of water present in its tanker is
less, it opens the water valve from the reservoir water tanker, and when it is excess amount of
water, it closes the reservoir water tanker. These two values are sensitive materials.
through the heat exchanger in order to loss its hotness temperature and gating to the syrup
room. After all this process the simple syrup will be produced.
There are two types of syrup preparation in the production of soft drink plant, those are: -
o Simple syrup: - Is the mixture of water and granulated sugar
o Finished (final) syrup: - In this unit there are huge tankers and they used to store and
Convert the simple syrup in to the final syrup, but before these it should be cheek the brix
and the amount of simple syrup. The next step is adding of flavor and other ingredients in
to the tanker, but those ingredients are different for different soft drinks. Then agitate
until the components are mix and it’s have a manual or standard for this work, so the
chemists cheek the quantity and quality in every 4 hours, after all this final syrup will be
produced.
agitate until mixed.[from the workers] After this entire step stop agitation of syrup and test
the brix, total volume and specification of finished syrup. Then hold the syrup for 24 hrs.
iii. Preparation / processing instruction for Miranda
Syrup preparation for marinade orange and the Ingredients for Merida orange: -
o Citric acid it’s organic acid that prepare acidic media and preventing from mold and
bacterial contamination
o Sunset yellow: it’s a chemical that bring the desired color for the final product
o Sodium chloride: it contribute for the better test of the product and also for long shelf
life
o Potassium sulfate: it’s a chemical that makes our product soft drink & makes it sharp
o Benzoate: it’s a preservative that use to prepare our product
o Liquid Flavor: that brings the desired orange flavor to our product.
Dissolve 0.940 kg of sodium benzoate in 4 L treated water, then add to the tank and agitate
until completely mixed. Then add 11.70kgs of citric acid anhydrous, 1.360kg sodium
chloride, 0.680kgs of potassium sulphate, and 0.345kgs of sunset yellow (color) and mix
them with the agitator and then add orange flavor (30.05kgs). This is for 2 unit finished syrup
preparation which is 1280L in volume. Finally, the brix of the syrup test by chemists and if it
fits to the standard; it will go to production line.
This machine uses different chemicals for washing bottles. These are:-
o Steam: which comes from the boiler room
o Caustic soda: for washing bottle after dissolving in a dissolving area with water at 75
up to 82 degree centigrade.
o Water: comes from water treatment room.
NB: - DIVO LE & DIVO NP are both added on the cold water.
These chemicals are the bottle washing elements that washes in their own steps. The washing
machine washes the bottles and gives to the drier machine which dries the bottles and transfer
to the conveyor. After this the conveyor feeds the bottles to the filler machine continuously.
The following steps show the procedure of the washing machine when it washes the bottles.
Returned Bottle (sales)→empty bottles stores/sales→ De palletizing→ Declassing→
Sorting→ Neck inspection→ Pre rinse clean→ Caustic soak→ Caustic spray jet→ Warm
Water spray→ Final rinse (Cold water) →Fresh water spray jet→ Clean bottles discharge
→Inspection
This machine is very important and usable to be effective for bottle washing and it’s suitable
to wash that bottle with a little (minimum) amount of time and labor. The bottle is waiting for
30 minute in the washer machine until in late up to final out, and it pass different stages.
Pre-rinse: -This is the first stage for bottle washing and the bottle is wash internally and
externally with soft water by using spray jet.
Caustic 1: -After pre rinse the bottle is going to caustic 1, this is a kind of bath and in this
bath there is 7000 L of caustic soda solution, also the caustic strength is must be 2 – 2.5 in
scale and the chemists is cheek this scale in every 4 hour, and the amount of caustic is 100 kg
In this section the temperature of caustic soda is must be 65 0C. Caustic 1 is used for removing
of the bacteria and microorganisms inside and outside of the bottle.
Caustic 2: -The difference between caustic one and caustic two: -the strength of caustic in
caustic 2 is less than caustic 1(or it measure 1 - 1.5 in caustic 2) and also the temperature is
decrease by sum amount like 25 -280C from caustic 1.
Warm water: -The temperature of this warm water is 45 -48 0C and the bottle is washed
internally and externally by using spray jet hole, those spray jets have 15 holes. Cold water:
-Also wash the bottle with cold water.
Final rinse: -This is the final stage for bottle washing process and the water is comes from
water treatment room, so the water is clearly treated in order to protect the bottle from
microorganism and other un-desire things.
2.2.6 Filling room
Process takes place in the filling room:
Empty bottle inspection
Mixing
Filling
Crowning
Full bottle inspection and
Date coding
i. Empty Bottle Inspection
In this process the washed bottles are inspected manually by peoples and electrically through
light screening in order to check any untreated bottle. The inspection includes properly
unwashed bottles, rust and bottles that cannot be used for specific kind of product. The
purpose of inspection is to insure the safety of the work in the processes. People inspect
manually 150 bottles per minute and 18,000 bottles per hour
After the syrup and water are mixed regarding to their ratio, CO 2 will be added on the
mixture. There is no material to receive carbon dioxide, it just comes online and mix with the
water and the syrup and will get into the carbonation tank. There is also a standard for carbon
dioxide added. Carbonation tank is used to dissolve the CO 2 thoroughly in the mixture. When
the CO2 completely mixed with the mixture then it is called a final product and will be ready
for filling. Before CO2 combined with treated water and syrup it should be cool by carbon
cooler in order to dissolve CO2 .because CO2 is a gas, it dissolves at low temperature and high
pressure .the objective of cooling CO2 is to preventing foaming during filing and also prevent
under filing. As the beverage is chilled, it absorbs carbonation. Most beverage operation use
cooling to 20oc for cold filling. The finished beverage is cooled by ammonia gas; the cooling
tower for ammonia compressor is available in the company.
viii. Filling
Filler is a machine which is used to fill the bottle with the drink that has been prepared in the
Para mix. It is connected with the Para mix and the crowner cork. This machine has bowl
pressure, bowl level, bowl liter, capacity, mode filler, bottle counter and temperature and
controlled by PLC system. These all things have their own purpose. The various filling
processes are selected at the operator panel. First the drink is stored in the bowl and above
this drink car bon dioxide gas will be placed and then when the empty bottle is transported by
the in feed conveyer through the in feed worm gear which pushes the bottles in sequenced
manner. Then the bottles are pressed against the filling valve by a lifting element called
piston. The piston will perceive the existence of the bottles during the lifting process. If the
bottle is present the processes is started and the bottle is filled. The corresponding filling
valve remains closed if the bottle is missing. The machine works by lubrication system
automatically .there are also 15 filling valves called vents and expanding tubes where these
tubes have small holes that are used to transport the gas as well as the drinks respectively. In
this section the co2 should be filled first in the bottles in order to balance the temperature and
pressure as well. When the fluid (drink) poured in to the bottle the gas occupying the
remaining space of the bottle goes up to the returned gas media through the vent tube.
ix. Crowner
It is a device used to seal the bottle with crown corks. It has cork feeder on top part, the cork
drop by the action of gravity to seal the incoming full bottle.
xii. Packing
The purpose of packing is to arrange the full & empty bottles in a proper order for the safety
of the bottles. In Gondar Pepsi cola plant packaging is done manually. The full bottle in the case is
will put by human
In this laboratory section different devices are used for different purposes. Such as;
Refractor meter
It is device in the laboratory section for the purpose of determination of brix after
decarbonate the beverage and also determine the brix from simple syrup and final syrup from
beverage decarbonate first because the brix we cannot determine before decarbonate because
carbon dioxide not visible the brix amount.
Decarbonator
It is a device for the laboratory section for the purpose of removing of carbon dioxide from
beverage to know the amount of brix on the device of refractor meter.
Conductivity meter
Is a device used to check the total dissolved solid in the water in the natural water is the
normalized measure of the water ability to conduct electric current? This is mostly influenced
by dissolved salts such as sodium chloride and potassium chloride the common unit for
electrical conduct is Siemens per meter most freshwater sources will range between 0.001
and 0.1 Semen per meter. The source of electrical conductivity may be an abundance of
dissolved salts due to poor irrigation management minerals from rain water runoff or other
discharges.
Turbidity meter:
It is a measure of the cloudiness of water. Cloudiness is caused by suspended (mainly soil
particle) and planktons (microscopic plants and animal) that are suspended in the water
column is the material in water that affects the transparency or light scattering of the water.
PH meter:
It is used to know basic, acidic or neutral the solution of in the laboratory section.
Chlorine tester:
It is a device used to determine the amount of chlorine in the production water and washing
water.
The objectives of laboratory testing are:-
• To check the quality and the acceptability of the final products or line products. Un-
packed area Bottle washer selecting of damaged Bottle Visual inspected Filling area
Capper /closure area labeling area Package area Full bottle area to the consumer
• To check the quality and acceptability of water, the chlorine content, hardness,
softener of the water from water treatment room and from concrete tanker and the
caustic amount in the bottle washer of the water.
• To check the quality of the simple and finished syrup from syrup room to producing
good quality product
• To check the water, the syrup and the class rooms must be free from any MOS. In the
laboratory, there are many activities are done according to the standard manual
PH: Most of the time raw waters PH lie between 6.5 and 8.5. But it is required to be 7 which
is neutral and this can be done by treating the water.
Conductivity: Is the primary measurement of mineral contamination in water. This
contamination will be checked in laboratory and depending on the result a correction will be
taken according to its range.
Turbidity: Is the coldness or haziness of the water and it is caused by the presence of non-
sucrose substances, such as poly saccharides, high molecular weight poly phenols and
suspended minerals (ash) that are generally invisible to the naked eye, similar to smoke in air.
This parameter quality also be checked and it must be a very low number for application. It is
measure by turbid meter.
Total Hardness: Hard water is water that has high mineral content (in contrast with soft
water).Hard water is formed when water percolates through deposits of calcium and
magnesium containing minerals such as lime stone, chalk and dolomite. Treating hard water
is used to keep the safety of machines such as boiler and bottle washer.
Alkalinity: Is a measure of the capacity of water to neutralize acid. It is parameter to be
checked and will take an action if the result exceeds the range.
Softener type of water is used for bottle washer, boiler and chiller purposes. As raw water,
softener water also will be checked it hardness, duty and conductivity.
Total Hardness: As it is stated earlier hardness is the amount of minerals such as calcium
and magnesium present in water .This also treated it change the hard water in to soft as much
as possible after knowing it result from LAB.
Duty: Is the number of the tank which holds water at processing time during sample taking
Conductivity: Like to the raw water, the mechanism is also similar to softener water. There
only difference is that the value will be lesser than that was in the raw water. It is because of
filtration. Most of the parameters that where checked under raw and softener water also will
be checked under treated water. The only and different parameter is that UV ray, because it is
the final step before going to in to production.
A sample will be taken from simple syrup to check it brix, color, turbidity and percent of
ash.
Brix: It is a sugar content of simple syrup. This amount varies depending on the product like
if its Pepsi the brix standard will be 54.00 for Miranda=62.70,for apple=57.60,for tonic= 55.4
and for 7-up=57.10.
Color: It is also the other parameter to judge the quality of simple syrup. The color tells as
weather the simple syrup is filtered properly or not. If the color of the simple syrup became
like water color, then we can say that it’s clean, unless otherwise it not. The apparatus used to
check color is called spectrometer.
Percent of Ash: This parameter tells as the quality of the sugar. Percent of ash rises, then the
sugars quality can be said t is low and vice versal. Under final syrup brix also will be
checked and Titrable acid is the other parameter to be checked.
Brix: The value of final syrup is different from it simple syrup, because dray component and
flavors are added to it. And there range is differ across the type of the product. For example
Pepsi=53.5 to54.00, Miranda=59.10, apple=52.10, tonic=48, 7-up=54.40.
Titrable Acid: Is a very use full and essential parameter which tell whether the sample has
acidic property or not, or if it has another unwanted substance, or if the dray component
didn’t added correctly or if the ageing Time was not correct and so all. This result will tell as
the answer for those questions. The substance used for titration is called sodium hydroxide.
Finished Product: - Whenever a finished product brought to laboratory, the first step is to
view whether there is a foreign material present in it by using bottle inspection glass. Then it
cork size and fill height will be measured by using cork measurement and fill height gage
respectively. After measuring temperature and pressure of the product in order to read carbon
dioxide, bicarbonate, remove carbon dioxide for measuring brix. If we measure the brix with
co2 present in it, it went give as the correct result because the system works oscillating, but
when co2 is present in it, it will start trapping. This all checkup it continuously performs in
every 20 min.
Hot Water from Bottle Washer: -
After washing the bottle with caustic, we wash them with hot water to remove the caustic.
But the hot water alkalinity is checked by titrating it with H2SO4 of 0.02N.
CHAPTER THREE
PROJECT WORK
3. CHARACTERIZATION OF WASTEWATER EFFLUENT IN GPCP
3. 1 INTRODUCTION
Now a day the main concern of this world is environmental pollutions. So many wastes
released from the industries can affect the global status of nature. Specifically the waste water
emitted from the factories causes a serious of problems in large portion of water (seas, leak
and rivers) and on human’s well beings. The water that released from the industries may be
solid, liquid and gas; all of the three wastes have no effect on the same way that other do but,
all of them potentially and ultimately polluting the water in different ways.
Soft drink industry forms a large part of the food and beverage industry. Thus it is important
to study the nature and amount of wastewater generated from the soft drink plants. Water is
an essential raw material in the soft drink production with a consumption of 2.5 to 3.5 litter of
water per liter of soft drink. The wastewater generated in this industry is mainly from bottle
washing, filler backwashing, washing of bottle machine, equipment’s, floors and pipe work
during flavor changing. The major contaminants in this effluent are caustic soda and sucrose.
Wastewater from bottle washing is almost 50% of the total waste water generated, which is
about 1.25 litter of wastewater per 1 litter of soft drink, bottle washing is performed by
washing machines that operate in different cycles.
Much of GPCP wastewater is generated from bottle washer continuously during production
of Pepsi and Mirinda. There is a generation of wastewater from syrup room during simple
syrup & filter washing. Washing process takes 10-15 minutes. Wastewater is also generated
from water treatment room during backwashing of sand filter & carbon purifier. 3 step & 5
step sanitation generates much of wastewater within 1 hour to 2 hour time interval
Odor: fresh wastewater may have a soapy or oily odor, which is somewhat disagreeable.
Stale wastewater has putrid odors due to hydrogen sulphide, and other products of
decomposition.
Turbidity: turbidity in wastewater is caused by a wide variety of suspended solids- in
general, stronger wastewater has higher turbidity.
The chemical quality of wastewater is expressed in terms of organic and inorganic
constituents-domestic wastewater generally contains 50 percent organic and 50 percent
inorganic matter. A general discussion on organic components, total suspended solids, and
inorganic slat of wastewater is given below.
Total solids (TS): organic and inorganic, settle able, suspended and dissolved matter.
Total suspended solid (TSS): portion of organic and inorganic solid that are not
dissolved. These solids are removed by coagulation or filtration.
Total Dissolved solid (TDS): portion organic and smaller than one mill micron (m μ) fall
in this category.
BOD5: Biochemical oxygen demand (5-d, 20˚C) it represents the biodegradable portion
of organic component. It is a measure of dissolved oxygen required by microorganisms
to stabilize the organic matter in 5 day.
COD: chemical oxygen demand, it is measure of organic matter and represents the
amount of oxygen required to oxidize the organic matter by strong oxidizing chemical
(potassium dichromate) under acidic condition.
Total nitrogen (TN: total nitrogen include organic nitrogen, ammonia, nitrite, and nitrate.
PH: is indication of acidic or basic nature of wastewater. A solution is neutral at PH 7.
The municipal wastewater contains microorganisms that play an important role in biological
waste treatment the principal groups of micro-organisms include bacteria, fungi, protozoa,
and algae.
Characterization of plant influent, effluent, and internal process streams provides plant
operations personnel with the information they need to properly control treatment processes.
As most water treatment processes are chemical reactions in nature the fundamentals of
wastewater chemistry are then necessary in understanding the wastewater characteristics and
hence in selecting, appropriate treatment technology to promote this understanding.
Wastewater characterization studies are conducted to determine the physical, chemical and
biological characteristics and the concentration of constituents in wastewater, and the best
means of reducing the pollutant concentrations.
Wastewater from the soft drink industry may include wasted soft drinks and syrup, water
from bottles and cans washing, detergents and caustics, and traces of lubricants used in the
production process machinery.
These pollutants contain organic and inorganic substances described by the 5-day
biochemical oxygen demand (BOD5), and chemical oxygen demand (COD). Since
wastewater from the soft drinks industry generally contains organic substances that are
readily biodegradable, biological processes are mainly used for its treatment. The
effectiveness/efficiency of the treatment depends on many factors, as described by Anielak in
a review of solutions and technologies for the treatment of food industry wastewater
It is estimated that almost 50% of waste water produced during the beverage production
comes from the process of bottle washing.
Caustic soda and sugar are also released along with water as major pollutants. Beverages
industries require large quantities of fresh water for cleansing and rinsing operations. Wasting
such a huge quantity of fresh water in the beverage industry has been a debate since many
decades. One basic cause of fresh water wastage is the reuse of glass bottles which requires a
huge expense of water as a rinsing and cleansing agent before they are refilled.
Ammonia mg/L 12 25 45
Nitrite mg/L 0 0 0
Nitrate mg/L 0 0 0
Total Phosphorus, as P mg/L 4 7 12
Organic mg/L 1 2 4
Inorganic mg/L 3 5 8
Faecal Coliform Col/100 mL 103 - 105 104 - 106 105 - 108
Source: Wastewater Engineering, Treatment and Reuse, Metcalf & Eddy, Inc., 4th Ed.,
McGraw-Hill Publishers, Boston MA, USA, 2003, p 186.
Table 6 Wastewater discharges to land or water regulation
3.3 OBJECTIVE
3.3.1 General Objective:
The main objective of this project is to characterize the wastewater generated in Gondar Pepsi
Cola Company before discharge to the environment.
CHAPTER FOUR
4. MATERIAL AND METHOD
4.1 MATERIAL AND EQUIPMENT USED
The following equipment and chemicals are used for conducting our project.
Equipment used
Thermometer: - an instrument that used to measure temperature of wastewater
sample.
DS meter: - an instrument, used to measure the Total Dissolved Solid (TDS)
present in the wastewater.
PH meter: - a device, used to measure the acidity or basicity of wastewater.
4.2 METHODOLOGY
For characterization of wastewater effluent in any plant sampling technique must be
conducted before any activity. A sample of wastewater was taken from different section of
Gondar Pepsi Cola Plant (GPCP). The sample was collected from the final effluent of the
plant, bottle washing effluent, simple syrup preparation room and water treatment plant. The
amount of wastewater effluent from GPCP varies from time to time due to the working of
different task such as: sanitation (five step and three step), simple syrup tank and filter
washing, backwashing of carbon purifier and sand filter in water treatment room and floor
washing of all processing room. A different sampling point was used for taking wastewater
sample due to the variation of effluent. Besides the above sampling points, a sample of waste
was taken from the common final effluent of the company after different tasks conducted.
Sampling was done during normal period of operation (during production), five step and
three step CIP period, backwashing in WTP, and washing in syrup room.
Temperature, PH, turbidity, TDS and TSS measurement was done for GPCP wastewater
effluent. The measurement technique for that characterization of wastewater effluent is
written as follows.
Determination of Temperature
The temperature of waste samples was measured using mercury thermometer at room
Temperature. There was a time gap between temperature measurement and sample taking
process, so the resulted temperature might be lower than accurate measurement.
Determination of PH
The PH of wastewater sample was measured using PH meter. The calibration was done by
using kcl solution, then a sample of waste was put to clean beaker and the probe was
immersed into the sample. Finally the displayed PH of wastewater was recorded.
Determination of total dissolved solids (TDS)
The total dissolved solid present in the wastewater sample was measured by DS meter which
is a product of Myron L Company. Wastewater sample was collected and added to the feeder
of DS meter, and then its bottom part was pressed to display TDS of sample.
Determination of Turbidity
The turbidity was determined photo electrically using turbidity meter. A sample of
wastewater was collected from the effluent line of GPCP. Turbidity of the waste was
measured and the results were expressed in term of turbidity units (NTU) for three different
sample.
Determination of TSS
A sample of wastewater was taken from GPCP wastewater effluent during production period
of Pepsi. TSS of this effluent was obtained by determining its TS firstly. A sample of
wastewater was measured and put in to evaporating dish. Sample contained evaporating dish
was subjected to evaporating using oven. Then the sample containing dish was removed from
oven and its mass was measured. Finally, total dissolved solid was calculated and total
suspended solid was obtained from TS and TDS. This method was repeated for a waste water
sample taken during sanitation and syrup and filter tank washing.
Sampling point
TSS(mg/l) 60 75 130
CHAPTER FIVE
5. RESULTS AND DISCUSSION
The temperature of wastewater effluent is different for different sampling. During production
period, the temperature of wastewater is 28 0c. This higher temperature comes from bottle
washing operation, which is processed at high temperature (steam temperature). In bottle
washer, there are steps that cause wastewater generation at higher temperature; those are hot
water rinse, caustic 1 and 2 rinses by heating using steam. During syrup tank and filter
washing, the temperature of the effluent has been 250c, which is measured at common
drainage pipe of bottle washer and washing wastewater. During weakly and product change
sanitation the temperature of wastewater is variable, from our measurement the temperature
fluctuates between 29 and 360c. This is due to CIP method.
According to the National Environment act, S.I No 5/1999 (wastewater discharge regulation),
all above temperature measurements are acceptable. NEA States temperature of wastewater
effluent from industry should be between 20 and 350c. Therefore, temperature of GPCP
wastewater effluent has no series impact on the environment.
We have found that, the PH of wastewater effluent from GPCP is 10.93 during production
period of Pepsi and Miranda, 10.87 during five step sanitation, 9.74 during syrup tank
washing and production process.
From the result we justify that, the wastewater has basic behavior. This is due to the usage of
caustic soda for washing bottles in bottle washer and for sanitation. GPCP uses much amount
of caustic soda for above purpose, this results high PH content wastewater generation.
From the standard discharge regulation NEA, the PH of wastewater discharge from industry
should be within a range of 6-9. But our PH value is out of this range, as stated above this is
due to caustic soda usage. High PH content wastewater has impact on aquatic life and the
environment therefore appropriate PH reduction method should be practiced before
discharging the wastewater to the environment.
Using DS meter we have found that the total dissolved solid of wastewater effluent is 1100
ppm for production time sample, 900 ppm for five step CIP wastewater sample and 1150 ppm
for syrup tank & filter washing wastewater sample. These values are acceptable based on
NEA wastewater discharge to land or water standards.
The TSS of GPCP wastewater effluent during production period is 60 mg/l. Based on NEA
Standards for Discharge of Effluent into Water or on Land, this value is acceptable. So the
total suspended solids of GPCP wastewater has no adverse effect on the aquatic life. During
sanitation much of wastewater is generated for one up to two hours this may increase the TSS
to 75mg/l in wastewater but it is acceptable for discharging to the environment. The
wastewater effluent during syrup tank washing is 130 mg/l. This value is above NEA
regulation due to the residue of DE left during syrup and filter tank washing.
The turbidity of wastewater was measured by turbidity meter. A value of 45.05 NTU during
production period, 54.65 NTU during sanitation and 345.89 NTU during syrup tank and filter
washing were obtained. Except washing period sample the other wastewater samples are
acceptable based on NEA standards for discharging the wastewater to the environment . The
source of high turbid wastewater is filter tank washing that contains DE residue. The strength
and concentration of wastewater generated during filter tank washing is higher than that of
operation period wastewater.
Temperature, PH, TDS, TSS and turbidity of GPCP wastewater effluent is measured and the
values are described on table 7. From table 7 some parameters are not conforms to standard.
The temperature and TDS of wastewater conforms to standard, but its PH exceeds the
maximum permissible limit. So PH has adverse effect on the environment. It is summarized
on table 9.
Absence of useful equipment in the plant and around sectors like COD meter, BOD
meter and the like.
Lack of full data.
We couldn’t measure all parameters of wastewater characterization due to availability
of equipment.
CHAPTER SIX
6. CONCLUSION AND RECOMMENDATION
6.1. CONCLUSION
From Gondar Pepsi Cola Plant, the characterization of wastewater is analyzed by determining
the physical and chemical property of wastewater effluent. Temperature, turbidity, PH, TSS
and TDS of wastewater effluent are measured and compared with NEA wastewater discharge
to water or land regulations. GPCP wastewater effluent has an average temperature of 27 0c,
average PH of 10.34, average TDS of 1025 ppm and TSS of 80 mg/l. From NEA regulation,
except PH the other parameters of GPCP wastewater effluent are acceptable for discharging
the wastewater to river. The main cause for high PH content of wastewater is caustic soda
usage for washing.
Generally by determining physical, chemical and biological parameters of wastewater
effluent, we can know the characteristics of wastewater, its degree of treatability and the
potential effect on the environment by comparing it with maximum permissible limit of
discharging wastewater to the environment.
6.2. RECOMMENDATION
We have done a project on characterization of GPCP wastewater effluent with some
limitations. We recommend that, for measuring the flow rate of GPCP wastewater effluent,
the drainage system must be suitable for sampling. It is advantageous if the construction of
drainage system passes through pipes and tanks that are suitable for sampling and treatment
process. The plant and the community will be safe if these wastewater properties are applied.
Simple treatment process should be applied by improving the current installation area of the
plant. Non treatment of wastewater might not be a series problem for a community compared
to a community pollutes the environment by itself, but characterization and simple treatment
process of waste water should be conducted to save the environment.
BOD and COD are essential parameters to know the characteristics of wastewater in GPCP.
So a further characterization of wastewater effluent in GPCP should be done by determining
BOD, COD and biological parameters. Wastewater property measurements such as: - BOD,
COD bottles and conductivity measurement should be present for analyzing wastewater
generation.
When we were in the factory we have seen all the production process of soft drinks. And as a
chemical engineering student we want to recommend the following things.
The plant has not effective and suitable drainage and waste disposal system it release almost
basic water at PH above 10 and it has badly odor these condition affects the aquatic life and
has many environmental impact. So it is possible to apply simple wastewater treatment
method, especially PH reduction by characterizing of wastewater effluent.
In bottle washer bottles are charged to pre cleaning section without removing the liquid inside
it. The liquid inside the bottle may contain waste water, urine, remaining of soft drink, oil and
related dirty flowing matters. And these dirty liquids are directly mix with cleaning water in
the pre cleaning section of washer. This cleaning water is used for on full day of continuous
washing. So we are suggesting that to remove or drain those dirty liquids from bottles before
entering to the washer. So that it can eliminate the contamination of bottles by unwanted
matters and increases the quality of cleaning water of the pre cleaning section.
There is a heat loss in CIP and boiler rooms. In the boiler room the hot water and hot caustic
tanks are not insulated. So it is possible to insulate the shell of the tank using the principle of
critical wall insulation thickens. In boiler plant, the chimney has a temperature of above
150oc so we can install air pre heater or economize.
Full bottles and empty bottles are dictated by human eye inspection this method is a very
back ward and it have lack of accuracy. If the bottle is detected improperly, broken bottle,
unfilled bottle or unpacked bottle and caustic carry bottle may pass. This lead to effect on
product quality. Also caustic is very dangers chemical so any residual of caustic that remain
in bottle may contact with the beverage and affect the customers of the products. So, it must
be replace human eye inspection by advanced technology electronics machine.
Because the plant uses old machines, it does not operate at its operation parameters that
shown on the manuals this affect the production process. For example it releases much
amount of waste gases to the environment and many bottles are broken during filling. As
much as possible use recently fabricated machinery and material to operate properly and
effectively.
Benefit and beneficiary
The benefit of this project is for management, knowing the amount and property of
wastewater generation in GPCP. The project provides a precondition for conducting
wastewater treatment process since there is no wastewater treatment process in GPCP.
CHAPTER SEVEN
7. OVERALL BENEFITS OF INTERNSHIP
7.1 BACKGROUND OF INTERNSHIP
Internships exist in a wide variety of industries and settings. An internship can be paid,
unpaid, or partially paid (in the form of a stipend). Internships may be part-time or full-time
and are usually flexible with student’s schedules. A typical internship lasts between one and
four months, but can be shorter or longer, depending on the organization involved. The act of
job shadowing may also constitute interning.
Internship is a great opportunity to practically prove the theoretical knowledge we got from
class into practice. Out of several departments that BIT is giving nowadays, chemical
engineering is one of those departments and also internship is one of great program that we
develop our theoretical and practical knowledge’s.
linkage coordinator we get the acceptance of MOHA soft drink S.C in Gondar Pepsi cola
plant.
During our time in the company, we observed almost all part of the company. We had a good
opportunity to deal with different sections of the company and each process in each section.
We were also capable of watching some processes from raw material feeding up to product
packaging.
The other experience we got is; how to control different machines when the production
process is still running, we worked with the laboratory assistant by while conducting different
tests
The challenging experience we got was finding solutions for existing problems, collecting
production data and specifying problems according to production quantity and quality.
7.2 MAIN BENEFITS OF INTERNSHIP
The experiences we gained during this internship program are categorized as;
o Practical skills
o Theoretical knowledge
o Inter-personal communication skills
o Team playing skills
o Leadership skills
o Work ethics & related issues, and finally
o Entrepreneurship skills
o Chemical preparation
o Solving machine problems
o Observing and controlling quality of the product
o The way of treating water, and
o How to check the pH variations in chemicals
and experiences we get form the internship with the theoretical knowledge we get from class.
This helped us in developing the theoretical knowledge and makes our previous knowledge
practically supported.
7.2.3 Improving Communication Skills
This one is the most common and important skill gained during our internship period. It helps
a person to interact with others in a better and pleasant manner. It is an art to present one’s
views, thoughts, and ideas to the listener.
It helped us in composing our project by asking question & info from the employees who
guided us in the best possible way. Our interactions and dealings with the workers made our
social interaction easy.
As a team member, someone contributes a lot in many ways. There by, this improves every
individual’s commutative knowledge of solving the existing problem. Being a team player,
everyone can improve the following
o Honesty
o Reliability
o Cooperating with collogues
o Punctuality
o Working independently
o Taking responsibility
o Creating goals
o Effective Communication
o Managing time effectively
o Being prepared to do everything for the team
Internship is an important tool for gaining experience and learning about one’s preferences
and interests. Perhaps most importantly, the experience obtained has a great importance up on
our life to choose and plan each of our future activity. Being an intern can build an individual
knowledgeable in;
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Polish), (2008)
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