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UNIVERSITI TUN HUSSEIN ONN MALAYSIA

Centre for Diploma Studies


Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

LEARNING OUTCOMES

At the end of this experiment, students should be able to:


• Understand the methods used to determine the specific gravity in the
laboratory
• Carry out the calculation processes used in determining the specific
gravity
• Identify the specific gravity (Gs) value for soil.

1.1 INTRODUCTION

The specific gravity of solid Gs is a dimensionless parameter that relates the


density of the soil particles s to the density of water w, or Gs = s /w . The
density of the soil particles s is defined as the mass in air of dry solids Ms at a
stated temperature divided by the volume of the solid Vs at the same stated
temperature, or s = Ms / Vs.

1.2 OBJECTIVES

The specific gravity (Gs) of a soil is defined as the ratio between the unit masses
of soil particles and water. Gs are useful for determining weight- volume
relationships.

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

1.3 THEORY

The specific gravity (Gs), of a material is defined as the ratio of the weight (or
mass) of a given volume of the material to the weight (or mass) of an equal volume
of water. In the case of a density bottle method:

A sample of pre-dried soil is placed in a standard density bottle, of which the mass
including the stopper is m1. The combined mass of soil, bottle and stopper is m 2.
De-aired, distilled water is added and the whole vacuumed to remove air prior to
topping up and insertion of the stopper. After drying the outside of the bottle,
stopper, soil and water, m3, is determined. The bottle is then emptied, refilled with
de-aired water only, the exterior again dried and the mass of bottle, stopper and
water, m4 is recorded. Then,

mass of soil particles


𝐺𝑆 =
mass of an equal volume of water

is found from the expression:

𝑚2 − 𝑚1
𝐺𝑆 =
(𝑚4 − 𝑚1 ) − (𝑚3 − 𝑚2 )

Where,
m2 – m1 is the mass of soil sample;
m4 – m1 is the mass of water contained by the density bottle;
m3 – m2 is the mass of water occupying the volume not occupied by the
soil and thus;

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

(m4 – m1) – (m3 – m2) is the mass of water occupying a volume equal to
that of the soil particles.

Hence the specific gravity Gs of a soil is calculated as follows:


𝑤𝑆
𝐺𝑆 =
𝑤𝑆 + 𝑤𝐹𝑊 − 𝑤𝐹𝑆

Where Ws is the weight of the dry soil, WFS is the weight of the flask filled with
soil and water and WFW is the weight of the flask filled with desired water only.

1.4 APPARATUS

1. Volumetric flasks (250 or 500 ml) with stoppers, numbered and calibrated
2. Vacuum pump.
3. Balance accurate to 0.01g
4. Distilled deaired water.
5. Thermometer, ranging from 0 to 500 C, accurate to 0.50 C
6. Drying oven
7. Evaporating dish

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

Figure 1: Apparatus for Determination of Specific Gravity

1.5 PROCEDURES

1. The soil samples (pass BS sieve 2mm) were taken from the oven dried
sample with temperature of 105 -110°C. Then the samples were cooled
with the dryer.
2. Washed the volumetric flasks with stoppers, keep it dry and weigh it. (m1).
3. 5 -10g soil sample were taken from soil sample passing BS 2 mm sieve and
put in the volumetric flasks and weight it with the stopper (m2).
4. Add distilled water in volumetric flask mentioned earlier and vacuum it to
remove air in 1 hour. After that, shake that flask and add the distilled water
to fulfill the flask and let it for 1 hour.
5. Dry the surface of flask (wipe with a cloth) and weigth the flask with the
content (m3).

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

6. Take out the soil and water from the flask, wash and clean it. After that add
distilled water and let it for 1 hour. Add distilled water if the water level in the
flask is decrease. Weight the flask with water (m4).
7. Repeat the test to calculate additional values of Gs until the values of Gs are
within 2 % of each other.

Figure 2: The process

1.6 COMMON ERROR

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

According to Rollings and Rollings (1996), common laboratory error for the
determination of the specific gravity of solids Gs are as follows:

1. Imprecise weights of density bottle and its contents (e.g., the flask is not
clean).
2. Moisture on the outside of the density bottle or on the inside of its neck.
3. Meniscus not level with mark on neck of density bottle.
4. Use of tap water or other water that is not distilled or dematerialized

Incomplete removal of entrapped air from soil suspension. This is often the most
serious error and will tend to lower the computed value.

1.7 CALCULATION EXAMPLE

Example:

An in situ test to determine the unit weight of a soil was carried out using the sand
replacement method. 4.620 kg of soil were extracted from the hole which was
then refilled using 3.600 kg of loose, dry, standard sand, the sand having a dry
density of 1.570 Mg/m3.

A specific gravity determination of the soil particles, using a density bottle yielded
the following data:
Mass of density bottle + stopper, m1 = 25.001 g
Mass of density bottle + stopper + oven dried soil, m2 = 36.909g
Mass of density bottle + stopper + soil + distilled water, m3 = 62.587g
Mass of density bottle + stopper + distilled water, m4 = 55.212 g

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

The results of a water content test on a sample of the soil were as follows:
Mass of tin + wet soil m5 = 24.104g
Mass of tin + dry soil m6 = 22.103g
Mass of tin m7 = 12.302g

Given that the specific gravity of the soil particles (Gs)


mass of soil particles
𝐺𝑆 =
mass of an equal volume of water
Determine:
(a) The specific gravity of the soil particles
(b) The moisture content

Solution:
(a) The specific gravity of the soil particles;
Mass of the solid ‘a’ = 36.909 – 25.001 = 11.908g
Submerged mass of the solid, m’s = m3 – m4
= 62.587 – 55.212 = 7.375 g
Mass of water displaced by the solids is (mw)Vs = ms – m’s
=11.908 – 7.375 = 4.533 g
Specific gravity of the particles = ms / (mw) Vs = 11.908 / 4.533 = 2.627

(b) The moisture content;

w = mw = m5 – m6 = 24.104 – 22.103
ms m6 – m7 22.103 – 12.302

= 0.204 or 20.4 %

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

1.8 DATA
Data Sheet
Location : Loc. No. :
Soil description: Sample No. :
Sample type : Depth of Sample : m
Operator: Date Started :

Test no. 1 2 3 4
Bottle no.

Mass of density bottle + stopper (m1)


Mass of density bottle + stopper + oven
dried soil (m2)
Mass of density bottle + stopper + soil
+ distilled water (m3)
Mass of density bottle + stopper +
distilled water (m4 )
Mass of soil sample (m2 – m1)

Mass of water contained by the density bottle


(m4 – m1)
Mass of water occupying the volume not
occupied by the soil and thus (m3 – m2)
Mass of water occupying a volume equal to
that of the soil particles (m4 – m1) – (m3 – m2)
Gs = mass of soil particles
Mass of an equal volume of water
Gs = m2 – m1 .
(m4 – m1) – (m3 – m2)

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

APPROVED BY

Average Specific gravity = .


d 60
Cu =
d 10 =

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UNIVERSITI TUN HUSSEIN ONN MALAYSIA
Centre for Diploma Studies
Laboratory Instruction Manual

SPECIFIC GRAVITY TEST

1.9 QUESTION & DISCUSSION

1. Define specific gravity of soil.


2. What typical values of the specific gravity for soil?
3. Why do we use vacuum while determining the specific gravity of soils?
4. What is the effect of the water temperature on the determination of the
specific gravity of soils?

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