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PPE Required:
OPERATIONAL STEPS
Introduction: this procedure validates the general function of the Reserval gas
analyzer. Use this procedure when starting up a Reserval at a new location, or
to re-validate the Reserval installation at an existing location.
1. Verify that the compressor air intake is located in uncontaminated air.
2. Verify that the Reserval lines from gas exhaust 1 and 2 are installed and
terminate outside the mud logging cabin.
3. Verify the air compressor regulator output pressure (min. 3 bars).
4. Verify the H2 Generator output pressure (0.5 bars).
5. Switch the Reserval ON, and wait for ignition of the FID flames.
6. Turn on the pump(s).
7. On the Reserval, verify on the screen that the pressures are within the
working range: air pressure 2 bar, H2 Pressure 0.5 bar, Gas OUT / Gas IN:
1.0 bar +/- 0.1 bar).
8. Verify on the Reserval screen that the flow rates are within the working range
(450 cc/min +/- 20 cc/min or 500 cc/min +/- 20 cc/min if Isotope Analyser is in
use).
9. Verify on the Reserval screen the FID Cell and column oven temperatures
are within the required operating range (FID: 150 deg. C +/- 2 deg. C,
Column oven: 50 deg. C +/- 0.5 deg C).
10. Wait for the baseline to become stable.
11. When the baseline is stable, carry out a full calibration check with
reference gases prior to commencing operations.
DETAILED PROCEDURE
2 Verify that the lines from gas exhaust 1 and 2 CAUTION: exhaust inside the cabin can result in
are installed and terminate outside the mud accumulation of toxic and/or flammable gases.
logging cabin.
6. Turn on the pump(s). Pump OUT if only gas OUT is being measured; Pump
OUT and Pump IN if Gas OUT-Gas IN measurement.
7. Verify that the pressures are within the Air pressure: 2 bar
working range. H2 Pressure 0.5 bar
Gas OUT: 1.0 bar +/- 0.1 bar
Gas IN (if used): 1.0 bar +/- 0.1 bar
8. Verify that the flow rates are within the Flow OUT if only gas OUT is being measured; Flow
working range. OUT and Flow IN if Gas OUT-Gas IN measurement.
Flow rate 450 cc/min +/- 20 cc/min or 500 cc/min +/-
20 cc/min if Isotope analyser is in use.
9. Verify the FID Cell and column oven FID: 150 deg. C +/- 2 deg. C:
temperatures are within the required Column oven: 50 deg. C +/- 0.5 deg C
operating range.
Injection #1 100 25 25 25 25 25 25
If calibration check results do not fall within the acceptable range, perform another calibration, followed by a
new calibration check.
END OF PROCEDURE
Sub Segment Date Version Developed by: Reviewed by: Validated by: Approved by:
GSS 20 Nov. 2014 2.2 G. Haines P. Laz P. Laz/ D. Kumar
G. Haines