Professional Documents
Culture Documents
PURIFICATION
UNIT
O2
CO2 O2,
APU N2
N2
Established in 1985, Universal Boschi was conceived to bring the latest cryogenic technology in India for
manufacturing world-class industrial & medical gas plants. Over a period of three and half decades, we
emerged as the No.1 company staying abreast of the latest cryogenic technology innovations having supplied
over 600+ air separation oxygen and nitrogen plants worldwide. We provide turnkey projects for industrial
and medical gas systems. We are leaders in the industry for manufacturing and supplying on-site systems for
producing continuous supply of high purity gases.
Ever since its establishment, Universal Boschi onsite gas products have earned the trust of customers by dint
of their being made in compliance with European standards for quality, manufacturing, performance and
customer service. Over the years, we have built up our reputation on delivering the high-performance products
backed up with world-class customer service. Our founder is a man of foresight and great business acumen
wanted to bring the best gas plant technologies to India so we could participate in the technological progress
of the world with our home-grown innovations. With his valuable guidance we have been able to make
Universal Boschi a trusted brand.
Immediately after our establishment, Universal Boschi got collaboration from a Genoa-based Italian
company, ING. L. & A Boschi, an acclaimed world leader in manufacturing cryogenic process based high
purity gas plants. The collaboration gave us the access to world-class technology and designing enabling us to
build internationally approved gas systems.
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PREFACE
Scope of this document is to provide a quick guide about equipment standard
operating instruction, risk involved, safety & maintenance in order to support
a safe operating environment. However, it is user responsibility to get proper
information from detailed study, training and skilled professionals to operate
with maximum safety and maintain zero hazards. This equipment is tested
and safe to run with normal parameters. Please refer to the equipment test
report.
Images and drawing are indicated for explanatory purpose only, all the
guidelines should be co-related with actual installation and application and
for clarification user must contact with relevant engineer or specialist or
OEM for clarification.
Safety Undertaking
It is the responsibility of the user to thoroughly review the instructions
contained herein and to become acquainted with the methods of operation and
maintenance suggested. The equipment is sold and supplied on the basis of
user express undertaking that you will take the steps specified in the
Book/Manual/Skilled Professional in order to ensure that the equipment sold
and supplied by us will be safe and without risk to the health of your works
when properly used.
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CONTENTS
Sr. No. CHAPTER CHAPTER NO.
1 Introduction 1.0
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1.0 INTRODUCTION
1.1 Working Principle:
Regeneration based air purification system termed as ‘’Molecular Sieve Battery’’ have two
recyclable vessels, battery-A & battery-B. One side works at a time to purify air and the other
recycles to be ready. This cycle is called regeneration & requires change over after each 8 hours.
Hence Air Purification Unit needs moisture & hydrocarbon free air to maintain the functionality of
Molecular Sieve, that’s why multilevel separators & filters has been provided withing the process
skid. Details are as below-
Oil Adsorber
Coil Cooler
Chilling Unit
Moisture Separator
Heater Pressure Max : 0.25 bar Cycle change over time : 8hr
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1.3 INSTALLATIOIN CONDITION
This equipment must be installed in a well-ventilated area. Maximum assembly height for
skid is 3500 mm and there should be minimum 5 mtrs. clearance from roof height so that lifting of
equipment and heat ventilation can be easy.
Process Skid designed and manufactured for indoor duty for applications where the process will be
subjected to extreme conditions for corrosive environment or harsh conditions.
Area should be free from Dust & heat should not be more than 40’C.
Vibration absorption technique should be applied during alignment of motor & pully there should
not be heavy vibration at installed floor from other equipment.
Foundation and Floorings
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2.0 Connected Equipment Description
After Cooler : To decrease the compressed air temperature and condensate the moisture.
Moisture Separator-1 : To purify compressed air by separating out the moisture, dust particles &
Coil cooler : Attached with Chilling unit to cool down air temperature between 5-10’C
Moisture Separator-2 : Secondary level of To purify compressed air by separating out the moisture,
dust particles & hydrocarbon along with water.
Carbon Filter(Oil Adsorber) : To adsorb hydrocarbon content from air and enhance the battery life.
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3.0 Safe operating Procedure
• Verify before starting supply of air pressure to the through process skid, keep open the air vent/drain
valve for gradual adjustment of pressure, cooling water should be on, chiller Should be on. Booster
outlet should not be higher that 48kg/cm2
3.1 After Cooler:
Cooling water should not be hard as water softener is recommended to use in water supply line
There should not be any leakage from water line or cooler tank.
Moisture Drain
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3.3 Cascade Cooler:
Waste Nitrogen based cooling system which works on heat exchange process with water filled inside
and makes the compressed air cold in order to decrease the load on chiller and save energy.
Coiled tube-based cooler which is attached with 4TR refrigeration unit to control the air temperature between
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Refrigeration Unit:
3.5 Oil adsorber: Air pressure before entering the oil adsorber should be free from moisture,
oil adsorber doesn’t need any operational changes as it is a static equipment.
• MSB vessels should be pressurized gradually, sudden supply of high pressure is not allowed. Before opening of
battery inlet make sure there should not be pressure in compressor pipeline. In order to reduce this risk, first
keep the battery valve open then start compressors.
• Bypass valves for heater air inlet top-up at inlet line should be always CLOSE, in normal condition. This valve is
provided to use only when column is isolated or exceptional regeneration is required.
• Keep monitoring pressure maximum 45 bar for the main air supply. If other side in recycle then 0.5 bar for
heater.
• Check the safety valve for main air each month, set point to blow off at 50 bar.
• Do not run the process if Chiller to battery air temp is higher than 22’C
and switching decision can be taken according process result. For more details se…..DRAWING 4.2
To start heating process, Supply air pressure 0.25-0.5 bar inside heater then start heater power. Target temp. at
TI-1 is 120’C then stop heater, and keep cooling up to TIC1201 achieves 40’c or less
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4.0 Regeneration of Air purification unit:
Air Purification unit are used purify the compressed air before supplying into the column for air separation. It has filled
with special adsorption chemical which adsorbs co2 from atmospheric air and supply only purest form of gas which
contains O2, N2 & other rare gases only. This adsorption process could be run for 8hrs and after that the chemical gets
saturated and need to regenerate to re-use. This process rotates each 8hr cycle to change one MSB to another.
MSB-A
8hrs cycle
MSB-B
N3 N4
A1
A2
A5 A6
A7
A3 A4
N1 N2
A1 45 kg/cm2 Air Inlet to MSB side A A3 45 kg/cm2 Air outlet from MSB side A
A2 45 kg/cm2 Air Inlet to MSB side B A4 45 kg/cm2 Air outlet from MSB side B
A5 MSB A Depressurizing/Gradual Pressurizing A6 MSB B Depressurizing/Gradual Pressurizing
A7 Depressurizing Vent A&B
N1 0.25 kg/cm2 N2 inlet to MSB A N2 0.25 kg/cm2 N2 vent out from MSB
N2 0.25 kg/cm2 N2 inlet to MSB A N4 0.25 kg/cm2 N2 vent out from MSB
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4.2 Check points for APU Regeneration:
1 Check the position of Air valves, only one MSB line should be used at a time.
2 Pressurising the APU Vessel and depressurizing should be always done gradually with special
attention.
3 Must have air pressure 0.25kg/cm2 in Heater inlet line before star-up the heating.
4 Hot air inlet to the MSB should not exceed 250˚C & outlet not more than 120˚C
5 Cooling/WN2 air inlet should be 15˚C or less
2 Power input in heater panel 415V AC. Status indicator should be on.
3 WN2 inlet outlet valve should be open to exhaust the hot air
4 Start heater and monitor temp and check ampere once in a day.
Never Open the APU valves suddenly when pressure before valve is more than 1 bar or higher, it can hit the
chemical due to sudden high pressure.
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4.3 Loop Drawing Regeneration Heater Control.
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6.0 Normal Stop Sequence
To stop APU unit means to stop the whole process.
* Open air vent/Drain valve of main air line
* Shutdown expander by cutting air supply and hydraulic bypass valve.
* Stop heater (If Battery has heated more than 70°c then don’t stop the process in the middle, need to
complete the heating & cooling cycle by isolated regeneration by using main air)
* Stop Chiller
* Stop Booster
* Stop compressor
Air Inlet
Air outlet
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9.0 General Preventive Maintenance
Daily Weekly Quarterly Yearly
Water level check to-up Blockage cleaning in Cleaning/flushing of Cleaning of water
in cascade cooler & drain line water line circuit by descaling
chiller agent
Heater Ampere check Tight the loosen nut- Dust filter cleaning Refrigerant checking &
bolts of all flanges & top up
fittings
Cleaning to protect Cleaning of elements of Cleaning of chiller
from rusting three stage aditional
filters
Replacement of filter
element of dust filter
Replacement of
elements of three stage
aditional filters
Drain valve
replacement
Filter cleaning of
battery inlet and outlet.
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9.1 Faults and Trouble shooting
Trouble Possible Cause
Water contents coming from battery vent Moisture drains not working, Blockage in
drain line
Panel Auto cut-off not working Relay output interlocking with contactor
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11. Adsorber Chemical Filling and Replacement:
Function: Each vessel of the Molecular Battery (Dryer) is filled with Molecular Sieve of 1.5 mm. Type 13-X. As the
process air passes through Molecular Sieve the Molecular Sieve will adsorb water vapor and CO2 from the air. Oil
Adsorber is filled with carbon. Here the Oil Vapor carried over from Air Compressor will be removed.
Note: Fill alumina up-to the level of welded joint of dish of each vessel.
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12. Safety Data Sheet for Applied Chemical
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Activated Alumina
1.Component Information-
Common Name: Activated Alumina, A-101
Chemical Name: Aluminum Hydroxide by weight 93%
2. Physical property
Appearance: Pure white free flowing balls/granules.
Odor: None.
Flash Point : N/A. This material does not give a flash
Point by conventional methods.
Stability : stable
Bulk Density: 800kg/m3
pH : 8.0 of 10% aqueous solution in water.
Vapor Pressure @250C : Not applicable
Viscosity, Brookfield: Not applicable
Solubility in Water : Non Soluble
Boiling Point : Not applicable
2.Hazards Identification-
HMIS RATING:-
Health : 1(Slight)
Flammability : 0(Minimal)
Reactivity : 0(Minimal)
Chronic : 0(Slight)
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7.1 Toxicological information
• Primary irritant effect:
• On the skin: Can cause skin irritation.
• On the eye: Can cause irritation to the eyes.
• Inhalation: Can cause upper respiratory tract irritation.
• Ingestion: Can cause irritation.
9. Personal Protection
Use NIOSH/MSHA approved respiratory protective equipment when air borne concentration of dust exceed
acceptable criteria.
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Activated Carbon
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13.0 Test Report
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14.0 Process Air Flow Indication:
45kg/cm
2
7kg/cm
2 0.5kg/cm
B 2
WN2 From
column
45kg/cm2 From
Booster
6-10’C
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15. Potential Hazards Information for Process Skid with Air Purification Unit:
Type of Risk Do not/Remarks Risk Level Spot Safety Measures before
Involved access the spots
Electrical Hazards
Do not expose to Low Electric panel, Use Electrical PPE +
conductors directly Heater vessel Grounding
Air Pressure Do not expose in Very Low Silencer Googles, Helmet
front of vent
High temperature Do not touch Very Low Heating line, Heater Handgloves 300°C
pipeline directly
Rotary moving Not to access during Very Low Chiller Fan Lockout/Tagout before
part running maintenance
Noise Do not open vent Low Exhaust Vent Ear Plug
without Ear Plug
Refrigerant/Gas Gas filling should be Very Low Chiller Compressor Safety Mask, Full PPE
done by proper tool
& special technician.
Declaration By OEM:
Information provided in the this manual are in order to support the user’s operational, maintenance and safety requirements, it is believed to be
acurate and best information, how ever it subject to corelate with actaul installation and engineering details.
User should make their own investigation to determine the suitability of the information for their particular purpose.
We assume no warranty & liability with respect to such information & Universal Boschi is no liable for any claim for loses or damage resulting
from its use.
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16. General Symbols & Safety Indications:
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*Recommended to paste these respective symbols on the equipment & introduce all the team member as per safety
requirements.
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