You are on page 1of 35

AIR

PURIFICATION
UNIT

O2

CO2 O2,
APU N2

N2

OPERATION & MAINTENANCE GUIDE

PUBLISHED BY : DEPARTMEN OF ENGINEERING


UNIVERSAL ING. L&A BOSCHI PLANTS PVT LTD
PUBLISHED VERSION: 2021.01
APPLIED FOR PLANT MODEL:
UBP-170, UB-150
About us

Established in 1985, Universal Boschi was conceived to bring the latest cryogenic technology in India for
manufacturing world-class industrial & medical gas plants. Over a period of three and half decades, we
emerged as the No.1 company staying abreast of the latest cryogenic technology innovations having supplied
over 600+ air separation oxygen and nitrogen plants worldwide. We provide turnkey projects for industrial
and medical gas systems. We are leaders in the industry for manufacturing and supplying on-site systems for
producing continuous supply of high purity gases.

Ever since its establishment, Universal Boschi onsite gas products have earned the trust of customers by dint
of their being made in compliance with European standards for quality, manufacturing, performance and
customer service. Over the years, we have built up our reputation on delivering the high-performance products
backed up with world-class customer service. Our founder is a man of foresight and great business acumen
wanted to bring the best gas plant technologies to India so we could participate in the technological progress
of the world with our home-grown innovations. With his valuable guidance we have been able to make
Universal Boschi a trusted brand.

Immediately after our establishment, Universal Boschi got collaboration from a Genoa-based Italian
company, ING. L. & A Boschi, an acclaimed world leader in manufacturing cryogenic process based high
purity gas plants. The collaboration gave us the access to world-class technology and designing enabling us to
build internationally approved gas systems.

info@universalboschi.com
PREFACE
Scope of this document is to provide a quick guide about equipment standard
operating instruction, risk involved, safety & maintenance in order to support
a safe operating environment. However, it is user responsibility to get proper
information from detailed study, training and skilled professionals to operate
with maximum safety and maintain zero hazards. This equipment is tested
and safe to run with normal parameters. Please refer to the equipment test
report.
Images and drawing are indicated for explanatory purpose only, all the
guidelines should be co-related with actual installation and application and
for clarification user must contact with relevant engineer or specialist or
OEM for clarification.

Safety Undertaking
It is the responsibility of the user to thoroughly review the instructions
contained herein and to become acquainted with the methods of operation and
maintenance suggested. The equipment is sold and supplied on the basis of
user express undertaking that you will take the steps specified in the
Book/Manual/Skilled Professional in order to ensure that the equipment sold
and supplied by us will be safe and without risk to the health of your works
when properly used.

info@universalboschi.com
CONTENTS
Sr. No. CHAPTER CHAPTER NO.
1 Introduction 1.0

2 Working Principle 1.1

3 Technical Specification 1.2

4 Installation Condition 1.3

5 Connected Equipment Description 2.0

6 Safe Operating Procedure 3.0

7 After Coller 3.1

8 Moisture Separator 3.2

9 Cascade Cooler 3.3

10 Coil Cooler (CHILLER) 3.4

11 Oil Adsorber 3.5

12 Air Purification Unit (MOLECULAR SIEVE BATTERY) 3.6

13 Automatic Regeneration Control Panel 3.7

14 Regeneration of Air purification unit 4.0

15 Regeneration Process & MSB Change over cycle 4.1

16 Check points for APU Regeneration 4.2

17 Loop Drawing Regeneration Heater Control 4.3

18 Process Skid Operational Checkpoints (Hourly) 5.0

19 Normal Stop Sequence 6.0

20 Emergency Stop 7.0

21 Long Term Shutdown 8.0

22 General Preventive Maintenance 9.0

23 Faults and Trouble shooting 9.1

24 List of Spare Parts Required for yearly maintenance 10.0

25 Adsorber Chemical Filling and Replacement 11.0

26 Safety Data Sheet for Applied Chemical 12.0

27 Test Report 13.0

28 Process Flow & Operation Parameters 14.0

29 Potential Hazards Information for Process Skid with Air 15.0


Purification Unit

30 General Symbols & Safety Indications 16.0

info@universalboschi.com
1.0 INTRODUCTION
1.1 Working Principle:
Regeneration based air purification system termed as ‘’Molecular Sieve Battery’’ have two
recyclable vessels, battery-A & battery-B. One side works at a time to purify air and the other
recycles to be ready. This cycle is called regeneration & requires change over after each 8 hours.
Hence Air Purification Unit needs moisture & hydrocarbon free air to maintain the functionality of
Molecular Sieve, that’s why multilevel separators & filters has been provided withing the process
skid. Details are as below-

Oil Adsorber M.S. Battery

Oil Adsorber

After Cooler Cascade Cooler


Drier Heater

Coil Cooler

Chilling Unit
Moisture Separator

Fig1.1 : Process Skid with Air Purification Unit*

1.2 Technical Specification: Air Purification Unit (Process Skid)

Power Requirement : 415V AC 50Hz Operating Pressure : 45 kg/cm2,

Environment Temp. Max : 45’C Application : Purification of Air.

Operating Air Flow : 1000 Nm3/hr Process Temp. Max. : 250°C

Heater Pressure Max : 0.25 bar Cycle change over time : 8hr

info@universalboschi.com
1.3 INSTALLATIOIN CONDITION

This equipment must be installed in a well-ventilated area. Maximum assembly height for
skid is 3500 mm and there should be minimum 5 mtrs. clearance from roof height so that lifting of
equipment and heat ventilation can be easy.

Process Skid designed and manufactured for indoor duty for applications where the process will be
subjected to extreme conditions for corrosive environment or harsh conditions.

Should be protected with direct contact with moisture/water.

Area should be free from Dust & heat should not be more than 40’C.

Vibration absorption technique should be applied during alignment of motor & pully there should
not be heavy vibration at installed floor from other equipment.
Foundation and Floorings

The foundation design is the end user’s responsibility. Local soil


conditions can affect the foundation design. Generally, vibration or shaking problems are less likely. As a rule of
thumb, when preparing the foundation, the mounting slab should be 8 to 10 inches thick with the overall length and
width 4 inches longer and wider on each side of the structural skid. Floor should be RCC Concrete 150 mm
thickness minimum and free from water logging.

info@universalboschi.com
2.0 Connected Equipment Description
After Cooler : To decrease the compressed air temperature and condensate the moisture.

Moisture Separator-1 : To purify compressed air by separating out the moisture, dust particles &

hydrocarbon along with water.

Cascade Cooler : Nitrogen based cooler, to decrease air temperature.

Coil cooler : Attached with Chilling unit to cool down air temperature between 5-10’C

Moisture Separator-2 : Secondary level of To purify compressed air by separating out the moisture,
dust particles & hydrocarbon along with water.

Carbon Filter(Oil Adsorber) : To adsorb hydrocarbon content from air and enhance the battery life.

Molecular Sieve Battery : Adsorpsorption of co2 from supply air.

Drier Heater : Regeneration and co2 removal from MS Battery.

Regeneration Control Panel : PID based Automatic control of Heating process.

Fig2.0: Purification and Process Skid Flow Diagram(P&ID)*

info@universalboschi.com
3.0 Safe operating Procedure

• Verify before starting supply of air pressure to the through process skid, keep open the air vent/drain
valve for gradual adjustment of pressure, cooling water should be on, chiller Should be on. Booster
outlet should not be higher that 48kg/cm2
3.1 After Cooler:

Air Flow 1000 Nm3/hr Air Temp. inlet 40-55’C ~


Air Pressure 45 kg/cm2 Cooling Water Pressure 2-3kg/cm2
Water temp inlet 25’C Cooling Water flow 3-4m3/hr ~

Cooling water should not be hard as water softener is recommended to use in water supply line

There should not be any leakage from water line or cooler tank.

3.2 Moisture separator:


Air pressure 45 kg/cm2 Air flow 1000Nm3/hr
Drain valve operating time Every 20 mins Outlet safety valve Point 51 kg/cm2

Moisture Drain

Fail to drain moisture can affect the whole process

info@universalboschi.com
3.3 Cascade Cooler:
Waste Nitrogen based cooling system which works on heat exchange process with water filled inside
and makes the compressed air cold in order to decrease the load on chiller and save energy.

Water Inlet Water Level indicator


Air pressure 45 kg/cm2 Air flow 1000Nm3/hr
Inlet Temperature 30-35’C Water level maintained 4-8 inch maximum

3.4 Pre-cooling unit (coil cooler):

Coiled tube-based cooler which is attached with 4TR refrigeration unit to control the air temperature between

6-10’C, at this temperature moisture gets removed by further separators.

Coil cooler Specification:


Air pressure 45 kg/cm2 Air outlet temperature 6-10’C
Inlet Temperature 20-25’C Water level maintained 80%

info@universalboschi.com
Refrigeration Unit:

Power Supply 415V AC, 50HZ, 3φ Refrigerant Type R407 C

Inlet Air temperature 25°C Outlet Temp. Set point 6-10 °C

Do not run chiller in following conditions

• If water is not available in tank or water temp. less than 10°c.


• If Refrigerant leakage or abnormal sound.
• Continuos trip and not achieving the cooling range.

3.5 Oil adsorber: Air pressure before entering the oil adsorber should be free from moisture,
oil adsorber doesn’t need any operational changes as it is a static equipment.

3.6 Air Purification unit (Molecular Sieve Battery)


• Make sure incoming air from chiller should be 5-10’C, moisture and contamination should be filtered & drain
out by multi stage filters.

• MSB vessels should be pressurized gradually, sudden supply of high pressure is not allowed. Before opening of
battery inlet make sure there should not be pressure in compressor pipeline. In order to reduce this risk, first
keep the battery valve open then start compressors.

• Confirm the ready status of connected equipment Column and Expander

• Bypass valves for heater air inlet top-up at inlet line should be always CLOSE, in normal condition. This valve is
provided to use only when column is isolated or exceptional regeneration is required.

• Keep monitoring pressure maximum 45 bar for the main air supply. If other side in recycle then 0.5 bar for
heater.

• Check the safety valve for main air each month, set point to blow off at 50 bar.

• Do not run the process if Chiller to battery air temp is higher than 22’C

3.7 Automatic Regeneration Control Panel


MSB regeneration can be done by Automatic/Manual process but temperature should be monitored

and switching decision can be taken according process result. For more details se…..DRAWING 4.2

To start heating process, Supply air pressure 0.25-0.5 bar inside heater then start heater power. Target temp. at

TI-1 is 120’C then stop heater, and keep cooling up to TIC1201 achieves 40’c or less

Do not run heater without air flow/pressure 0.25kg/cm2.

info@universalboschi.com
4.0 Regeneration of Air purification unit:
Air Purification unit are used purify the compressed air before supplying into the column for air separation. It has filled
with special adsorption chemical which adsorbs co2 from atmospheric air and supply only purest form of gas which
contains O2, N2 & other rare gases only. This adsorption process could be run for 8hrs and after that the chemical gets
saturated and need to regenerate to re-use. This process rotates each 8hr cycle to change one MSB to another.

MSB-A
8hrs cycle
MSB-B

N3 N4

A1
A2
A5 A6
A7

A3 A4

N1 N2

Fig: 4.0 Air Purification Unit

A1 45 kg/cm2 Air Inlet to MSB side A A3 45 kg/cm2 Air outlet from MSB side A
A2 45 kg/cm2 Air Inlet to MSB side B A4 45 kg/cm2 Air outlet from MSB side B
A5 MSB A Depressurizing/Gradual Pressurizing A6 MSB B Depressurizing/Gradual Pressurizing
A7 Depressurizing Vent A&B
N1 0.25 kg/cm2 N2 inlet to MSB A N2 0.25 kg/cm2 N2 vent out from MSB
N2 0.25 kg/cm2 N2 inlet to MSB A N4 0.25 kg/cm2 N2 vent out from MSB

4.1 Regeneration Process & MSB Change over cycle


What is regeneration of Molecular Sieve Battery?
It is a reverse flushing process in which hot air is used to escape out co2 adsorbed inside the molecular sieve, this
process includes heating and cooling sequentially.
During regeneration of MSB hot & then cold air flow can used from Waste Nitrogen or moisture free air if N2 is not
available.
Regeneration process runs continuously with-in the plant production process, one MSB runs in line and the same time
another used for regeneration.

info@universalboschi.com
4.2 Check points for APU Regeneration:
1 Check the position of Air valves, only one MSB line should be used at a time.
2 Pressurising the APU Vessel and depressurizing should be always done gradually with special
attention.
3 Must have air pressure 0.25kg/cm2 in Heater inlet line before star-up the heating.
4 Hot air inlet to the MSB should not exceed 250˚C & outlet not more than 120˚C
5 Cooling/WN2 air inlet should be 15˚C or less
2 Power input in heater panel 415V AC. Status indicator should be on.
3 WN2 inlet outlet valve should be open to exhaust the hot air
4 Start heater and monitor temp and check ampere once in a day.

Never Open the APU valves suddenly when pressure before valve is more than 1 bar or higher, it can hit the
chemical due to sudden high pressure.

info@universalboschi.com
4.3 Loop Drawing Regeneration Heater Control.

Dwg4.2: Regeneration Heater Control System

5.0 Process Skid Operational Checkpoints (Hourly)


Air Pressure Drain Temp.
Air compressor
✓ ✓ ✓
Water pressure Oil Pressure Drain
Booster Pressure & temp.
✓ ✓ ✓
Points
Drain Drain Drain
Moisture Separator ✓ ✓ ✓
Temp Vibration Noise
Chiller function ✓ ✓ ✓
Level Temp Leakage
Cooling water level & Temp. ✓ ✓ ✓
Air Pressure Temperature Leakage
Battery A/B online ✓ ✓ ✓
Wn2 pressure Temperature Ampere
Battery heater ✓ ✓ ✓

info@universalboschi.com
6.0 Normal Stop Sequence
To stop APU unit means to stop the whole process.
* Open air vent/Drain valve of main air line
* Shutdown expander by cutting air supply and hydraulic bypass valve.
* Stop heater (If Battery has heated more than 70°c then don’t stop the process in the middle, need to
complete the heating & cooling cycle by isolated regeneration by using main air)

* Stop Chiller
* Stop Booster
* Stop compressor

7.0 Emergency Stop


To stop in Emergency suddenly press red button of compressor & booster.

Air Inlet

Air outlet

Open the oil bypass lever for expander. Bypass


Cut power supply of heater.
Open the drains to Release air pressure.

8.0 Long Term Shutdown


Long term shutdown more than 3 days
Needs to close all valve of battery and drain
Fully close Wn2 gate valve connected with top column line
Release water from after cooler chiller and Cascade cooler

info@universalboschi.com
9.0 General Preventive Maintenance
Daily Weekly Quarterly Yearly
Water level check to-up Blockage cleaning in Cleaning/flushing of Cleaning of water
in cascade cooler & drain line water line circuit by descaling
chiller agent
Heater Ampere check Tight the loosen nut- Dust filter cleaning Refrigerant checking &
bolts of all flanges & top up
fittings
Cleaning to protect Cleaning of elements of Cleaning of chiller
from rusting three stage aditional
filters

Water hardness check Heater element Corrosion


resistance check Protection/Painting

Replacement of filter
element of dust filter

Replacement of
elements of three stage
aditional filters

Drain valve
replacement

Filter cleaning of
battery inlet and outlet.

Shutdown & Lockout before maintenance and repair.

info@universalboschi.com
9.1 Faults and Trouble shooting
Trouble Possible Cause

Check air pressure after booster

Air Pressure Drop after battery Drain valve leakage

Dust filter blockage

Moisture passing to adsorber

Air temperature outlet more than 40’C Chiller function

Regeneration cooling not completed

Property of chemical decreased

Rise in pressure of MSB in regeneration more Leakage from air valve


than 0.3 kg/cm2
Bypass pass open or leakage

Low air flow with pressure less than 0.25


kg/cm2
Heating Temperature going high faster than
2hrs

Heating time high Moisture content mixed with MSB, Check


moisture separator function and chiller

High regeneration air pressure

Water contents coming from battery vent Moisture drains not working, Blockage in
drain line

Chiller not operating at 6-10’C

Output PID Range setting 120’C

Panel Auto cut-off not working Relay output interlocking with contactor

10.0 List of Spare Parts Required for yearly maintenance:


Sr. No. Part Name Part Number Quantity
1 Dust Filter Element UBP130-DF 1 Nos.
2 3 mm H.P Gasket UBP-HP-3MMCG 2 Rolls
3 Pressure Guage 100 kg/cm2 UBP130-MSB-2PG 2 Nos.
4 Temp. Gauge UBP130-MSB-3TG 2 Nos.
5 Drain Ball Valve 1 ‘’ UBP130-2DV 2 Nos.
6 3 Stage Filter Element UBP130-3ADF 1 Set
7 Safety valve UBP-130-PSV50 1 Nos.

info@universalboschi.com
11. Adsorber Chemical Filling and Replacement:
Function: Each vessel of the Molecular Battery (Dryer) is filled with Molecular Sieve of 1.5 mm. Type 13-X. As the
process air passes through Molecular Sieve the Molecular Sieve will adsorb water vapor and CO2 from the air. Oil
Adsorber is filled with carbon. Here the Oil Vapor carried over from Air Compressor will be removed.

Life of these chemical is more than 8 years* in normal parameters of operation.


Factors affecting the quality of these chemical are foreign particles like moisture, oil if passed to it, overheating, over
pressure and sudden pressure.
In case of any performance abnormality observed user must check the chemical quality visually by opening it and
change with new.

11.1 Chemical Bed Making Process

Note: Fill alumina up-to the level of welded joint of dish of each vessel.

info@universalboschi.com
12. Safety Data Sheet for Applied Chemical

info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
Activated Alumina
1.Component Information-
Common Name: Activated Alumina, A-101
Chemical Name: Aluminum Hydroxide by weight 93%

2. Physical property
Appearance: Pure white free flowing balls/granules.
Odor: None.
Flash Point : N/A. This material does not give a flash
Point by conventional methods.
Stability : stable
Bulk Density: 800kg/m3
pH : 8.0 of 10% aqueous solution in water.
Vapor Pressure @250C : Not applicable
Viscosity, Brookfield: Not applicable
Solubility in Water : Non Soluble
Boiling Point : Not applicable

2.Hazards Identification-
HMIS RATING:-
Health : 1(Slight)
Flammability : 0(Minimal)
Reactivity : 0(Minimal)
Chronic : 0(Slight)

3. Potential Health Affects


Inhalation: Prolonged exposure to dust of Alumina
may cause respiratory tract irritation.
Ingestion: Not known adverse effect.
Eye Contact: Not known adverse effect.
Skin Contact: Not known adverse effect.

5. First Aid Measure


Ingestion: Seek medical attention if large
quantities of alumina balls/granules
are ingested.
Inhalation: Not applicable.
Eye Contact: No adverse effect.

6. Fire Fighting Measure


Flash Point: Non- flammable
Lower Explosion Limit: Not applicable
Upper Explosion Limit: Not Applicable
Auto Ignition Temperature: Not Applicable

7. Accidental Release Measure


Spills: No special procedure are required for clean-up of spills or leaks. Spherical shape of spilled
Pellets can create slip hazard.

info@universalboschi.com
7.1 Toxicological information
• Primary irritant effect:
• On the skin: Can cause skin irritation.
• On the eye: Can cause irritation to the eyes.
• Inhalation: Can cause upper respiratory tract irritation.
• Ingestion: Can cause irritation.

8. Handling and Storage


Store under closed and dry condition

9. Personal Protection
Use NIOSH/MSHA approved respiratory protective equipment when air borne concentration of dust exceed

acceptable criteria.

10. Disposable Consideration for Waste Alumina Balls/Granules

Dispose off according to Pollution Control Norms.

Note: Seller makes no warranty, expressed or implied, concerning the


Product or the merchantability or fitness thereof for any purpose, except that the
product conforms to contracted specification and that the product does not
infringe any valid India patent. In no event shall seller be liable for incidental
Or consequential damages, whether buyer’s claim is based on contract, breach or
warranty, negligence or otherwise

info@universalboschi.com
Activated Carbon

Section 1: Chemical Product indentification


Product Name Activated Charcoal or Activated Carbon
Chemical Name Activated Charcoal
Chemical Formula C

info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
info@universalboschi.com
13.0 Test Report

info@universalboschi.com
14.0 Process Air Flow Indication:

45kg/cm
2

7kg/cm
2 0.5kg/cm
B 2
WN2 From
column

45kg/cm2 From
Booster

6-10’C

Pipeline Colour Code:

Yellow: Waste Nitrogen

Blue : Main Air

Green : Cooling Water, Moisture Drain

14.1 Air Process Parameters

Equipment Pressure Temperature Remarks


Air Compressor to Booster 7 kg/cm2 45-50 ˚C
Booster to After Cooler 45kg/cm2 50-55˚C
After Cooler to cascade 45 kg/cm2 30- 35˚C
cooler
Cascade cooler to chiller 45 kg/cm2 20-25˚C
Chiller to MSB 45 kg/cm2 6-10˚C
MSB to Column inlet 45 kg/cm2 12-18˚C

info@universalboschi.com
15. Potential Hazards Information for Process Skid with Air Purification Unit:
Type of Risk Do not/Remarks Risk Level Spot Safety Measures before
Involved access the spots
Electrical Hazards
Do not expose to Low Electric panel, Use Electrical PPE +
conductors directly Heater vessel Grounding
Air Pressure Do not expose in Very Low Silencer Googles, Helmet
front of vent
High temperature Do not touch Very Low Heating line, Heater Handgloves 300°C
pipeline directly
Rotary moving Not to access during Very Low Chiller Fan Lockout/Tagout before
part running maintenance
Noise Do not open vent Low Exhaust Vent Ear Plug
without Ear Plug
Refrigerant/Gas Gas filling should be Very Low Chiller Compressor Safety Mask, Full PPE
done by proper tool
& special technician.

TO BE OPERATED BY TRAINED & SKILLED OPERATOR ONLY.

Declaration By OEM:
Information provided in the this manual are in order to support the user’s operational, maintenance and safety requirements, it is believed to be
acurate and best information, how ever it subject to corelate with actaul installation and engineering details.
User should make their own investigation to determine the suitability of the information for their particular purpose.
We assume no warranty & liability with respect to such information & Universal Boschi is no liable for any claim for loses or damage resulting
from its use.

info@universalboschi.com
16. General Symbols & Safety Indications:

info@universalboschi.com
*Recommended to paste these respective symbols on the equipment & introduce all the team member as per safety
requirements.

Notes :______________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
____________________________________________________________________________
_____________________________________________________

User Details: (To be filled by buyer)


Company Name: ………………………………… Plant Model: …………………………………………
Contract No: ………………………………………. Commissioned by: Er……………………………..
Commissioning Cert. Date: …………………. Auth. User Name: ………………………………….

info@universalboschi.com

You might also like