SERVICE IMPACT

HESS
S P E C I A LT Y C H E M I C A L & W E L L
S T I M U L AT I O N
June 2022
 01 O U R J O U R N E Y

02 C O N T R A C T & T R A C K R E C O R D S

03 V A L U E O F S E R V I C E S

E N G I N E E R I N G S T U D Y &
04 L A B R E S E A R C H S

Table of Content 05 R E S T O R E T E C H N O L O G Y

D E F E N D T E C H N O L O G Y
06
Service Impact Introduction 07 B O O S T T E C H N O L O G Y

08 P R O D U C T C O N V E Y A N C E

09 C H E M I C A L B O O K

10 C A S E S T U D Y
 01 OUR JOURNEY

Deleum Head Office

Blending Facility
Kemaman
1 IN-HOUSE TECHNOLOGY &
DEVELOPMENT CENTRE

Bangsar, Kuala Lumpur

Research & Development

Facility
Bangsar, Kuala Lumpur

Asian Su p p ly B ase
Labuan 2 >200 WELLS/LINES
T R EAT ED GL OB AL

START-OF 2000 W ITH IN-HOUSE RESEARCH

Indonesia Operation

AND
Jakarta

BESPOKE FORMULATION THAT

3 ONE STOP SOLUTION
CENTRE

N OW BIRT H T O PR ODU C TION ENH AN C EM EN T SEGMENT PART OF D E L E U M OILF IELD

SERVICES.

MAJORITY IN-HOUSE ELEMENTS AND PROVEN TRACK RECORD. DELEUM STRIVES

TO INCENTIVIZE VALUE RETURN TO LOCAL AND INTERNATIONAL CLIENTS 3
 Restoring Well Production

▪ Thermochemical Wax Treatment

▪ Organic Deposit & Downhole Emulsion Treatment

RESTORE
▪ Inorganic Scale Treatment
▪ Microbial Treatment
▪ Sealant Treatment
▪ Heavy Crude Treatment
▪ Sludge + Emulsion Treatment
▪ Foam Stick Treatment

Mitigation Strategy To Curb Production Threat(s)

▪ Scale Inhibition Program

DEFEND
▪ Microbial Control
▪ Water Control
▪ Sand Control

Promoting Full Field Performance

▪ Drag Reducing Agent

BOOST
▪ Friction Reducer
▪ Performance Lubricant

4
 ENGINEERING STUDY & LAB RESEARCH
04 (Inhouse Research & Development Centre)

RESEARCH ORGANIC DEPOSIT

Extended SARA, WAT, Pour Point, Dissolution Test, Treatment program

DEVELOPMENT SCALE ISSUE

TECHNOLOGY XRD, XRF, FTIR, Water analysis, Dissolution Test, Descaling program

CENTRE MICROBIAL STUDY

Deleum inhouse technology hub for analysis
support, product development & recipe
optimization
Souring study, Incubation, Efficacy test, Deployment program
SCALE INHIBITION
Water-Scaling analysis, Simulation, Qualification, Inhibition program

DESLUDGING
Sludge characterization, Lab Pre-test, Breaker, Application

SAND CONTROL
Well Screening, Lab Pre-test, Stimpro, Coreflood, Deployment program

WATER CONTROL
Well Screening, Pre-Testing, Sand Pack, Coreflood, Deployment program

5
RESTORE TECHNOLOGY
Restoring well production
▪ Thermochemical Wax Treatment
▪ Organic Deposit & Downhole Emulsion Treatment
▪ Inorganic Scale Treatment
▪ Microbial Treatment
▪ Sealant Treatment
▪ Heavy Crude Treatment
▪ Sludge + Emulsion Treatment
▪ Foam Stick Treatment

6
 RESTORE
01 O RG A N IC D E P O S I T & E M U L S IO N T R E AT ME NT
(Micro-emulsion Treatment For Production Enhancement)

Deleum Approach
• Stable micro-emulsion chemical in tackling complex lattice organic
structure .
• Wellbore treatment of emulsion for further long term production
assurance .
• Niche treatment for Naphtenate beside conventional corrosive acid(s).
Naphtenate exist from
interaction of crude & water
which further produce solid (pix)
and stable crude emulsion
Unique Features
• Specialty micro-emulsion pack to dissolve/disperse deposit.
• Works in high or low temperature condition.
• Organic component; compatible with crude.
• No sludge induce upon reaction.
• API improvement characteristic .
• Element of wettability improvement
• Flexible usage for well stimulation, pipeline flow assurance & surface facilities.

• Stable micro-emulsion chemical (not HF)

• Slow kinetic reaction (not easily spent)
• Primary solution in tackling naphtenate deposit
• Improve API & sandface wettability
• Metallurgy friendly
Wettability Improvement
chemical & crude showing 0 deg
Reference Paper: OTC-25003, OTC-26524 7
= perfect wetting
 RESTORE
01 O RG A N IC D E P O S I T & E M U L S IO N T R E AT ME NT
(Micro-emulsion Treatment For Production Enhancement)

What is ?
• Two immiscible phases attain solubilization by addition of
surfactant/co-surfactant
• Clear fluid phase (1/4 of visible wave spectrum ~150nm)
• Thermal stable (>5 years storage)
• Reaction in aqueous solution

Why Microemulsion
• Mechanism of acid attack is governed by diffusion
• Reaction rate reduced by intro weak acid
• Environment friendly to further inhibit acidization formulation
• Capable of deep penetration in tight reservoirs
• Improve relative permeability to oil and no sludge by-reaction
• Efficacy can be demonstrated by core flood experiments

Our Support
• In-house study and modelling for formation stimulation
• Coreflood study & reverse flow to simulate economical gain
• Deployment and pre-post monitoring
 RESTORE
01 O RG A N IC D E P O S I T & E M U L S IO N T R E AT ME NT
(Micro-emulsion Treatment For Production Enhancement)

No. Client Year Problem Service Remarks

1 East 2003 Skin remedial Lab testing Boost production 125-150%
Malaysia Pumping treatment
(TE)
2 East 2005 Enhancement of low production well Lab testing Boost production 200%
Malaysia Pumping treatment
(TK)
3 East 2007 Removal of wax comingling scales in Lab testing Boost production 125-150%
Malaysia tubing. API 38 PP 15degC Pumping treatment
(SM)
4 East 2012 Wax findings Lab testing Boost production 150-900%
Malaysia Pumping treatment
(BA)
5 Cendor & 2016-2022 Complex microcrystalline wax Lab testing Boost production 50-150%
West Pumping treatment
Desaru
6 Indonesia 2017-2019 Complex wax in-tubing cleaning Lab testing Boost production 150%
(DURI) Pumping treatment
7 North 2019-2020 Napthenate dominant Lab testing Boost production 800%
Sabah Pumping treatment
(SJ)

Not limited to

9
DEFEND TECHNOLOGY
Mitigation strategy to curb production threat(s)
▪ Scale Inhibition Program
▪ Microbial Control
▪ Sand Control
▪ Water Control

10
 DEFEND
02 SAND CONTROL
(Maximised Sand Free Production)

Deleum Approach
• Surface & subsurface assessment to define most cost effective sand control technology (mechanical / chemical)

Agglomerant Agent Conglomerant Agent

• Suitable for non-existence mechanical sand control
• Encapsulated resin pills for bonding at downhole
condition
Adsorptions Untreated Treated
Agglomerated
Process

• Surface charge alteration (coating of active solution)

• Strengthen attraction between particles

Screening Lab Evaluation Qualification

▪ Candidate ▪ XRD ▪ Synthetic plug/sandpack

▪ Agglomeration ▪ Return permeabiity analysis

Market Deleum • High flash point, solvent free

• Resin base • Polymer base • 30-60% active agent – rest is carrier fluid (ISW)
• Sticky filming • Ionic charge alteration • Low injection pressure & viscosity
• Impair permeability • Improved • Activates at cloud point (50 degC)
• Deploy thru CTU • Surface bullhead • Environment friendly
• <40ft interval • Longer zone
treatment
• Permanent ductility • Adapt to downhole condition 11
 DEFEND
02 AGGLOMERANT CHEMICAL
(Aqueous Solution to Bind Sand/Fines)

S a n d T R E AT R
▪ Active chemical in controlling fines migration in wells State : Liquid
▪ Designed suitable for bottom hole temperature in excess of 300degF Color : Dark
(148degC)
▪ Chemical bind sand/ceramic proppant to holds them in place without Odour : Pungent
negatively affecting permeability of treated zone amine/ammonia
Specific : 0.99-1.15
gravity
Downhole Application pH : 5-8
▪ Pre-condition well with chemical cleaner (ie. Acid etc.) Flash Point : >100degC
▪ SandTREAT chemical mixed on fly with brine and bullhead into sand
producing zone Viscosity : <2000 cps
▪ SandTREAT concentration in treatment brine 5-7%
▪ Shut-in well for 24 hours

12
 DEFEND
02 AGGLOMERANT CHEMICAL
(Aqueous Solution to Bind Sand/Fines)

No. Client Year Problem Service Remarks

1 East 2015-2019 High sand/fine produce exceed allowable Lab testing Successful; but due to
Malaysia pptb Coreflood wrong design sand screen
Contact angle installed, surface
measurement agglomerant chemical to be
LPSA injected
UCS
SEM
2 Indonesia 2018-2019 High sand/fine produce exceed allowable Study & Lab testing
pptb

3 India 2019-2020 High sand/fine produce exceed allowable Study & lab testing
pptb
4 East 2020 Sand/fine able to pass thru desander Coagulation study Pilot/trial successful deploy
Malaysia system Bullheading
treatment

Deleum & Partner(s) Track Record

13
 DEFEND
03 CONGLOMERANT CHEMICAL
(Resin Agent In Consolidating Sand Formation)

S a n d T R E AT R
▪ Combination of Pack A + Pack B + Pack C Pack A (Proprietary Epoxy Resin)
▪ Common resin agent used with solvent and generate environment/safety Appearance : Hazy viscous
issues liquid
▪ SandTREAT promotes economical approach thru encapsulated technology &
friendly to environment Relative : 1.1
Density
Advantages & Difference Pack B (Amine)
▪ High flash point, solvent free
Appearance : Amber Liquid
▪ Environmental friendly and safe operation
▪ Lower injection viscosity Relative : 0.95
▪ Built-in spacer for regain permeability (No overflush requirement) Density
▪ 40-60% active chemical in water phase for liquid formulation Pack C (Bind)
▪ Water remains as spacer after emulsion breaks and releases curing agent to
consolidate sand Appearance : Viscous white-
yellow
Downhole Application Relative : 1.0
▪ Ratio of Pack A + Pack B + Pack C designed based on reservoir property Density
▪ Higher water phase volume creates higher permeability regain but weaker
strength
▪ Post flush only required to flush Pack A fluid out of tubing
No. Client Year Problem Service Remarks
1 East 2022 High sand/fine produce exceed allowable Lab testing On-going study
Malaysia pptb Coreflood
LPSA, UCS

14
 DEFEND
04 WAT E R CO N T RO L
(RPM)

RPM(Plug-S)
• Inverse emulsion polymer where particles
selective towards water bearing formation
• Absorb on rock and selective swelling to
control flow of formation fluid
• Indepentdent to lithology
• Thermally stable upto 350degF

Water Shut Off(Plug -N)

• Gel type to tackle sustain annulus pressure
(SAP), zone shut off for next perf plan,

Deployment Analysis
simulation for effective Stage 1 Stage 2 Stage 3
placement downhole (Screen) (Qualification) (Design)
▪ K 1-5000md ▪ Gel optimization ▪ Fluid invasion &
▪ BHT >60degC ▪ Formation study pressure simulation
▪ No cross flow between ▪ Compatibility ▪ Post flush
zones ▪ Coreflood
▪ WC 50-90%

• Selective towards water bearing formation

• Assessment of suitability deployment
• Simulation of gel placement for effective treatment
• Low risk (minimal to no damage on effective permeability)
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 DEFEND
04 WAT E R S E L E C T IV E R P M
(Polymer base chemical in tackling water issues)

Plug GEL S
▪ Selective reduction relative permeability to water with little to no effect on
oil
▪ Water based system with high shear and salinity tolerance
▪ Low concentration levels of chemicals 2-8 gpt
▪ Lithology independent
▪ Environmentally acceptable

Features
▪ Advanced latch down mechanism on formation surfaces for robust
performance
▪ Continuous water exposure expands polymer and decreased water channel
flow
▪ Hydrocarbon do not react with polymer
▪ Low molecular weight material for less restriction to hydrocarbon flow
▪ Thermal operation envelope 140degF-350degF (60-177 degC)
▪ Low risk (minimal to no damage to effective permeability of hydrocarbon State : Liquid
flow)
Color : Clear
Odour : Slight
Specific : 1.03
gravity
pH : 10-12
Viscosity : 10-25 cp
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 DEFEND
05 C RO S S L I N KE R WAT E R S H U T O F F
(Polymer crosslinker for zone shut off)

Plug GEL N4 State : Microbead

▪ Low molecular weight polyacrylamide polymer Color : White
▪ Dissolves readily in fresh water & brines
Bulk density : ~0.75 g/cm3
▪ Gelant preparation with strong phase
▪ High temperature tolerant upon cross-linked Gel time : 3 hrs @50ddegC
▪ 4% in gel system (rest TSW and additive) 1-1/2 hrs
@70degC

Features
▪ Advanced latch down mechanism on formation surfaces for robust
performance
▪ Continuous water exposure expands polymer and decreased water channel
flow
▪ Hydrocarbon do not react with polymer
▪ Low molecular weight material for less restriction to hydrocarbon flow
▪ Thermal operation envelope 140degF-350degF (60-177 degC)
▪ Low risk (minimal to no damage to effective permeability of hydrocarbon
flow)
▪ >3 years shelf life (subject to storing condition)

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 DEFEND
05 C RO S S L I N KE R WAT E R S H U T O F F
(Polymer crosslinker for zone shut off)

No. Client Problem Service Remarks

1 East High SAP at casing & packer Pumping treatment Reduction to < 100psi
Malaysia
2 East High SAP prior rig entry Pumping treatment Spot gel; sustain pressure to 100 psi
Malaysia
3 East High SAP prior rig entry Pumping treatment Kill well for plug setting, MIT & tubing cut
Malaysia

4 East High SAP prior rig entry Pumping treatment Recorded 0 psi at THP CHP SCP
Malaysia

*SAP: Sustain Annulus Pressure

Deleum & Partner(s) Track Record

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 DEFEND
06 CROSS LINKER RPM
(Gel Chemical for water coning)

Plug GEL N5 State : White granular

powder
▪ High molecular weight polyacrylamide polymer
▪ Good solubility in wide range salinity tolerance Color : White
▪ Cross-linked with metal/organic agents to form gel system Bulk density : ~0.8 g/cm3
▪ Profile control treatments in modify reservoir permeability characteristic
Gel time : 3 hrs @50ddegC
and improve injection/production profiles
1-1/2 hrs
@70degC

Features
▪ In-depth blocking of high permeability zones
▪ Sealing fractures
▪ Treatment for water coning

19
 DEFEND
06 CROSS LINKER RPM
(Gel Chemical for water coning)

No. Client Problem Service Remarks

1 East High SAP prior rig entry Pumping treatment Successful spot resin and reduce PBU rate at
Malaysia surface annulus within allowable pressure
2 West High SAP (1000 psi) due to gas Pumping treatment 29bbl injected B-annulus, reduce pressure
Malaysia migration. Gel introduced to seal 1180-930 psi; due to large casing void and
gas leak high formation injectivity could not seal off
leak
3 West High SAP (500 psi) due to poor Pumping treatment 10bbl injected PCP. Seal leak and sustain
Malaysia cement bond at casing shoe pressure <100 psi
exposing formation pressure into A-
Annulus
4 West High SAP (600 psi) due to poor Pumping treatment 10bbl injected B-annulus. Seal leak and
Malaysia cement bond at casing shoe sustain pressure <100 psi
exposing formation pressure into B-
Annulus

5 West High SAP (395 psi) due to gas Pumping treatment 1bbl injected C-annulus. Seal gas migration
Malaysia migration thru micro channeling leak to sustain 0 psi and comply to WRM
guideline

6 West High SAP (650 psi) due to gas
Malaysia migration thru micro channeling
7 West High SAP (410 psi) due to gas
Malaysia migration thru micro channeling
*SAP: Sustain Annulus Pressure
Pumping treatment 1bbl injected C-annulus. Seal gas migration
leak to sustain 0 psi; gradual pressure build-
up after 3 month. Still within WRM limit
Pumping treatment 1bbl injected C-annulus. Seal gas migration
leak to sustain 0 psi and comply to WRM
guideline 20
15 P R O D U C T C O N V E YA N C E
(Main Surface Equipment)

Mini Triplex Pump (1”) Chemical Dump Bailer

Electrical Driver Downhole Tools
1.2 MT 1,5”-2.5” chamber
0.5 bpm Customizable shoe size
3500 psi Acid rated

HP LF Pump Chemical Injection Pump

Pneumatic Pneumatic
0.12 MT 0.007 MT
0.06 bpm 0.002 bpm
6800 psi

Triplex PG Pump (4.5”) Genset 60/66 KVA /

Diesel Driver (450 BHP) Airpack
DNV skid DNV skid
Split skid (5.0 + 6.0 MT) 3.2/1.5 MT
8.0 bpm
8000 psi

Lite Hydraulic Pump(1.5”) 50bbl Mixer Tank

Hydraulic Driver (100 BHP) DNV skid
DNV skid 4.3 MT
Split skid (1.1 MT x 3)
0.9 bpm
3500 psi 21
16 CHEMICAL BOOK

W E L L S T I M U L AT I O N COMMODITY
Wax Dissolver (Thermal) SC-DWAX pH Controller MEA
Wax Dissolver (1 pack) S C - D S O LV E Biocide A SC-BIOCONT A
Descaler SC-DSCALE Biocide B SC-BIOCONT B
Surfactant Treatment S C - D S O LV E H2S Scavenger S C - O I L M AT E
API Improver S C - M U LT I F LO W Corrosion Inhibitor (OP) SC-CORCONT 400
Asphaltene Dissolver S C - D A S P H A LT Corrosion Inhibitor (GP) SC-CORCONT 500
Chelate Agent S C - D E L M AT R I X Demulsifier SC-DELMUL
Foulant Cleaner SC-ANTIFOULANT Scale Inhibitor SC-SCALECLEN
Foam Stick SC-FOAMSTIX Heavy Crude Oil Treatment S C - M U LT I F LO W
Gas Stick SC-GASSTIX Desludger SC-DSLUDGE
Treated Brine S C - D E L PA C K
S A N D & WAT E R C O N T R O L
Heavy Duty Degreaser SC-DGREASE
Conglomerate Binder S C - S A N D T R E AT A
Rig Wash (Heavy) SC-RIGCLEAN
Binder S C - S A N D T R E AT B
Rig Wash (Lite) SC-ECOCLEAN
Agglomerate Binder S C - S A N D T R E AT C
3-in-1 (O2S, CI, Biocide) SC-HYDROSAFE
RPM Polymer Gel SC-Plug S & N

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