KBCNMU University Practical exam guidelines for students

Subject: BP306P-Physical Pharmaceutics-I

Instructions:
1. Keep your hall ticket, ID card, clean apron, and certified manual with you.
2. The practical exam will be in the pharmaceutics lab.
3. Students will have to perform experiments individually as given by the examiner.
4. Keep the record in the lab after completion of the exam and sign on the attendance
register.
5. Mobile phones are not allowed on college premises.
6. Read the experiments and questions given to you thoroughly.
7. Discussion with other students will not be allowed.
8. Keep any reading materials outside the lab.
9. Write the aim, observations or observation table, calculation (if any), graph (if any),
and result in your answer sheet.
10. Any changes will be communicated time to time.

Exam schedule:

Batch Date Day Reporting time

A 25 Jan 2024 Thursday 08:30 am

B 25 Jan 2024 Thursday 12:30 pm

C 24 Jan 2024 Wednesday 08:30 am

D 24 Jan 2024 Wednesday 12:30 pm

Possible Experiments
A. Determination the solubility of Benzoic acid in water by volumetric analysis at room
temperature.
B. Determination the solubility of Potassium Chloride in water at different temperature
by evaporation method.
C. To determine Critical solution temperature of Phenol-Water system.
D. To determine Surface tension of given liquid by drop number method.

*** All the students are assigned a code with their respective aim. Perform the
experiment accordingly. All practicals will be included in each batch.
Sample questions for Synopsis

Batch A & B
1. Draw a well labelled diagram of Stalagmometer.
2. Define solubility
3. Write formula of HLB calculation by saponification method.
4. Write any two limitations of Nernst's distribution law.
5. Enlist four examples of partially miscible liquids.
6. Define pH and Buffers.
7. Enlist methods of solubility analysis of saturated solutions.
8. Write equation of Freundlich and Langmuir isotherm.
9. Define Critical solution temperature.
10. Write formula of surface tension calculation by drop number method.

Batch C & D
1. Draw HLB scale.
2. Define surface tension.
3. Write Statement of Nernst's distribution law.
4. Define Acid number and saponification number.
5. Define surfactants.
6. Write about pH titration method.
7. Write Henderson Hasselbalch equation for Weak acid.
8. Enlist factors affecting the solubility of drug.
9. Write any two Applications of Nernst's distribution law.
10. Enlist methods for surface tension determination.