IRPC PUBLIC COMPANY LIMITED

Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 1 of 7

搅拌器单机试车方案
AGITATOR COMMISSIONING PROCEDURE

B Issue for Review 18,Oct.2016 Prawit P. Zhang Bo Liu Jian

A Issue for Squat check 15,Sept.2016 Prawit P. Zhang Bo Liu Jian

Rev. Description Date ORIG REVIEW APP.

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand
 IRPC PUBLIC COMPANY LIMITED
Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 2 of 7

CONTENTS

1. 目的 Purpose .................................................................................................................................................... 3
2. 参考 References................................................................................................................................................ 3
3. 范围和责任 Scope and responsibilities .......................................................................................................... 3
4. 90DN56 试运方案 Commissioning procedure for 90DN56 .......................................................................... 3
4.1 试车前准备工作 Pre-commissioning preparations ........................................................................... 3
4.2 试车注意事项及要点 Notes and major points of commissioning .................................................... 4
4.3 90DN56 试运 90DN56 commissioning: .............................................................................................. 4
5. 97DN11A/B 试运 97DN11A/B commissioning: ............................................................................................. 5
6. 记录表格 Recording forms ............................................................................................................................. 6
Appendix:TEST PROCEDURE FOR EKATO MECHANICAL SEALS( 90DN56 Vendor manual) ............ 7

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand
 IRPC PUBLIC COMPANY LIMITED
Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 3 of 7

1. 目的 Purpose

通过试运检验搅拌器的设计、制造、安装质量，检验其是否能够达到设计参数和工艺要求，把发现
的问题在装置开车前解决。
To inspect the quality of design, manufacture and installation of the agitators through commissioning,
whether the design parameters and process requirements can be met, and settle the issues found prior to unit
starting.

2. 参考 References

16-CMM-PRO-00-001 Pre-commissioning procedure

16-CMM-PRO-00-007 Pre-commissioning and commissioning schedule
90DN56,97DN11A/B Vendor drawings

3. 范围和责任 Scope and responsibilities

本项目的搅拌设备有 90DN56，97DN11A/B，主要参数如下：
The agitation equipments for this project are 90DN56, 97DN11A/B, which major parameters are as follows:

ITEM NO. DESCRIPTION RPM DIRECTION SEAL TEST MEDIUM

90DN56 Purge Vessel Agitator 5 Clockwise Mechanical PP powder
97DN11A/B Additive Mixer 19.7/39.3 Clockwise Mechanical

本方案适用于上述搅拌器，搅拌器的单机试车由机械工程师负责。
This procedure is applied to the agitators above, the mechanical engineers are responsible for the agitator
commissioning.

4. 90DN56 试运方案 Commissioning procedure for 90DN56

4.1 试车前准备工作 Commissioning preparations

4.1.1 配电室已投用，氮气已引入。
Electrical substation have been put into use, nitrogen has been introduced.

4.1.2 电气、仪表具备使用条件。
Service conditions of electrical, instrument have been provided.

4.1.3 试车用的工、器具以及监测器具准备齐全。
Complete preparation of tools, appliances and monitors for commissioning.

4.1.4 参加试车的有关单位人员已到现场监护。
Personnel of related organizations involving in commissioning has arrived at the site for supervision.

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand
 IRPC PUBLIC COMPANY LIMITED
Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 4 of 7
4.1.5 90D56/90DN56 及相关的工艺管线已清洗干净，吹扫气密合格。
90D56/90DN56 and related process lines have been cleaned, air tight of purge gas is qualified.

4.2 试车注意事项及要点 Notes and major points of commissioning

4.2.1 搅拌器应尽量在工作条件下试运。
The agitators shall be commissioned under operating conditions as far as possible.

4.2.2 搅拌器启动前，密封系统必须正常投用。
The sealing system must be put into proper service prior to starting the agitators.

4.2.3 运行中出现下列现象，应立即停车处理：
Shutdown and handle immediately in case of occurring follow phenomena:

4.2.3.1 电机电流急速上升。
The motor current has increased dramatically.

4.2.3.2 减速箱有异常声音或油温异常。
Abnormal noises or temperature presenting in the reducing gearboxes.

4.2.3.3 搅拌器严重刮壁。
Severe scraping of agitators.

4.3 90DN56 试运 90DN56 commissioning:

该搅拌器在反应器进行搅拌试验之前，只能进行空载试运，在 90D56 内有 PP 粉末后进行带料试运：

No-load commissioning can only be carried out for this agitator prior to the agitation test for the reactors.
After loading PP powders into 90D56, on-load commissioning will be carried out:

4.3.1 密封试运 Sealing commissioning

外观检查确认 90DN56 安装合格，紧固部位没有松动。

Appearance inspection to confirm the installation of 90DN56 is qualified, no loose in tightening positions.

检查并清理干净油路系统，如有必要，用润滑油冲洗相关部位直至合格，加入合格的润滑油。
Check and clean the oil system, flush relevant positions with lube oil until they are qualified, if necessary.
Add qualified lube oil.

按搅拌器厂家文件“密封试验方案 300096‘EKATO 机械密封的试验方案’”测试密封。

Test seals per manufacturer document of the agitator Seal Test Procedure 300096“TEST PROCEDURE FOR
EKATO MECHANICAL SEALS”.

启动润滑油泵 90DN56-P01，试运油泵，检查油压、油位是否达到要求。

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand
 IRPC PUBLIC COMPANY LIMITED
Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 5 of 7
Start the lube oil pump 90DN56-P01, commissioning and check the requirements of pressure and level are
met.

4.3.2 空载试运 No-load commissioning

手动盘车，检查搅拌器与罐壁间隙是否均匀，是否达到要求。
Hand barring and check the clearance between the agitator and wall is uniform, the requirements are met.

送电，点动，检查转向，并检查是否有异常现象。
Energizing, inching, check the rotation and normal phenomena.

启动搅拌器，运行 2-5 分钟，停车，再次检查紧固部位是否有松动，并再次紧固。

Start the agitator, running for 2-5 min, then stop, check the loose in tightening positions, and re-tighten.

启动搅拌器，运行 1.5 小时，记录数据，并检查是否达到要求。

Start the agitator, running for 1.5 h, record the data and check the requirements are met.

4.3.3 带负荷试运 On-load commissioning

在反应器进行出料试验后，脱气仓内将有粉料，可以带料试运：
After discharging test for the reactors, there are powders inside the purge columns, on-load commissioning
may be carried out.

将粉料控制到 80%左右。
Control the level of powders about 80%.

启动搅拌器再次试运。
Start the agitator and commissioning again.

注意检查粉料温度，不要使之升高到 90℃以上。
Be careful to check the powder temperature, which shall not exceed 90℃.

在进行粉料输送系统试运之前，完成该搅拌器的试运。
The commissioning of this agitator is completed prior to commissioning of powder conveying system.

5. 97DN11A/B 试运 97DN11A/B commissioning:

5.1 检查搅拌器，确认安装正确，无缺损部件。
Check the agitator, confirm it is installed properly, without any missing or damaged parts.

5.2 加油、盘车确认搅拌器正常后送电。
Add oil, barring and confirm the agitator is in normal condition before energizing.

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand
 IRPC PUBLIC COMPANY LIMITED
Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 6 of 7
5.3 点动，确认运行方向正确，并运行顺畅，空转一小时，停车。
Inching, confirm the direction of operation is correct and running smoothly, then running with no load and
stop.

6. 记录表格 Recording forms

记录：压力表 PI903511 压力（静态试验，5 分钟内<2.0bar），油温从哪测？

Recording: pressure of pressure gauge PI903511 (static test, <2.0bar within 5min.), where to measure the
temperature?

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand
 IRPC PUBLIC COMPANY LIMITED
Polypropylene Ⅲ Expansion
Project（PPE）
AGITATOR COMMISSIONING
PROCEDURE
Originator Project No.: T6601-01DD Project No : CAP-05-10-14-043-112100
Document No.: 16-CMM-PRO-00-022 REV.B Page 7 of 7

Appendix:
TEST PROCEDURE FOR EKATO MECHANICAL SEALS( 90DN56 Vendor manual)

1) Static Test Procedure

For each double- or triple-acting liquid lubricated mechanical seal a static test will be performed.
a) Pressurization of the seal chamber with a pressure overlay of 5 bar g (0.5 MPa)
b) Check of pressure loss for:
· Mechanical seals with a shaft diameter up to 160 mm the allowed pressure loss
during 5 minutes must be in a range of max. 1.0 bar
· Mechanical seals with a shaft diameter above 160 mm （90DN56 shaft diameter 260mm）
the allowed pressure loss during 5 minutes must be in a range of max. 2.0 bar.
Exception: for series ESD23 impossible

2) Dynamic Test Procedure

· Test run with atmospheric pressure and operating speed for ½ hour
· Test run with operating pressure and operating speed for 1 ½ hours
· Except for
- Operating pressure above 26 bar: 3 hours
- Seals with shaft diameter above 220 mm: 3 hours
· Check of seal liquid temperature(?) after stable conditions are reached at operating pressure
and operating speed
· Observation of leakage rate (<260ml/day) when running at operating pressure(0.3MPag) and
operating speed
3) Inspection of material certificates (product wetted parts)
4) Visual inspection
The total duration of the test procedure is approximately 2 hours (3 ½ hours).
Results are noted in a test certificate.

This Document belongs to IRPC and is confidential.

Polypropylene III Expansion Project, the Kingdom of Thailand