Ag (ppm) Al (%wt) As (ppm) Bi (ppm) Ca (%wt) Cd (ppm) Co (ppm) Cr (ppm) Cu (ppm)

Oreas 622
Hasil 125 6.10 113 5.94 2.40 532 46.6 55.5
Nilai CRM 102 5.77 109 5.05 2.14 460 36.0 33.9
SD Low 92.1 4.90 92 4.39 1.9 404.8 24.3 16.2
SD High 111.9 6.64 126 5.71 2.38 515.2 47.7 51.6

Oreas 141
Hasil 2.90 852 393 2832
Nilai CRM 1.58 789 324 2453
SD Low 1.25 702 237 2159
SD High 1.91 876 411 2747

Oreas 142
Hasil 3.42 624 295 1685
Nilai CRM 1.22 584 242 1466
SD Low 0.86 470 191 1271
SD High 1.58 698 293 1661

AMIS 0019
Hasil 388
Nilai CRM 337
SD Low 232
SD High 442

AMIS 0020
Hasil 294
Nilai CRM 260
SD Low 191
SD High 329
Cu (%wt) Fe (%wt) K (%wt) Mg (%wt) Mn (%wt) Mo (ppm) Na (%wt) Ni (ppm) P (%wt) Pb (ppm)

0.577 4.71 1.99 0.640 0.072 18.8 0.729 32.36 0.043

0.486 4.31 1.72 0.562 0.060 17.4 0.729 27.90 0.033
0.462 3.557 1.33 0.439 0.051 12.51 0.567 20.04 0.021
0.510 5.063 2.11 0.685 0.069 22.29 0.891 35.76 0.045

0.96 80.2
2.28 59.0
1.41 47.6
3.15 70.4

1.37 66.1
2.99 54.3
2.42 42.9
3.56 65.7
Pb (%wt) Sb (ppm) Sn (%wt) Sn (ppm) Sr (ppm) Zn (ppm)

2.53 215.1 25.5 76

2.21 195.0 7.01 52
2.009 156.3 3.86 31
2.411 233.7 10.16 73

4091
6061
5527
6595

2802
2436
2190
2682

0.111 6041
1.094 5212
0.728 4138
1.460 6286

0.628 2645
0.698 2286
0.530 1716
0.866 2856
 Ag-Ax Ag-Ax Al-Rd Al-Rd Copy As-Ax As-Ax
Solution Label 328.068 338.289 396.152 1 396.152 188.980 193.696
nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm

BLK STD 0 0 0 0 0 0
Std 0.1 ppm 0 0 0 --
Std 0.2 ppm 0 0 0 --
Std 0.5 ppm 1 1 1 1
Std 1 ppm 1 1 1 1
Std 2 ppm 2 2 2 2
Std 5 ppm 5 5 5 5
Std 10 ppm 10 10 10 10
Std 20 ppm 20 20 20 20
Std 25 ppm 25 25 25 25
Std 50 ppm 50 50 50 50
Blank Hydrite
Std 1 ppm 1 1
Std 2 ppm 2 2
Std 5 ppm 5 5
Std 10 ppm 10 10
Std 20 ppm 20 20
Std 50 ppm -- --
Blank Si
Std 2 ppm
Std 5 ppm
Std 10 ppm
Std 20 ppm
Std 50 ppm
Blank P
Std 2 ppm
Std 5 ppm
Std 10 ppm
Std 20 ppm
Std 50 ppm
Blank MIX B
Std 0.1 ppm
Std 0.2 ppm
Std 0.5 ppm
Std 1 ppm
Std 2 ppm
Std 5 ppm
Std 10 ppm
Std 20 ppm
Blank REE
Std 0.1 ppm
 Std 0.2 ppm
Std 0.5 ppm
Std 1 ppm
Std 2 ppm
Std 5 ppm
Std 10 ppm
Std 20 ppm
Initial Calibration Verification
Continuing Calibration Blank
RINSE 0 0.0015 u Uncal 0.0000 u -0.0110 u -0.0084 u
RINSE 0 0.0001 u Uncal 0.0000 u -0.0091 u -0.0060 u
BLK 1 -0.0018 u Uncal 0 149 149

OR 60D 50X 14 8.7639 u Uncal 4 111 97

OR 460 50X 7 1.9088 u Uncal 7 151 99

OR 60D 5 4 Uncal 3.4608 o 41 38

OR 460 1 31 Uncal 6.3228 o 145 96
RINSE 0.0003 u -0.0016 u Uncal 0 -0.0031 u -0.0067 u
RINSE 0.0000 u 0.0013 u Uncal 0 -0.0050 u -0.0178 u

MET TEST/A 50X 23 5.7894 u Uncal 4 1545 1540

MET TEST/D.A 50X 7783 7694 Uncal 4 1482 1481

MET TEST/B 50X 58 26 Uncal 4 1580 1549

MET TEST/D.B 50X 28 -7.0835 u Uncal 4 1487 1439

MET TEST/C 50X 11 7 Uncal 4 1424 1415

MET TEST/D.C 50X 345 298 Uncal 4 1560 1501

MET TEST/D 50X 22 -2.1153 u Uncal 4 1398 1431

MET TEST/D.D 50X 5613 5526 Uncal 4 1454 1434

MET TEST/A 1 2 Uncal 3.8332 o 1352 1347

ME TEST/D.A 729 720 Uncal 3.8264 o 1339 1344
MET TEST/B 2 2 Uncal 4.0317 o 1429 1432
ME TEST/D.B 2 2 Uncal 4.1700 o 1457 1457
MET TEST/C 3 2 Uncal 4.1463 o 1418 1421
ME TEST/D.C 328 321 Uncal 4.2125 o 1471 1477
MET TEST/D 2 2 Uncal 4.2338 o 1401 1396
ME TEST/D.D 1 -0.1435 u Uncal 4.3231 o 1458 1458
RINSE 0 0.0024 u Uncal 0 0 0
RINSE 0 -0.0001 u Uncal 0 0 0

OR 99B 50X 133 104 Uncal 1 578 552

OR 99B 92 91 Uncal 0 29 28
RINSE 0 0 Uncal 0 -0.0044 u -0.0037 u
RINSE -0.0001 u -0.0017 u Uncal 0 -0.0084 u -0.0071 u
MPC-0015/A 50X 131 110 Uncal 0 94939 95317

MPC-0015/B 50X 98 93 Uncal 0 93161 93187

MPC-0016/A 50X 300 257 Uncal 0 20036 20037

MPC-0016/B 50X 530 489 Uncal 0 19132 19117
MPC-0015/A 75 72 Uncal 0 58492.337265488.0057
o o
MPC-0015/B 76 74 Uncal 0 57507.700664387.1460
o o
MPC-0016/A 266 263 Uncal 0 16490.545017055.4858
o o
MPC-0016/B 465 462 Uncal 0 16442.112716813.4988
o o
RINSE 0 0 Uncal 0 1 1
RINSE 0 -0.0017 u Uncal 0.0000 u 1 1
RINSE 0 -0.0041 u Uncal 0.0000 u 0 0
RINSE -0.0002 u -0.0013 u Uncal 0.0000 u 0 0

OR 99B 100X 333 250 Uncal 1 1406 1392

0015/A 100X 96 39.5765 u Uncal 0 85451 85612

0015/B 100X 99 67 Uncal 0 84132 84208

RINSE -0.0001 u 0.0005 u Uncal 0.0000 u 0 0

RINSE -0.0005 u 0.0019 u Uncal 0.0000 u 0 0.0110 u
BLK 4 ACID 0 0 Uncal 0 0 0

OREAS 622/A 5X 130 139 Uncal 6.3529 o 122 116

OREAS 622/B 5X 136 135 Uncal 6.2032 o 116 116

OREAS 141/A 5X 3 3.3918 u Uncal 9.7702 o 847 832

OREAS 141/B 5X 3 2.4962 u Uncal 9.8984 o 874 856

OREAS 142/A 5X 3 -2.9643 u Uncal 10.8186 o 640 637

OREAS 142/B 5X 3 -0.3174 u Uncal 10.7275 o 677 650

AMIS 0019/A 5X 32 23 Uncal 8.7766 o 256 253

AMIS 0019/B 5X 32 28 Uncal 8.8844 o 248 241

AMIS 0020/A 5X 25 28 Uncal 5.9538 o 257 255

AMIS 0020/B 5X 23 23 Uncal 5.5974 o 250 242

OREAS 622/A ORI 124 120 Uncal 5.98 116 113

OREAS 622/B ORI 126 120 Uncal 6.21 116 112
OREAS 141/A ORI 4 39 Uncal 9.7639 o 848 838
OREAS 141/B ORI 3 40 Uncal 10.0435 o 855 843

OREAS 142/A ORI 4 35 Uncal 10.6527 o 630 621

OREAS 142/B ORI 3 35 Uncal 10.1724 o 618 613

AMIS 0019/A ORI 32 26 Uncal 8.3043 o 219 214

AMIS 0019/B ORI 28 20 Uncal 8.0235 o 214 209
AMIS 0020/A ORI 22 21 Uncal 5.3684 o 229 224
AMIS 0020/B ORI 22 19 Uncal 5.1497 o 229 223
RINSE -0.0001 u -0.0029 u Uncal 0 0.0033 u 0
RINSE 0 -0.0008 u Uncal 0 -0.0011 u -0.0059 u
 Ca-Rd Cr-Rd
Ba-Rd Bi-Rd Ca-Rd Cd-Rd Co-Rd Cr-Rd Cu-Rd
455.403 223.061 422.673 Copy 1 228.802 230.786 276.653 Copy 1 327.395 nm
422.673 276.653
nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm ppm
nm ppm nm ppm
0 0 0 0 0 0 0 0 0
0 -- 0 -- 0 0 0 0 0
0 0.2 0 -- 0 0 0 0 0
1 0.5 1 -- 1 1 1 1 1
1 1 1 -- 1 1 1 1 1
2 2 2 2 2 2 2 2 2
5 5 5 5 5 5 5 5 5
10 10 10 10 10 10 10 10 10
20 20 20 20 20 20 20 20 20
25 25 25 25 25 25 25 25 25
50 50 50 50 50 50 50 50 50
 0 0.0162 u Uncal 0 -0.0028 u -0.0007 u 0.0006 u 0.0000 u -0.0020 u
0 0.0092 Uncal 0 0 0 0 0 0.0018 u
2 -0.4952 u Uncal 0 1 1 1 0 13

242 -27.1054 u Uncal 11 -8.2953 u 5.4479 u 56 0 93

935 44.7227 u Uncal 1 -5.4994 u 21 400 0 348

224 -1.1234 u Uncal 9.8540 o 0 8 24 0 77

844 -4.7152 u Uncal 0.6846 o -0.0515 u 13 355 0 123
0 -0.0008 u Uncal 0 -0.0027 u 0.0009 u 0 0 -0.0024 u
0 0.0094 u Uncal 0 -0.0016 u -0.0003 u 0.0015 u 0.0000 u -0.0055 u

63 39.0111 Uncal 11 -8.4901 u 22 92 0 71

154 127.003 Uncal 11 -2.2173 u 2.3816 u 145 0 45

61 -3.2808 u Uncal 10 -14.0606 u 4.4280 u 114 0 49

47 10.6992 u Uncal 10 -11.3684 u 6.0534 u 97 0 34

120.4034
60 Uncal 10 -18.9693 u 6.8343 u 94 0 53
u

77 98.4091 u Uncal 11 -19.3289 u 7.6927 u 126 0 63

59 -49.8067 u Uncal 10 -6.0938 u 12.4922 u 119 0 23

 -125.3822
161 Uncal 11 -16.0495 u 5.3429 u 119 0 64
u

40 -0.5540 u Uncal 10.0076 o 8 9 80 0 37

39 -2.5989 u Uncal 9.9821 o 7 8 80 0 34
40 -0.6849 u Uncal 10.1434 o 9 10 90 0 38
42 -1.2375 u Uncal 10.5365 o 9 10 92 0 38
44 -3.3796 u Uncal 10.5979 o 8 10 76 0 41
42 3.5702 u Uncal 10.7721 o 9 10 80 0 37
42 -0.4296 u Uncal 10.9440 o 9 10 91 0 39
43 -0.9662 u Uncal 11.1795 o 8 10 94 0 40
-0.0006 u -0.0001 u Uncal 0 -0.0033 u -0.0007 u 0.0039 u 0.0000 u -0.0018 u
-0.0014 u -0.0065 u Uncal 0 -0.0024 u -0.0053 u 0.0017 u 0.0000 u -0.0040 u
600.4708
11 Uncal 0 -1.9281 u 215 87 0 361199.2108 o
u
13 178.2443 Uncal 0 5 193 87 0 310072.3644 o
-0.0013 u 0.0122 u Uncal 0 -0.0023 u 0 -0.0014 u 0.0000 u 7
-0.0022 u -0.0063 u Uncal 0 -0.0038 u 0 -0.0039 u 0.0000 u 2
56 793.56 Uncal 0 488 24 114 0 329150.6065 o
106.7891
58 u Uncal 0 487 -5.1241 u 137 0 321603.1936 o

53 70.2660 u Uncal 0 73 0.2566 u 119 0 253798

27 65.5749 u Uncal 0 81 20.2787 u 90 0 247238
33 26.6574 Uncal 0 488 11 129 0 299551.4022 o
38 28.5055 Uncal 0 471 11 122 0 289290.4534 o
7 23.9286 Uncal 0 93 1 113 0 226123.6521 o
7 14.4681 Uncal 0 81 1 106 0 220360.7661 o
-0.0020 u -0.0074 u Uncal 0 0.0003 u -0.0029 u 0.0045 u 0.0000 u 7
-0.0022 u -0.0325 u Uncal 0 -0.0036 u -0.0011 u 0.0045 u 0.0000 u 2
-0.0024 u 0.0115 u Uncal 0 -0.0040 u 0.0018 u -0.0013 u 0.0000 u 1
-0.0023 u 0.0089 u Uncal 0 -0.0026 u -0.0020 u -0.0013 u 0.0000 u 0
286.4848
93 Uncal 1 -16.7582 u 147 123 0 286440
u

-191.3061
55 Uncal 1 423 12.4840 u 148 0 295627
u

-289.0911
87 Uncal 1 447 43 103 0 304733
u

-0.0023 u 0.0074 u Uncal 0 -0.0039 u -0.0006 u 0.0005 u 0.0000 u 0

-0.0025 u -0.0090 u Uncal 0.0000 u -0.0030 u 0.0026 u 0.0016 u 0.0000 u 0
0 0.0183 Uncal 0 -0.0037 u 0 0 0 0

1339 1.0325 u Uncal 2 566 47 63 0 5834

1595 14.2524 u Uncal 2 562 46 57 0 5703

310 359.5502 Uncal 3 5 27 119 0 2849

313 383.1391 Uncal 3 3 30 136 0 2867

545 286.2354 Uncal 3 5 34 137 0 1783

554 315.6783 Uncal 3 5 35 140 0 1824

314 172.0637 Uncal 0 66 18 259 0 425

350 153.5145 Uncal 0 66 15 261 0 433

653 68.0794 Uncal 0 26 10 355 0 330

344 64.2442 Uncal 0 25 14 340 0 321

988 13 Uncal 2.2842 o 521 44 57 0 5282

1138 6 Uncal 2.3735 o 542 46 54 0 5595.7460 o
317 392.9652 Uncal 2.5728 o 3 30 119 0 2848
314 393.6416 Uncal 2.6082 o 4 28 143 0 2817

532 295.2797 Uncal 2.5710 o 6 32 128 0 1693

523 294.1391 Uncal 2.5098 o 6 33 126 0 1677

241 143.6764 Uncal 0 62 19 238 0 389

255 141.6474 Uncal 0 61 18 232 0 386
251 58.4522 Uncal 0 24 13 320 0 292
313 54.5451 Uncal 0 24 13 313 0 297
0 0.0119 u Uncal 0 -0.0027 u -0.0017 u 0 0 0
0 -0.0085 u Uncal 0 0.0000 u -0.0008 u -0.0002 u 0.0000 u 0
 Fe-Rd Mg-Rd Mn-Rd
Fe-Rd K-Rd K-Rd Copy Li-Rd Mg-Rd Mn-Rd
259.940 Copy 1 766.491 1 766.491 610.365 383.829 Copy 1 257.610 Copy 1
259.940 383.829 257.610
nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm
nm ppm nm ppm nm ppm
0 0 0 0 0 0 0 0 0
0 -- 0 -- 0 0 0 0 0
0 -- 0 -- 0 0 0 0 0
1 -- 1 -- 1 1 1 1 1
1 1 1 -- 1 1 1 1 1
2 2 2 -- 2 2 2 2 2
5 5 5 5 5 5 5 5 5
10 10 10 10 10 10 10 10 10
20 20 20 20 20 20 20 20 20
25 25 25 25 25 25 25 25 25
50 50 50 50 50 50 50 50 50
Uncal 0.0000 u Uncal 0.0000 u Uncal 0.0031 u 0.0000 u -0.0019 u 0.0000 u
Uncal 0 Uncal 0.0000 u Uncal -0.0084 u 0.0000 u 0 0
Uncal 0 Uncal 0 Uncal 11 0 1 0

Uncal 2 Uncal 2 Uncal 6389 1 692 0

Uncal 19 Uncal 1 Uncal 7546 1 336 0

Uncal 1.8995 o Uncal 1.5385 o Uncal 6002.2309 o 0.6002 o 630 0

Uncal 15.7892 o Uncal 1.2564 o Uncal 7152.9576 o 0.7153 o 308 0
Uncal 0 Uncal 0.0000 u Uncal 0 0 0 0
Uncal 0 Uncal 0 Uncal 0 0 0 0

Uncal 4 Uncal 1 Uncal 13269 1 1435 0

Uncal 3 Uncal 1 Uncal 13220 1 1432 0

Uncal 3 Uncal 1 Uncal 12724 1 1382 0

Uncal 3 Uncal 1 Uncal 12436 1 1361 0

Uncal 3 Uncal 1 Uncal 12769 1 1402 0

Uncal 3 Uncal 1 Uncal 13464 1 1475 0

Uncal 3 Uncal 1 Uncal 13091 1 1571 0

Uncal 3 Uncal 1 Uncal 13277 1 1434 0

Uncal 2.6619 o Uncal 0.8285 o Uncal 12540.7754 o 1.2541 o 1281 0

Uncal 2.6501 o Uncal 0.8262 o Uncal 12556.0647 o 1.2556 o 1274 0
Uncal 2.8093 o Uncal 0.8750 o Uncal 12778.1187 o 1.2778 o 1316 0
Uncal 2.8853 o Uncal 0.8999 o Uncal 13154.1659 o 1.3154 o 1342 0
Uncal 2.7378 o Uncal 0.8995 o Uncal 13419.9244 o 1.3420 o 1368 0
Uncal 2.8004 o Uncal 0.9114 o Uncal 13471.7321 o 1.3472 o 1397 0
Uncal 2.9513 o Uncal 0.9250 o Uncal 13694.9621 o 1.3695 o 1414 0
Uncal 3.0048 o Uncal 0.9417 o Uncal 13947.9466 o 1.3948 o 1442 0
Uncal 0 Uncal 0 Uncal 0 0 0 0
Uncal 0 Uncal 0 Uncal 0 0 0 0

Uncal 38.6405 o Uncal 0 Uncal 2534 0 293 0

Uncal 26.9797 o Uncal 0 Uncal 2007 0 235 0

Uncal 0 Uncal 0.0000 u Uncal 0 0 0 0
Uncal 0 Uncal 0.0000 u Uncal 0.0089 u 0.0000 u -0.0003 u 0.0000 u
Uncal 6 Uncal 0.0271 u Uncal 177 0 42 0

Uncal 5 Uncal 0 Uncal 404 0 57 0

Uncal 1 Uncal 0 Uncal 373 0 53 0

Uncal 1 Uncal 0 Uncal 410 0 48 0
Uncal 4.6440 o Uncal 0 Uncal 44 0 34 0
Uncal 4.4738 o Uncal 0 Uncal 41 0 32 0
Uncal 0.7573 o Uncal 0 Uncal 216 0 44 0
Uncal 0.7491 o Uncal 0 Uncal 211 0 43 0
Uncal 0 Uncal 0.0000 u Uncal 0 0 -0.0009 u 0.0000 u
Uncal 0 Uncal 0.0000 u Uncal -0.0117 u 0.0000 u -0.0018 u 0.0000 u
Uncal 0 Uncal 0.0000 u Uncal -0.0005 u 0.0000 u -0.0021 u 0.0000 u
Uncal 0 Uncal 0.0000 u Uncal -0.0078 u 0.0000 u -0.0021 u 0.0000 u

Uncal 31 Uncal 0 Uncal 2253 0 282 0

Uncal 5 Uncal 0 Uncal 445 0 83 0

Uncal 5 Uncal -0.0104 u Uncal 426 0 40 0

Uncal 0 Uncal 0.0000 u Uncal -0.0103 u 0.0000 u -0.0020 u 0.0000 u

Uncal 0 Uncal 0.0000 u Uncal -0.0213 u 0.0000 u -0.0023 u 0.0000 u
Uncal 0 Uncal 0.0000 u Uncal 0 0 0 0

Uncal 5.1457 o Uncal 2.02 Uncal 6702 0.670 780 0.078

Uncal 5.0946 o Uncal 2.01 Uncal 6636 0.664 756 0.076

Uncal 17.6607 o Uncal 1 Uncal 5638 1 1177 0

Uncal 17.7687 o Uncal 1 Uncal 5684 1 1189 0

Uncal 20.8158 o Uncal 1 Uncal 4602 0 3591 0

Uncal 21.0058 o Uncal 1 Uncal 4658 0 3691 0

Uncal 10.4963 o Uncal 3.4762 o Uncal 8018 1 1211 0

Uncal 10.8936 o Uncal 3.5614 o Uncal 8273 1 1246 0

Uncal 7.4192 o Uncal 3 Uncal 3896 0 362 0

Uncal 7.2303 o Uncal 3 Uncal 3784 0 354 0

Uncal 4.60 Uncal 1.94 Uncal 6267.4244 o 0.627 709 0.071

Uncal 4.82 Uncal 2.04 Uncal 6531.3117 o 0.653 737 0.074
Uncal 15.6251 o Uncal 0.6568 o Uncal 5641.4916 o 0.5641 o 1150 0
Uncal 15.7703 o Uncal 0.6524 o Uncal 5646.4476 o 0.5646 o 1156 0

Uncal 17.6759 o Uncal 0.7916 o Uncal 4494 0 3404 0

Uncal 17.3858 o Uncal 0.7764 o Uncal 4360 0 3321 0

Uncal 9.3754 o Uncal 3.3278 o Uncal 7536.1401 o 0.7536 o 1136 0

Uncal 9.1262 o Uncal 3.2803 o Uncal 7519.0473 o 0.7519 o 1115 0
Uncal 6.4468 o Uncal 2.4627 o Uncal 3562 0 330 0
Uncal 6.4698 o Uncal 2.4735 o Uncal 3553 0 328 0
Uncal 0 Uncal 0 Uncal 0 0 0 0
Uncal 0 Uncal 0.0000 u Uncal 0.0136 u 0.0000 u 0 0
 Na-Rd
Mo-Rd Na-Rd Ni-Rd P-Ax Sb-Rd Se-Ax Se-Ax
202.032 589.592 Copy 1 231.604 213.618 Pb-Rd 220.353 231.146 196.026 196.026
589.592 nm ppm
nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm
nm ppm
0 0 0 0 0 0 0 0 0
0 0 -- 0 --
0 0 -- 0 0
1 1 -- 1 1
1 1 -- 1 1
2 2 -- 2 2
5 5 5 5 5
10 10 10 10 10
20 20 20 20 20
25 25 25 25 25
50 50 50 50 50

1 1 1
2 2 2
5 5 5
10 10 10
20 20 20
-- 50 --

2
5
10
20
50
 -0.0169 u Uncal 0.0000 u -0.0108 u -0.0060 u -0.0121 u 0.047 Uncal -0.0360 u
-0.0176 u Uncal 0 0 0.0002 u 0 -0.0419 u Uncal -0.0354 u
-0.5195 u Uncal 0 1 1 6 3.9719 Uncal -4.3648 u

-156.8711
-70.3956 u Uncal 1 5.0958 u 479 98 41.4217 u Uncal
u

-120.3654
-77.3135 u Uncal 0 11.3812 u 2079 80 -12.4257 u Uncal u

1 Uncal 0 7 396 19 1.4507 u Uncal -5.1851 u

22 Uncal 0 62 1799 69 22.9821 Uncal -7.9126 u
-0.0232 u Uncal 0 -0.0138 u 0 0 0.0111 u Uncal -0.0339 u
-0.0205 u Uncal 0 -0.0199 u 0 -0.0009 u 0.0008 u Uncal -0.0421 u

-67.0677 u Uncal 0 24.7658 u 1393 46.9227 u 893.7937 Uncal -150.7987

u

-192.3832
-91.0107 u Uncal 0 -33.5226 u 1453 54 813.703 Uncal
u

-174.5781
-100.4480 u Uncal 0 -28.0726 u 1246 6.3471 u 917.7062 Uncal
u

-213.6917
-63.3109 u Uncal 0 -11.4853 u 1553 124 991.9241 Uncal u

-137.6637
-94.1726 u Uncal 0 -13.6376 u 1288 91 573.6195 Uncal
u

-191.9008
-98.4587 u Uncal 0 54 1314 96 964.8152 Uncal u

-173.4222
-97.9514 u Uncal 0 -8.7656 u 1253 -4.4905 u 987.1712 Uncal
u
 -159.5114
-72.7768 u Uncal 0 -23.9895 u 1663 55 685.129 Uncal
u

8 Uncal 0 15 1074 7 882.0054 Uncal -0.8928 u

8 Uncal 0 16 1083 10 876.3619 Uncal 0.3213 u
9 Uncal 0 16 1099 11 877.4104 Uncal 0.7018
9 Uncal 0 21 1155 51 903.2528 Uncal 1.4743 u
6 Uncal 0 15 1136 13 865.5255 Uncal 1.5009 u
7 Uncal 0 15 1159 9 856.4583 Uncal 1.9922
9 Uncal 0 16 1158 9 1011.6192 Uncal -0.0045 u
8 Uncal 0 17 1182 12 1045.3456 Uncal 0.9657
-0.0154 u Uncal 0 -0.0110 u 0 -0.0049 u 0.0091 u Uncal -0.0297 u
-0.0190 u Uncal 0 -0.0100 u 0 0.0049 u 0.0176 Uncal -0.0286 u

-89.7722 u Uncal 0 -24.1147 u 4097 894 340.6937 Uncal 185.5282

-0.6186 u Uncal 0 43 1755 728 40.6763 Uncal 299.8181

-0.0181 u Uncal 0 -0.0092 u 0 0 0.0239 u Uncal -0.0210 u
-0.0190 u Uncal 0.0000 u -0.0097 u 0 0 0.0299 Uncal -0.0116 u
-62.0828 u Uncal 0 -83.8635 u 3524 253 2572.7682 Uncal 368.9277

-83.4844 u Uncal 0 -27.5646 u 4015 117.7526 u 2383.5455 Uncal 83.356

-77.4806 u Uncal 0 -95.0214 u 2866 170 1455.2814 Uncal 74.0739

-65.3734 u Uncal 0 -64.5686 u 2933 114 1412.0719 Uncal 76.7477
16 Uncal 0 10 1801 135 2230.3556 Uncal 141.0532
17 Uncal 0 11 1876 135 2147.9411 Uncal 157.1795
19 Uncal 0 1 1497 40 1470.2935 Uncal 202.2181
20 Uncal 0 3 1548 39 1465.9874 Uncal 209.5393
-0.0188 u Uncal 0 -0.0043 u 0 0.0079 u 0.06 Uncal -0.0199 u
-0.0160 u Uncal 0.0000 u -0.0144 u 0 0.0064 u 0.0969 Uncal -0.0306 u
-0.0202 u Uncal 0.0000 u -0.0157 u 0 0.0037 u 0.0443 Uncal -0.0305 u
-0.0216 u Uncal 0.0000 u -0.0088 u 0 0.0110 u 0.0015 u Uncal -0.0315 u

-148.6674 u Uncal 1 -40.6467 u 3263 1010 5.4665 u Uncal 41.1877

-164.5353
-155.7688 u Uncal 1 -8.4427 u 3611 246 1924.6997 Uncal
u

-216.6425
-177.8429 u Uncal 1 -77.2076 u 3017 296 2432.7699 Uncal
u

-0.0220 u Uncal 0.0000 u -0.0050 u -0.0088 u 0.0029 u 0.0283 u Uncal -0.0384 u

-0.0254 u Uncal 0.0000 u -0.0103 u 0.0037 u -0.0052 u 0.0471 Uncal -0.0426 u
-0.0219 u Uncal 0 -0.0040 u 0 0 0.034 Uncal -0.0337 u

3.3 Uncal 0.72 32 465 27872 189.8231 Uncal -16.3850 u

 8.7 Uncal 0.73 32 487 26922 220.4814 Uncal -15.9116 u

-7.2806 u Uncal 0 58 237 109 36.4854 Uncal -20.1810 u

-6.5198 u Uncal 0 64 362 85 46.1659 u Uncal -19.7571 u

-5.8748 u Uncal 0 59 373 69 28.1882 Uncal -19.4082 u

-7.3492 u Uncal 0 63 524 85 24.4141 Uncal -15.5174 u

-6.9235 u Uncal 0 41 571 759 586.2316 Uncal -24.6785 u

-6.9932 u Uncal 0 49 574 784 626.3619 Uncal -20.0723 u

-9.4901 u Uncal 0 34 425 704 367.3087 Uncal -13.3244 u

-7.9641 u Uncal 0 37 417 706 344.776 Uncal -21.7819 u

18.4 Uncal 0.6845 o 32 429 24963 210.7718 Uncal -0.2463 u

19.3 Uncal 0.7162 o 33 440 25694 219.5107 Uncal -0.1205 u
0.78 Uncal 0 64 450 85 55.4614 Uncal -3.6847 u
1.14 Uncal 0 64 458 75 59.6303 Uncal -2.9319 u

0.4249 Uncal 0 57 525 67 46.0611 Uncal -4.6988 u

1.3710 Uncal 0 56 464 65 52.9771 Uncal -3.3414 u

-0.2810 u Uncal 0 40 507 705 593.6388 Uncal -3.6852 u

0.2752 u Uncal 0 39 473 699 577.7663 Uncal -3.1110 u
-0.7014 u Uncal 0 33 378 634 364.5754 Uncal -1.4089 u
0.6686 u Uncal 0 33 379 634 348.0141 Uncal -0.9244 u
-0.0255 u Uncal 0.0000 u -0.0167 u 0 0 0.0123 u Uncal -0.0333 u
-0.0221 u Uncal 0.0000 u -0.0154 u 0.0082 u 0 0.0407 u Uncal -0.0291 u
 Si-Rd Sn-Rd Sn-Rd Sr-Rd Ti-Rd Ti-Rd Copy V-Rd Zn-Rd
251.432 189.925 189.925 430.544 334.941 1 334.941 292.401 Zn-Rd 213.857 334.502
nm ppm
nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm nm ppm

0 0 0 0 0 0 0 0 0
0 0 0 0 0 0
0 0 0 0 0 0
1 1 1 1 1 1
1 1 1 1 1 1
2 2 2 2 2 2
5 5 5 5 5 5
10 10 10 10 10 10
20 20 20 20 20 20
25 25 25 25 25 25
50 50 50 50 50 50

1 1
2 2
5 5
10 10
20 20
50 --

2
5
10
20
50
 0 Uncal 0.048 0 0 0 -0.0040 u -0.0008 u Uncal
0 Uncal 0.0094 0 0 0 0 0.0006 u Uncal
11 Uncal 4.6815 1 15 0 1 2 Uncal

325 Uncal 166.0379 u 249 1812 0 75 69 Uncal

3990 Uncal 115.5696 279 5440 1 285 131 Uncal

353 Uncal 7.9001 242 1673 0 68 45 Uncal

3271 Uncal 15.2367 330 5039 1 256 106 Uncal
0 Uncal 0.0609 0.0029 u 0 0 0 0.0000 u Uncal
0 Uncal 0.0304 u 0 0 0 0.0007 u -0.0021 u Uncal

620 Uncal 210.8981 78 1863 0 164 99 Uncal

1045 Uncal 418.9185 78 1738 0 152 92 Uncal

811 Uncal 336.546 95 1756 0 125 113 Uncal

1125 Uncal 212.7857 105 1634 0 127 73 Uncal

862 Uncal 266.7219 109 1596 0 143 87 Uncal

1329 Uncal 234.5102 148 1720 0 150 119 Uncal

724 Uncal 136.5806 134 1642 0 142 84 Uncal

 1393 Uncal 324.2391 175 1757 0 136 111 Uncal

494 Uncal 3.054 119 1501 0 124 62 Uncal

486 Uncal 4.2178 118 1510 0 123 62 Uncal
527 Uncal 6.3402 124 1602 0 128 66 Uncal
549 Uncal 4.899 127 1660 0 133 70 Uncal
505 Uncal 4.3482 125 1626 0 132 66 Uncal
517 Uncal 2.5244 128 1671 0 136 65 Uncal
567 Uncal 10.2269 128 1653 0 137 68 Uncal
570 Uncal 6.2543 130 1696 0 139 71 Uncal
0 Uncal 0.0523 0.0020 u 0 0 0.0027 u -0.0021 u Uncal
0 Uncal 0.03 0 0 0 -0.0018 u -0.0002 u Uncal

7359 Uncal 734.5984 107 578 0 17 2709 Uncal

6102.50 o Uncal 379.342 101 389 0 5 2255 Uncal

0 Uncal 0.0341 0 0 0 0.0031 u 0 Uncal
0 Uncal 0.0161 u 0.0019 u 0 0 0 0 Uncal
1468 Uncal 671.2431 130 152 0 -10.7186 u 120 Uncal

1669 Uncal 763.8068 108 135 0 0.1081 u 108 Uncal

679 Uncal 246.201 25.9807 u 204 0 -13.3180 u 94 Uncal

356 Uncal 391.8598 38.7615 u 188 0 -20.9590 u 116 Uncal
883 Uncal 314.0861 66 97 0 1 73 Uncal
854 Uncal 302.6885 63 91 0 0.2225 u 67 Uncal
149 Uncal 119.373 19 157 0 5 49 Uncal
150 Uncal 111.993 19 162 0 5 45 Uncal
0 Uncal 0.0206 0.0083 u 0 0 -0.0032 u -0.0017 u Uncal
0 Uncal 0.0454 0 0 0 -0.0047 u -0.0008 u Uncal
0 Uncal 0.0556 0.0040 u 0 0 0.0001 u -0.0009 u Uncal
0.06 u Uncal 0.0395 0.0030 u 0 0 -0.0016 u -0.0017 u Uncal

5942 Uncal 1188.4066 140 901 0 -0.5365 u 2489 Uncal

582 Uncal 1004.6257 134 362 0 -7.8637 u 227 Uncal

834 Uncal 524.5747 143 224 0 2.4243 u 127 Uncal

0 Uncal 0.066 0.0080 u 0.0002 u 0.0000 u -0.0017 u -0.0020 u Uncal

0 Uncal 0.0170 u 0.0051 u 0 0 -0.0020 u 0.0007 u Uncal
0.03 u Uncal 0.0439 0.0022 u 0 0 0 0 Uncal

1060 Uncal 24.8818 78 1776 0 53 114777.6328 o Uncal

1052 Uncal 26.042 82 1781 0 51 114603.1296 o Uncal

3580 Uncal 4372.4177 174 5658 1 206 4311 Uncal

3642 Uncal 4376.0804 173 5692 1 208 4248 Uncal

4191 Uncal 6623.0417 183 5689 1 208 2981 Uncal

4299 Uncal 7278.1159 180 5888 1 215 3002 Uncal

2187 Uncal 1057.6243 60 3670 0 132 6691 Uncal

2251 Uncal 1161.0018 56 3813 0 134 6886 Uncal

1594 Uncal 948.9301 68 3063 0 101 2889 Uncal

1610 Uncal 521.5921 71 3006 0 100 2838 Uncal

940 Uncal 25.9303 75 1661 0 49 80944.6653 o Uncal

983 Uncal 19.8017 78 1788 0 51 83133.3620 o Uncal
3309 Uncal 4226.2053 167 5572.3047 o 0.5572 o 203 4092 Uncal
3378 Uncal 4167.5151 168 5651.7376 o 0.5652 o 205 4090 Uncal
6304.7570
3839 Uncal 174 5464.3106 o 0.5464 o 199 2832 Uncal
o

3752 Uncal 6461.2507 168 5406 1 196 2771 Uncal

o
1982 Uncal 10779.542 59 3491 0 123 6099 Uncal
1906 Uncal 10984.033 48 3450 0 119 5984 Uncal
1382 Uncal 7234.042 64 2696 0 93 2639 Uncal
1399 Uncal 5328.793 64 2801 0 92 2652 Uncal
0 Uncal 0.0572 -0.0011 u 0 0 0 0 Uncal
0 Uncal 0.0232 0 0 0 0.0007 u 0 Uncal
 Zr-Rd
343.823
nm ppm

0
0
0
1
1
2
5
10
20
25
50
 0
0.0009 u
1

59

238

44
187
0
0

73

348

106

575

64

69

39
 626

23
20
37
23
30
27
23
24
-0.0006 u
0

114

42
0
0.0003 u
19

49

72
34
4
3
6
22
0.0011 u
0
0
0

58

49

41

-0.0004 u
0.0005 u
0

157
 159

207

211

239

246

55

54

43

38

150
155
210
213

240

233

52
47
44
37
0.0005 u
0.0025 u