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Superior client serv ice. Electrical confidence.

CARGILL LIMITED

2016 Transformer Oil Sampling


and
Analysis

June 7, 2016 File: C3330-10

Project Manager: George Shehata, P.Eng.

info@magnaiv.com Engineering & Technical Field Services Canada


www.magnaiv.com United States
Chile
1103 Parsons Road SW
Edmonton, AB T6X 0X2
Superior client serv ice. Electrical confidence. p 780.462.3111 f 780.462.9799 tf 800.462.3157

File: C3330-10
June 28, 2016
CARGILL LIMITED Via: email
801 LOW LEVEL ROAD fax
NORTH VANCOUVER, BC V7L 1A7 mail
Attention: Mr. Ron Ludwig
Supervisor, Electrical
Dear Sir:

Re: Oil Sampling and Analysis – North Vancouver Facility


We are pleased to submit the insulating fluid report and test sheets for the three (3) transformers
and one (1) OCB located at the North Vancouver facility. The transformer sampling was
performed by James Powell on June 7, 2016 in accordance with ASTM D923 and D3613
standards. The laboratory testing was completed by The Chemlab of Calgary. Review of results
and analysis was provided by the undersigned.

Based on the analysis of the laboratory results, all equipment is in good condition and suitable
for continued service. Once again, both the East and West transformers are showing elevated
Ethylene indicating higher temperature internal heating however, since there has been no
significant generation and all other dissolved gases and standard fluid quality tests are within
IEEE acceptable limits for in-service equipment, the units are of no immediate concern. Annual
sampling is highly recommended to monitor any further generation. The Sub 2 transformer is
filled with Natural Ester (FR3) – it appears there is elevated Ethane however, the limits indicated
are for mineral oil only. Natural ester generates Ethane under normal operation (test limit is
400PPM) therefore the current value is within acceptable limits. In addition, the interfacial
tension appears low however, the test limit is 18 for Natural ester. As such all values meet the
recommended test limits for natural ester. The OCB is showing all dissolved gases and tested
fluid quality properties to be within acceptable limits. All equipment is classified as category
Type 1. Equipment in this category shows acceptable test results, with some showing minor
elevated gas levels. Close observation of dissolved gases in the oil, along with the fluid quality
properties, provides the most valuable information about your equipment health. All units are
recommended for annual resampling with electrical tests performed at 2 year intervals. This
testing schedule will allow us to maintain a comprehensive trend of all properties, and provide
accurate analysis on the condition and operational reliability of your equipment. Please see
Section 3.0 – Summary of Results and Deficiencies for a complete breakdown.

info@magnaiv.com Engineering & Technical Field Services Canada


www.magnaiv.com United States
Chile
We trust this report meets with your approval and requirements. Should you need further
information or assistance, please do not hesitate to contact us. Thank you for retaining the
services of Magna IV Engineering. We look forward to being of service to you again in the future.
Yours Truly,
MAGNA IV ENGINEERING

Stephanie Parsons
Oil Analysis Project Manager

3 | Page
INDEX

1.0. SCOPE OF WORK .......................................................................................................................... 5


2.0. SUMMARY OF TESTS ....................................................................................................................... 6
3.0. SUMMARY OF RESULTS AND DEFICIENCIES ................................................................................ 8
4.0. TEST RESULTS ................................................................................................................................... 9

4 | Page
1.0. SCOPE OF WORK
As per Magna IV Engineering’s standard practices for transformer oil sampling, our scope
of work consisted of:
 Providing Transformer Inspection
 Recording Nameplate Data
 Reading and resetting Gauges
 Providing Inspection Report
 Procurement of oil samples in accordance with ASTM D923 & D3613
- obtain one syringe for gas-in-oil analysis & moisture content
- obtain bottle sample for fluid quality tests
 The Chemlab of Calgary performs all analytical tests, consisting of:
 Gas Analysis (DGA) D-3612
 Moisture Content D-1533B
 Interfacial Tension D-971
 Acid Number D-974
 Color Number D-1500
 Visual Examination D-1524
 Dielectric Breakdown D1816 @ 1mm

 The Chemlab is responsible for proper disposal of samples.


 Analysis of Laboratory results by Magna IV Engineering. Tools utilized:
 Duval Triangle
 GA Key Gas Method
 DGA Rogers Ratio Method
 DGA Cellulose
 DGA IEEE/ANSI
 Specific History and Trending (Generation vs. Time)
 Document, interpret and evaluate results, and recommend corrective or follow up
action.
 Prepare traditional summary sheets and lifetime trending graphs.
 Prepare report detailing findings, recommendations and corrective action as
required.

5 | Page
2.0. SUMMARY OF TESTS
For your reference and confirmation of the specific tests performed and their analytical
value, we provide the following highlight information. All transformer tests were
performed as per the latest ASTM standards.

Specific tests performed include:

 ASTM D1816 - Liquid Dielectric Test


The dielectric breakdown voltage of an insulating liquid is important as a measure of
the liquid’s ability to withstand electric stress without failure. It serves to indicate the
presence of contaminating agents, such as water, dirt, moisture, cellulosic fibers or
conducting particles in the liquid, one or more of which may be present in significant
concentrations when low dielectric breakdown values are found by test. However, a
high dielectric breakdown voltage does not indicate that the concentrations of
contaminants that are present in the liquid between the electrodes are not large
enough to negatively affect the average breakdown voltage of the liquid when
tested by this method.

 ASTM D971 - Interfacial Tension


This method has been shown by practice to give a reliable indication of the presence
of hydrophilic compounds. When certain contaminants such as soaps, paints
varnishes and oxidation products are present in the oil, the film strength of the oil is
weakened, thus requiring less force to rupture. For oils in service, a decreasing value
indicates the accumulation of contaminants and oxidation products, which may
attack the insulation and interfere with the cooling of transformer windings.

 ASTM D1533 - Moisture Content


The electrical characteristics of an insulating liquid are deleteriously affected by its
water content. A high water content may make a dielectric liquid unsuitable for some
applications because a deterioration in properties such as dielectric breakdown
voltage may occur. This test is suitable for use in acceptance specifications, in control
of processing and in evaluating the condition of dielectric liquids in service.

 ASTM D974 - Neutralization Number


The acid number of an oil is a measure of the amount of acidic materials present. As
oils age in service the acidity, and therefore the acid number, increases. A used oil
having a high acid number indicates the oil is either oxidized or contaminated with
materials such as varnish, paint or other foreign matter. This test serves as an indicator
of the potential of the oil to form sludge.

 ASTM D1500 – Color Number


The color of a new oil is generally accepted as an index of the degree of
refinement. For oils in service, an increasing or high color number is an indication of
contamination, deterioration or both.

6 | Page
 ASTM D3612 - Dissolved Gas Analysis
Gas analysis is based upon the fact that both electrical insulating oil and cellulosic
insulation break down under abnormal thermal or electrical stress. The results of these
stresses are both volatile and non-volatile gases, known as fault gases. Gas analysis is
the technique that identifies fault gases, relates their quantity, generation rate and
relevant ratios to type and severity of fault.

Typical fault gases analyzed are:


Hydrogen H2
Methane CH4
Ethane C2H6
Ethylene C2H4
Acetylene C2H2
Carbon Monoxide CO
Carbon Dioxide CO2

Typical types of transformer problems that can be detected are:


 thermal degradation
- low temperature
- high temperature (hot spot)
 arcing
 partial discharges
 degradation of paper insulation

Increased frequency or periodic testing will significantly increase the value and
accuracy of fault gas analysis.

7 | Page
3.0. SUMMARY OF RESULTS AND DEFICIENCIES
Transformers typically can be broken down into the following categories:

Type 1 Transformers in this category show acceptable test results, with a few
transformers showing signs of minor non-serious overheating (re-test
recommended in one year). Variations of Type 1 transformers may exist
pending past records and age of units.
Type 2 This category covers any transformer showing test results where some concern
is evident (re-test recommended in six months).
Type 3 Transformers in this category show signs of serious fault gas concentrations or
very poor chemical properties (prompt re-tests or further investigations are
required).
Type 4 Mechanical deficiencies (corrective action to be taken as soon as possible or
as recommended).

Please refer to the test sheets (5 pages) for a detailed breakdown of results and
recommendations. Following is the Summary of Results and Deficiencies.

Transformer
Analysis Recommended
Identification / Year Comments
Type Retest
Serial Number Manufactured

Slight elevation in Ethylene – higher


temperature internal heating – no
immediate concern. All other dissolved
East TX gases and tested fluid properties within
1967 1 1 Year acceptable limits. Annual sampling highly
293639 recommended to monitor any further
generation. Check loading conditions and
cooling means. No major deficiencies
noted.
Slight elevation in Ethylene – higher
temperature internal heating – no
immediate concern. All other dissolved
West TX gases and tested fluid properties within
1967 1 1 Year acceptable limits. Annual sampling highly
293638 recommended to monitor any further
generation. Check loading conditions and
cooling means. No major deficiencies
noted.
All dissolved gases and standard fluid quality
Sub 2 properties within acceptable limits for
2010 1 1 Year Natural Ester Insulating fluid. Annual
1059001354 sampling should be maintained. No major
deficiencies noted.
All dissolved gases and standard fluid quality
6OCB1 properties within acceptable limits showing
1967 1 1 Year no significant change. Annual sampling
60503 should be maintained. No major
deficiencies noted.

8 | Page
4.0. TEST RESULTS
Following is a copy of all individual test results. We recommend you review the results
and graphs at your convenience to better understand our analysis and the condition of
your equipment.

Each piece of equipment consists of the following 4 pages of documentation:


Page 1 Transformer nameplate, identification name, oil and gas results and any
notable comments and deficiencies.
Pages 2&3 Graphs for all generated gases and chemical analysis tests. This provides a
more visual idea of determining the trending of these gases. All limits are
based upon standards widely accepted throughout the industry.
Page 4 Inspection sheet, nameplate data, gauge recordings.

9 | Page
Cargill Terminal
East - TX
S/N: 293639

Oil & Gas Results


C3330-10

Nameplate Information
Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Nameplate Information
Serial Number: 293639 kV Rating: 72.000/0.575 Designation: East - TX
Apparatus Type: TRN Manufacturer: WESTINGHOUSE Fluid Type: OIL
kVA Rating: 4000 Year Manufactured: 1967 Fluid Capacity (G): 750
Sample Date: Jun-7-2016 Jun-10-2015

Job Number: C3330-10 C3330-7

Dissolved Gas Analysis D3612-C Limits Expressed in PPM


Hydrogen (H₂) 100 4 5

Methane (CH₄) 120 3 3

Ethane (C₂H₆) 65.0 3.2 3.1

Ethylene (C₂H₄) 50.0 62.0 58.2

Acetylene (C₂H₂) 2.0 0.0 0.0

Carbon Monoxide (CO) 1000 146 194

Carbon Dioxide (CO₂) 10000 7180 7550

Oxygen (O₂) 29000 27500

Nitrogen (N₂) 66800 71200

Total Dissolved Combustible Gas 218 263

Total Gas Content (%) 10.320 10.660

Fluid Quality Analysis Limits Voltage Class >69kV - <230kV


Moisture Content D1533 (ppm) 25 16 17

Interfacial Tension D971 (mN/m) 30.0 31.8 32.4

Acid Number D974 (mg KOH/g) 0.150 0.018 0.022

Color Number D1500 (Relative) 3.5 L1.5 1.5

Visual Examination D1524 (Relative) CLEAR CLEAR CLEAR

Dielectric Breakdown @ 1mm D1816 (kV) 28 33 40

Dielectric Breakdown D877 (kV) 26

Power Factor @ 25°C D924 (%) 0.5

Power Factor @ 100°C D924 (%) 5.0

Additional Fluid Quality Tests Limits


PCB D4059 (ppm) 2.0 - 3.7

Specific Gravity D4052 (Relative) 0.91

Oxidation Inhibitor D2668 (%) 0.08 - 0.3

Notes:

Magna IV Engineering Serial Number: 293639 Page 1 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Historic Graphs and Diagnostic Charts
Total Gas Content (%) Key Gas Comparison (ppm)
(All Gases) 160
12
140
10
120
8 100
6 80
4 60
40
2
20
0
0
Jun-16

Jun-15
CO - H2 - Meth - Et h - Et hy - Ace

Combustible Gases
Methane (CH4) Ethane (C2H6) Ethylene (C2H4)

3.5 70
3.5
3 60
3
Parts Per Million

Parts Per Million

Parts Per Million


2.5 2.5 50
2 2 40
1.5 1.5 30
1 1 20
0.5 0.5 10
0 0 0
Jun-16

Jun-15
Jun-16

Jun-15

Jun-16

Jun-15
Acetylene (C2H2) Hydrogen (H2) Carbon Monoxide (CO)
1 6 250
0.9
0.8 5 200
Parts Per Million

Parts Per Million

Parts Per Million

0.7 4
0.6 150
0.5 3
0.4 100
0.3 2
0.2 1 50
0.1
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Non-Combustible Gases
Carbon Dioxide (CO2) Thousands Nitrogen (N2) Thousands Oxygen (O2)
8000 80 35
7000 70 30
Parts Per Million

Parts Per Million

Parts Per Million

6000 60 25
5000 50
20
4000 40
15
3000 30
2000 20 10
1000 10 5
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Magna IV Engineering Serial Number: 293639 Page 2 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Fluid Analysis
Moisture Content Interfacial Tension Acid Number
30 (Should be <Limit) (Should be >Limit) (Should <Limit)
35 0.16
25
30 0.14
Parts Per Million

20 25 0.12

mg KOH/g
0.1

mN/m
15 20
0.08
15
10 0.06
10 0.04
5 5 0.02
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15
Color Number Dielectric Breakdown D877 Dielectric Breakdown D1816
4 (Should be <Limit) (Should be >Limit) (Should be >Limit)
45
3.5
40
3 35
2.5 30
2 25

kV
1.5 20
15
1
10
0.5 5
0 0
Jun-16

Jun-15

Jun-16

Jun-15

Actual Values
Acceptable Limits

Magna IV Engineering Serial Number: 293639 Page 3 of 3


PREPARED FOR

CARGILL
OIL FILLED EQUIPMENT INSPECTION SHEET CANF-5E006
WO# C3330-10 TAG # EAST TX DATE June 7, 2016
SITE CARGILL TERMINAL TEST BY JMP
AREA MAIN SUB STANDARD MAINTENANCE APPROVED BY

NAMEPLATE DATA
EQUIPMENT TX KVA 4000 # OF TAPS 5
MANUF. WESTINGHOUSE PRI VOLTS 72KV TAP FOUND/LEFT 3 / 3
TYPE ONAN SEC VOLTS 575 %IMPED 3.70%
SO# 293639 AMPS WEIGHT
YEAR 1967 CAPACITY LTRS 750 GALS TEMP RISE
OIL TYPE MINERAL SYSTEM BREATHING
DATE OF LAST OIL CHANGE (IF KNOWN) UNKNOWN

PRE-SAMPLING CHECKLIST
CRITERIA YES NO CRITERIA YES NO COMMENTS
ADEQUATE CLEARANCE PCB CONTAMINATED 3.7 PPM
TANK PRESSURE (Min: -1 Psi (-6.89 kPa)) LOW OIL LEVEL (GAUGE @ LOW) PROPER LEVEL

INSPECTIONS
DESCRIPTION YES NO DESCRIPTION OK FAIL COMMENTS
BREATHERS SILICA DESICANT CONDITION BLUE
HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION DUSTY
LV BUSHINGS ACCESSIBLE LV BUSHING CONDITION DUSTY
RADIATORS INSTALLED RADIATOR CONDITION N/A
CONSERVATOR TANK OIL LEAKS (WHERE) OK
GROUNDING (2 LOCATIONS) CORROSION / RUST ACCUMULATION PAINT IS GOOD
PHYSICAL DAMAGE DIRT ACCUMULATION DUSTY
NITROGEN ADDED
RELIEF VALVE INSTALLED

GAUGE DOCUMENTATION
GAUGE READING DRAGHAND RESET GAUGE READING
OIL TEMP 40 °C 50 °C NO OIL LEVEL SEE DIAGRAM AT RIGHT
WINDING TEMP N/A YES / NO PRESSURE PSI KPA

SAMPLE DATA
SAMPLE COLOR SAMPLE POINT BOTTOM VALVE
STRAW WHITE ORANGE BLACK SEDIMENT NO
STRAW YELLOW REDDISH ORANGE OTHER: AMB. TEMP 27.0 °C
LEMON YELLOW BROWN HUMIDITY 78 %
Sampler: JMP Syringe #: DM 635 PO# for Sampling Lab: 1006975
Tests Required (Internal Purposes Only) REPORT RUSH: NO
DGA D3612C Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:
Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation) 1. NO WINDING TEMP GAUGE
Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP TRANSFORMER IS IN A VAULT
Acid Number D974 Power Factor 100°C D924 Viscosity D88

Color/Visual D1500, D1524 Specific Gravity D1298 Other:


Dielectric 2.5mm D877 PCB

East Tx Oil Filled Equipment Inspection Page 1 of 1


Cargill Terminal
West - TX
S/N: 293638

Oil & Gas Results


C3330-10

Nameplate Information
Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Nameplate Information
Serial Number: 293638 kV Rating: 72.000/0.575 Designation: West - TX
Apparatus Type: TRN Manufacturer: WESTINGHOUSE Fluid Type: OIL
kVA Rating: 4000 Year Manufactured: 1967 Fluid Capacity (G): 750
Sample Date: Jun-7-2016 Jun-10-2015

Job Number: C3330-10 C3330-7

Dissolved Gas Analysis D3612-C Limits Expressed in PPM


Hydrogen (H₂) 100 7 8

Methane (CH₄) 120 5 5

Ethane (C₂H₆) 65.0 4.3 4.1

Ethylene (C₂H₄) 50.0 71.9 64.8

Acetylene (C₂H₂) 2.0 0.0 0.0

Carbon Monoxide (CO) 1000 212 231

Carbon Dioxide (CO₂) 10000 4880 4640

Oxygen (O₂) 28300 24300

Nitrogen (N₂) 74300 68400

Total Dissolved Combustible Gas 300 313

Total Gas Content (%) 10.780 9.770

Fluid Quality Analysis Limits Voltage Class >69kV - <230kV


Moisture Content D1533 (ppm) 25 13 7

Interfacial Tension D971 (mN/m) 30.0 32.3 32.8

Acid Number D974 (mg KOH/g) 0.150 0.014 0.014

Color Number D1500 (Relative) 3.5 L2.0 2

Visual Examination D1524 (Relative) CLEAR CLEAR CLEAR

Dielectric Breakdown @ 1mm D1816 (kV) 28 39 36

Dielectric Breakdown D877 (kV) 26

Power Factor @ 25°C D924 (%) 0.5

Power Factor @ 100°C D924 (%) 5.0

Additional Fluid Quality Tests Limits


PCB D4059 (ppm) 2.0 - 6

Specific Gravity D4052 (Relative) 0.91

Oxidation Inhibitor D2668 (%) 0.08 - 0.3

Notes:

Magna IV Engineering Serial Number: 293638 Page 1 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Historic Graphs and Diagnostic Charts
Total Gas Content (%) Key Gas Comparison (ppm)
(All Gases) 250
12
10 200
8
150
6
100
4
2 50
0
0
Jun-16

Jun-15
CO - H2 - Meth - Et h - Et hy - Ace

Combustible Gases
Methane (CH4) Ethane (C2H6) Ethylene (C2H4)

6 80
5
70
5
4
Parts Per Million

Parts Per Million

Parts Per Million


60
4 50
3
3 40
2 30
2
20
1 1
10
0 0 0
Jun-16

Jun-15
Jun-16

Jun-15

Jun-16

Jun-15
Acetylene (C2H2) Hydrogen (H2) Carbon Monoxide (CO)
1 9 250
0.9 8
0.8 7 200
Parts Per Million

Parts Per Million

Parts Per Million

0.7 6
0.6 150
5
0.5
4
0.4 100
0.3 3
0.2 2 50
0.1 1
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Non-Combustible Gases
Carbon Dioxide (CO2) Thousands Nitrogen (N2) Thousands Oxygen (O2)
6000 80 30

5000 70 25
Parts Per Million

Parts Per Million

Parts Per Million

60
4000 50 20

3000 40 15

2000 30 10
20
1000 10 5

0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Magna IV Engineering Serial Number: 293638 Page 2 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Fluid Analysis
Moisture Content Interfacial Tension Acid Number
30 (Should be <Limit) (Should be >Limit) (Should <Limit)
35 0.16
25
30 0.14
Parts Per Million

20 25 0.12

mg KOH/g
0.1

mN/m
15 20
0.08
15
10 0.06
10 0.04
5 5 0.02
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15
Color Number Dielectric Breakdown D877 Dielectric Breakdown D1816
4 (Should be <Limit) (Should be >Limit) (Should be >Limit)
45
3.5
40
3 35
2.5 30
2 25

kV
1.5 20
15
1
10
0.5 5
0 0
Jun-16

Jun-15

Jun-16

Jun-15

Actual Values
Acceptable Limits

Magna IV Engineering Serial Number: 293638 Page 3 of 3


PREPARED FOR

CARGILL
OIL FILLED EQUIPMENT INSPECTION SHEET CANF-5E006
WO# C3330-10 TAG # WEST TX DATE June 7, 2016
SITE CARGILL TERMINAL TEST BY JMP
AREA MAIN SUB STANDARD MAINTENANCE APPROVED BY

NAMEPLATE DATA
EQUIPMENT TX KVA 4000 # OF TAPS 5
MANUF. WESTINGHOUSE PRI VOLTS 72KV TAP FOUND/LEFT 3 / 3
TYPE ONAN SEC VOLTS 575 %IMPED 3.70%
SO# 293638 AMPS WEIGHT
YEAR 1967 CAPACITY LTRS 750 GALS TEMP RISE
OIL TYPE MINERAL SYSTEM BREATHING
DATE OF LAST OIL CHANGE (IF KNOWN) UNKNOWN

PRE-SAMPLING CHECKLIST
CRITERIA YES NO CRITERIA YES NO COMMENTS
ADEQUATE CLEARANCE PCB CONTAMINATED 6 PPM
TANK PRESSURE (Min: -1 Psi (-6.89 kPa)) LOW OIL LEVEL (GAUGE @ LOW) PROPER LEVEL

INSPECTIONS
DESCRIPTION YES NO DESCRIPTION OK FAIL COMMENTS
BREATHERS SILICA DESICANT CONDITION BLUE
HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION DUSTY
LV BUSHINGS ACCESSIBLE LV BUSHING CONDITION DUSTY
RADIATORS INSTALLED RADIATOR CONDITION N/A
CONSERVATOR TANK OIL LEAKS (WHERE) OK
GROUNDING (2 LOCATIONS) CORROSION / RUST ACCUMULATION PAINT IS GOOD
PHYSICAL DAMAGE DIRT ACCUMULATION DUSTY
NITROGEN ADDED
RELIEF VALVE INSTALLED

GAUGE DOCUMENTATION
GAUGE READING DRAGHAND RESET GAUGE READING
OIL TEMP 35 °C 40 °C NO OIL LEVEL SEE DIAGRAM AT RIGHT
WINDING TEMP N/A YES / NO PRESSURE PSI KPA

SAMPLE DATA
SAMPLE COLOR SAMPLE POINT BOTTOM VALVE
STRAW WHITE ORANGE BLACK SEDIMENT NO
STRAW YELLOW REDDISH ORANGE OTHER: AMB. TEMP 26.0 °C
LEMON YELLOW BROWN HUMIDITY 78 %
Sampler: JMP Syringe #: CO 376 PO# for Sampling Lab: 1006975
Tests Required (Internal Purposes Only) REPORT RUSH: NO
DGA D3612C Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:
Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation) 1. NO WINDING TEMP GAUGE
Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP TRANSFORMER IS IN VAULT.
Acid Number D974 Power Factor 100°C D924 Viscosity D88 2. IMPERIAL GALLONS
Color/Visual D1500, D1524 Specific Gravity D1298 Other:
Dielectric 2.5mm D877 PCB

West Tx Oil Filled Equipment Inspection Page 1 of 1


Cargill Terminal
Sub 2
S/N: 1059001354

Oil & Gas Results


C3330-10

Nameplate Information
Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Nameplate Information
Serial Number: 1059001354 kV Rating: 12.400/0.575 Designation: Sub 2
Apparatus Type: TRN Manufacturer: COOPER Fluid Type: ESTER
kVA Rating: 3000 Year Manufactured: 2010 Fluid Capacity (L): 1250
Sample Date: Jun-7-2016 Jun-10-2015

Job Number: C3330-10 C3330-7

Dissolved Gas Analysis D3612-C Limits Expressed in PPM


Hydrogen (H₂) 100 36 36

Methane (CH₄) 120 6 6

Ethane (C₂H₆) 65.0 192.9 195.6

Ethylene (C₂H₄) 50.0 6.3 8.2

Acetylene (C₂H₂) 2.0 0.0 0.0

Carbon Monoxide (CO) 1000 36 38

Carbon Dioxide (CO₂) 10000 310 330

Oxygen (O₂) 1500 2400

Nitrogen (N₂) 67600 66000

Total Dissolved Combustible Gas 277 284

Total Gas Content (%) 6.970 6.900

Fluid Quality Analysis Limits Voltage Class ≤69kV


Moisture Content D1533 (ppm) 35 12 15

Interfacial Tension D971 (mN/m) 25.0 23.3 22.9

Acid Number D974 (mg KOH/g) 0.200 0.020 0.024

Color Number D1500 (Relative) 3.5

Visual Examination D1524 (Relative) CLEAR CLEAR CLEAR

Dielectric Breakdown @ 1mm D1816 (kV) 23 37 47

Dielectric Breakdown D877 (kV) 26

Power Factor @ 25°C D924 (%) 0.5

Power Factor @ 100°C D924 (%) 5.0

Additional Fluid Quality Tests Limits


PCB D4059 (ppm) 2.0 - <0.5

Specific Gravity D4052 (Relative) 0.91

Oxidation Inhibitor D2668 (%) 0.08 - 0.3

Notes:
07/06/2016 : Limits based on Mineral Oil Insulating Fluid.
All Results considered normal for Natural Ester Insulating Fluid.

Magna IV Engineering Serial Number: 1059001354 Page 1 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Historic Graphs and Diagnostic Charts
Total Gas Content (%) Key Gas Comparison (ppm)
(All Gases) 250
8
7 200
6
5 150
4
3 100
2
1 50
0
0
Jun-16

Jun-15
CO - H2 - Meth - Et h - Et hy - Ace

Combustible Gases
Methane (CH4) Ethane (C2H6) Ethylene (C2H4)

7 9
250
8
6
200 7
Parts Per Million

Parts Per Million

Parts Per Million


5 6
4 150 5
3 4
100
3
2
50 2
1
1
0 0 0
Jun-16

Jun-15
Jun-16

Jun-15

Jun-16

Jun-15
Acetylene (C2H2) Hydrogen (H2) Carbon Monoxide (CO)
1 40 40
0.9 35 35
0.8
30 30
Parts Per Million

Parts Per Million

Parts Per Million

0.7
0.6 25 25
0.5 20 20
0.4 15 15
0.3
10 10
0.2
0.1 5 5
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Non-Combustible Gases
Carbon Dioxide (CO2) Thousands Nitrogen (N2) Thousands Oxygen (O2)
350 80 3
300 70 2.5
Parts Per Million

Parts Per Million

Parts Per Million

250 60
50 2
200
40 1.5
150
30 1
100 20
50 10 0.5

0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Magna IV Engineering Serial Number: 1059001354 Page 2 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Fluid Analysis
Moisture Content Interfacial Tension Acid Number
40 (Should be <Limit) (Should be >Limit) (Should be <Limit)
30 0.25
35
30 25
Parts Per Million

0.2
25 20

mg KOH/g
0.15

mN/m
20
15
15 0.1
10
10
5 0.05
5
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15
Color Number Dielectric Breakdown D877 Dielectric Breakdown D1816
(Should be <Limit) (Should be >Limit) (Should be >Limit)
50
45
40
35
30

kV
25
20
15
10
5
0

Jun-16

Jun-15

Actual Values
Acceptable Limits

Magna IV Engineering Serial Number: 1059001354 Page 3 of 3


PREPARED FOR

CARGILL
OIL FILLED EQUIPMENT INSPECTION SHEET CANF-5E006
WO# C3330-10 TAG # SUBSTATION 2 DATE June 7, 2016
SITE CARGILL TERMINAL TEST BY SB
AREA SUB 2 STANDARD MAINTENANCE APPROVED BY

NAMEPLATE DATA
EQUIPMENT TX KVA 3000 # OF TAPS 5
MANUF. COOPER PRI VOLTS 12.4Kv TAP FOUND/LEFT 3 / 3
TYPE ONAN SEC VOLTS 575 %IMPED
SO# 1059001354 AMPS WEIGHT
YEAR 2010 CAPACITY 1250 LTRS GALS TEMP RISE
OIL TYPE FR3 SYSTEM BREATHING
DATE OF LAST OIL CHANGE (IF KNOWN) NEW TRANSFORMER

PRE-SAMPLING CHECKLIST
CRITERIA YES NO CRITERIA YES NO COMMENTS
ADEQUATE CLEARANCE PCB CONTAMINATED UNKNOWN
TANK PRESSURE (Min: -1 Psi (-6.89 kPa)) LOW OIL LEVEL (GAUGE @ LOW) PROPER LEVEL

INSPECTIONS
DESCRIPTION YES NO DESCRIPTION OK FAIL COMMENTS
BREATHERS SILICA DESICANT CONDITION NOT USED
HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION
LV BUSHINGS ACCESSIBLE LV BUSHING CONDITION
RADIATORS INSTALLED RADIATOR CONDITION OK
CONSERVATOR TANK OIL LEAKS (WHERE) OK
GROUNDING (2 LOCATIONS) CORROSION / RUST ACCUMULATION PAINT IS GOOD
PHYSICAL DAMAGE DIRT ACCUMULATION DUSTY
NITROGEN ADDED
RELIEF VALVE INSTALLED

GAUGE DOCUMENTATION
GAUGE READING DRAGHAND RESET GAUGE READING
OIL TEMP 40 °C 40 °C NO OIL LEVEL SEE DIAGRAM AT RIGHT
WINDING TEMP N/A YES / NO PRESSURE 1 PSI KPA

SAMPLE DATA
SAMPLE COLOR SAMPLE POINT BOTTOM VALVE
STRAW WHITE ORANGE BLACK SEDIMENT NO
STRAW YELLOW REDDISH ORANGE OTHER: AMB. TEMP 26.0 °C
LEMON YELLOW BROWN HUMIDITY 40 %
Sampler: SB Syringe #: DS 264 PO# for Sampling Lab: 1006975
Tests Required (Internal Purposes Only) REPORT RUSH: NO
DGA D3612C Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:
Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation) 1. NO WINDING TEMP GAUGE
Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP TRANSFORMER IS IN A VAULT
Acid Number D974 Power Factor 100°C D924 Viscosity D88

Color/Visual D1500, D1524 Specific Gravity D1298 Other:


Dielectric 2.5mm D877 PCB

Substation 2 Oil Filled Equipment Inspection Page 1 of 1


Cargill Terminal
6OCB1
S/N: 60503

Oil & Gas Results


C3330-10

Nameplate Information
Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Nameplate Information
Serial Number: 60503 kV Rating: 72.000 Designation: 6OCB1
Apparatus Type: OCB Manufacturer: GE Fluid Type: OIL
kVA Rating: Year Manufactured: 1967 Fluid Capacity (G): 575
Sample Date: Jun-7-2016 Jun-10-2015

Job Number: C3330-10 C3330-7

Dissolved Gas Analysis D3612-C Limits Expressed in PPM


Hydrogen (H₂) 100 0 1

Methane (CH₄) 120 1 1

Ethane (C₂H₆) 65.0 0.0 0.0

Ethylene (C₂H₄) 50.0 0.8 0.7

Acetylene (C₂H₂) 2.0 0.0 0.0

Carbon Monoxide (CO) 1000 25 31

Carbon Dioxide (CO₂) 10000 560 580

Oxygen (O₂) 30300 27400

Nitrogen (N₂) 65500 63900

Total Dissolved Combustible Gas 27 34

Total Gas Content (%) 9.630 9.200

Fluid Quality Analysis Limits Voltage Class >69kV - <230kV


Moisture Content D1533 (ppm) 25

Interfacial Tension D971 (mN/m) 30.0 32.0 32.5

Acid Number D974 (mg KOH/g) 0.150 0.022 0.025

Color Number D1500 (Relative) 3.5 L1.5 1.5

Visual Examination D1524 (Relative) CLEAR CLEAR CLEAR

Dielectric Breakdown @ 1mm D1816 (kV) 28 32 36

Dielectric Breakdown D877 (kV) 26

Power Factor @ 25°C D924 (%) 0.5

Power Factor @ 100°C D924 (%) 5.0

Additional Fluid Quality Tests Limits


PCB D4059 (ppm) 2.0 - <0.5

Specific Gravity D4052 (Relative) 0.91

Oxidation Inhibitor D2668 (%) 0.08 - 0.3

Notes:
2016-06-07 : All results considered normal for OCB operation

Magna IV Engineering Serial Number: 60503 Page 1 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Historic Graphs and Diagnostic Charts
Total Gas Content (%) Key Gas Comparison (ppm)
(All Gases) 30
12
25
10
8 20

6 15
4 10
2
5
0
0
Jun-16

Jun-15
CO - H2 - Met h - Eth - Et hy - Ace

Combustible Gases
Methane (CH4) Ethane (C2H6) Ethylene (C2H4)

1.2 0.9
1
0.8
1 0.7
0.8
Parts Per Million

Parts Per Million

Parts Per Million


0.8 0.6
0.6 0.5
0.6
0.4
0.4
0.4 0.3
0.2 0.2
0.2
0.1
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15
Acetylene (C2H2) Hydrogen (H2) Carbon Monoxide (CO)
1 1.2 35
0.9
1 30
0.8
Parts Per Million

Parts Per Million

Parts Per Million

0.7 25
0.8
0.6 20
0.5 0.6
0.4 15
0.3 0.4
10
0.2 0.2 5
0.1
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Non-Combustible Gases
Carbon Dioxide (CO2) Thousands Nitrogen (N2) Thousands Oxygen (O2)
700 70 35
600 60 30
Parts Per Million

Parts Per Million

Parts Per Million

500 50 25
400 40 20
300 30 15
200 20 10
100 10 5
0 0 0
Jun-16

Jun-15

Jun-16

Jun-15

Jun-16

Jun-15

Magna IV Engineering Serial Number: 60503 Page 2 of 3


Fluid Test Report Cargill Limited
Maintenance Cargill Terminal
Fluid Analysis
Moisture Content Interfacial Tension Acid Number
(Should be <Limit) (Should be >Limit) (Should <Limit)
35 0.16
30 0.14
25 0.12

mg KOH/g
0.1
20

mN/m
0.08
15
0.06
10 0.04
5 0.02
0 0

Jun-16

Jun-15

Jun-16

Jun-15
Color Number Dielectric Breakdown D877 Dielectric Breakdown D1816
4 (Should be <Limit) (Should be >Limit) (Should be >Limit)
40
3.5
35
3
30
2.5
25
2
20

kV
1.5 15
1 10
0.5 5
0 0
Jun-16

Jun-15

Jun-16

Jun-15

Actual Values
Acceptable Limits

Magna IV Engineering Serial Number: 60503 Page 3 of 3


PREPARED FOR

CARGILL
OIL FILLED EQUIPMENT INSPECTION SHEET CANF-5E006
WO# C3330-10 TAG # 6 OCB1 DATE June 7, 2016
SITE CARGILL TERMINAL TEST BY JMP
AREA MAIN SUB STANDARD MAINTENANCE APPROVED BY

NAMEPLATE DATA
EQUIPMENT OCB KVA # OF TAPS N/A
MANUF. GE PRI VOLTS 72KV TAP FOUND/LEFT /
TYPE WSO SEC VOLTS %IMPED N/A
SO# 60503 AMPS 1200 WEIGHT
YEAR 1967 CAPACITY LTRS 575 GALS TEMP RISE N/A
OIL TYPE MINERAL SYSTEM BREATHING
DATE OF LAST OIL CHANGE (IF KNOWN) UNKNOWN

PRE-SAMPLING CHECKLIST
CRITERIA YES NO CRITERIA YES NO COMMENTS
ADEQUATE CLEARANCE PCB CONTAMINATED < 0.5 PPM
TANK PRESSURE (Min: -1 Psi (-6.89 kPa)) LOW OIL LEVEL (GAUGE @ LOW) NO GAUGE

INSPECTIONS
DESCRIPTION YES NO DESCRIPTION OK FAIL COMMENTS
BREATHERS SILICA DESICANT CONDITION NOT USED
HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION SOME CHIPS
LV BUSHINGS ACCESSIBLE LV BUSHING CONDITION N/A
RADIATORS INSTALLED RADIATOR CONDITION N/A
CONSERVATOR TANK OIL LEAKS (WHERE) OK
GROUNDING (2 LOCATIONS) CORROSION / RUST ACCUMULATION PAINT IS POOR
PHYSICAL DAMAGE DIRT ACCUMULATION NONE VISIBLE
NITROGEN ADDED
RELIEF VALVE INSTALLED

GAUGE DOCUMENTATION
GAUGE READING DRAGHAND RESET GAUGE READING
OIL TEMP 26 °C YES / NO OIL LEVEL SEE DIAGRAM AT RIGHT
WINDING TEMP YES / NO PRESSURE PSI KPA

SAMPLE DATA
SAMPLE COLOR SAMPLE POINT BOTTOM VALVE
STRAW WHITE ORANGE BLACK SEDIMENT YES / NO
STRAW YELLOW REDDISH ORANGE OTHER: AMB. TEMP 23.0 °C
LEMON YELLOW BROWN HUMIDITY 78 %
Sampler: JMP Syringe #: DS 901 PO# for Sampling Lab: 1006975
Tests Required (Internal Purposes Only) REPORT RUSH: NO
DGA D3612C Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:
Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation)

Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP

Acid Number D974 Power Factor 100°C D924 Viscosity D88

Color/Visual D1500, D1524 Specific Gravity D1298 Other:


Dielectric 2.5mm D877 PCB

6 OCB1 Oil Filled Equipment Inspection Page 1 of 1

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