Professional Documents
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Prof. Solomon Debbarma, sdebbarma@iitb.ac.in Phone: 8837237899 (M); 7131 (O)
Some images are taken from the internet and used for educational purposes only
What are we going to learn
❖Purpose of asphalt concrete mix design
❖Hveem mix design method
❖Marshall method of mix design
❖Specimen preparation in the laboratory
❖Importance of density and voids analysis
❖Superpave mix design method
❖Evaluation of moisture susceptibility
❖Characterization of Asphalt Concrete
❖Recycling of Asphalt Concrete
What is asphalt and asphalt concrete?
• Asphalt, also known as bitumen, is a sticky, black, highly viscous liquid or semi-solid form
of petroleum.
• It may be found in natural deposits or may be a refined product
• Asphalt concrete is a sustainable paving solution made from a mixture of aggregates,
binder, and filler
• Asphalt is the binder used in asphalt concrete pavements
Hot-Mix Asphalt (HMA) consists of two basic ingredients: aggregate and asphalt binder
Because asphalt binder and aggregates are mixed between 150 ℃ - 176 ℃
Tests on asphalt
• Test on asphalt binder is important to
determine the conventional and rheological
properties of asphalt.
• It ensures that an asphalt mix will be
capable of withstanding road conditions
(traffic and environmental conditions)
Elastic solid at low Viscous fluid at
❖ Asphalt binder tests temperatures high temperatures
➢ Penetration test
• Penetration test is the oldest asphalt test.
• Measures the hardness or softness of asphalt by
measuring the depth of penetration of standard loaded
needle in 5 s while maintaining asphalt sample
temperature at 25 ℃
• More viscous the asphalt, the less distance needle is able
to penetrate
• Hence, the penetration value for viscous asphalt is less
• AASHTO T 49 and ASTM D 5: Penetration of Bituminous
Materials
Tests on asphalt
➢ Ductility test
• The ductility test (figure on left) measures asphalt binder ductility by stretching a
standard-sized briquette of asphalt binder (figure on right) to its breaking point.
• The stretched distance in centimetres at breaking is then reported as ductility. Like
the penetration test, this test has limited use since it is empirical and conducted at
only one temperature (25° C (77° F))
• AASHTO T 51 and ASTM D 113: Ductility of Bituminous Materials
Tests on asphalt
➢ Softening point test
• The softening point is defined as the temperature at which a
bitumen sample can no longer support the weight of a 3.5-g steel
ball.
• Basically, two horizontal disks of bitumen, cast in shouldered brass
rings (Figure 1), are heated at a controlled rate in a liquid bath while
each supports a steel ball.
• The softening point is reported as the mean of the temperatures at
which the two disks soften enough to allow each ball, enveloped in
bitumen, to fall a distance of 25 mm (1.0 inch)
• AASHTO T 53 and ASTM D 36: Softening Point of Bitumen (Ring-
and-Ball Apparatus)
• This test simulates short term aged asphalt binder for physical property testing.
• Asphalt binder is exposed to elevated temperatures to simulate manufacturing and
placement aging. This test provides a quantitative measure of the volatiles lost during the
aging process.
• Take unaged asphalt binder samples in cylindrical glass bottles and place in a rotating
carriage within an oven (figure on right). The carriage rotates within the oven while the
325°F (163°C) temperature ages the samples for 85 minutes. Samples are then stored for use
in physical properties tests or the PAV.
• AASHTO T 240 and ASTM D 2872. Effect of Heat and Air on a Moving Film of Asphalt (Rolling
Thin-Film Oven Test)
Tests on asphalt
➢ Pressure Aging Vessel (PAV) test
• This test (figure on left) provides simulated long term aged asphalt binder for physical
property testing.
• Asphalt binder is exposed to heat and pressure to simulate in-service aging over a 7 to 10 year
period. Long term aged asphalt binder to be tested at intermediate and cold temperatures to
determine fatigue and low temperature cracking (Figure on right) resistance.
• The basic PAV procedure takes RTFO aged asphalt binder samples, places them in stainless
steel pans and then ages them for 20 hours in a heated vessel pressurized to 305 psi (2.10 MPa
or 20.7 atmospheres). Samples are then stored for use in physical property tests.
• AASHTO R 28: Accelerated Aging of Asphalt Binder Using a Pressurized Aging Vessel (PAV)
Tests on asphalt
➢ Bending Beam Rheometer (BBR) test
• The BBR test (see figure on top) provides a measure of
low temperature stiffness and relaxation properties of
asphalt binders.
• These parameters give an indication of an asphalt
binder’s ability to resist low temperature cracking. The
BBR is used in combination with the DTT to determine
an asphalt binder’s low temperature PG grade.
• The basic BBR test uses a small asphalt beam that is
simply supported (figure on left) and emersed in a cold
liquid bath . A load is applied to the center of the beam
and its deflection is measured against time
• Stiffness is calculated based on measured deflection and
standard beam properties and a measure of how the
asphalt binder relaxes the load induced stresses is also
measured. BBR tests are conducted on PAV aged asphalt
binder samples. The test is largely software controlled.
• AASHTO T 313: Determining the Flexural Creep Stiffness
of Asphalt Binder Using the Bending Beam Rheometer
(BBR)
Tests on asphalt
➢ Direct tension tester (DTT) test
• The DTT test (see figure above) provides a measure of low temperature stiffness and relaxation
properties of asphalt binders.
• These parameters give an indication of an asphalt binder’s ability to resist low temperature
cracking. The DTT is used in combination with the BBR to determine an asphalt binder’s low
temperature PG grade determination.
• Measures the stress and strain at failure of a specimen of asphalt binder pulled apart at a constant
rate of elongation. Test temperatures are such that the failure will be from brittle or brittle-ductile
fracture. The test is of little use at temperatures where the specimen fails by ductile failure
(stretches without breaking).
• AASHTO T 314: Determining the Fracture Properties of Asphalt Binder in Direct Tension (DT)
Tests on asphalt
➢ Dynamic Shear Rheometer (DSR) test
• The DSR (figure on left) test is used to characterize the viscous and elastic behavior of
asphalt binders at medium to high temperatures.
• This characterization is used in the Superpave PG asphalt binder specification.
• The basic DSR test uses a thin asphalt binder sample (figure on middle) sandwiched
between two circular plates. The lower plate is fixed while the upper plate oscillates
back and forth across the sample at 10 rad/sec (1.59 Hz) to create a shearing action.
• DSR tests are conducted on unaged, RTFO aged and PAV aged asphalt binder samples.
The test is largely software controlled.
Tests on asphalt
➢ Dynamic Shear Rheometer (DSR) test
The sequence and chemical structure of the monomers determine the physical
properties of the resulting polymer.
❖ Elastomers:
Polymers, which on addition to bitumen impart elasticity to bitumen, much like a rubber band,
are categorized as Elastomers. Elastomers resist deformation from applied stress by stretching
and recovering their shape quickly when stress is removed. They significantly improve flexibility
and cyclic loading properties (fatigue life) of the mixes in addition to improved durability and
strength properties of the bituminous mix.
❖ Plastomers:
Plastomers have a tough, rigid, three-dimensional network that is resistant to deformation.
Plastomers stiffen the bitumen and mixes, much like a hard plastic. Plastomers impart durability
and strength to the bituminous concrete mixes over all service temperatures but do not improve
elasticity and cyclic loading properties of the mix. All kinds of plastics fall under this category
Properties Improved by Polymers
• A sufficient increase in viscosity, prevents plastic
deformation.
• An increase in flexibility and elasticity of binder at
low temperatures to delay the crack formation
(mainly due to fatigue failure) and loss of chipping.
• High thermostability, improved homogeneity and
aging resistance, thus helping to reduce the
hardening of the binder during mixing, laying and
pavement service life.
➢ Thermoplastic
❖ Plastomers:
• Low Density Polyethylene (LDPE)
Various • Ethylene Vinyl Acetate (EVA)
❖ Elastomers:
Polymer
• Ethylene Butyl Acrylate (EBA)
Modified • Styrene Butadiene Rubber (SBR)
Bitumen • Styrene Butadiene Styrene (SBS)
(PMB) • Polyisoprene, Chloroprene
• Polybutadiene, Ethylene Ter Polymer
• Natural Rubber, Waste Tyre Rubber
➢ Thermosets
❖ Epoxy Resins
Crumb Rubber Modified Bitumen (CRMB)
❖ CRMB is Conventional Bitumen with treated Crumb
Rubber Additive at high temperature which results
in
– Incorporation of 2-4 per cent Natural Rubber into bitumen thus improves the properties of
the later substantially and rubberized bitumen is found to be an excellent binder for roads.
– Bitumen was heated to about 140°C and small amounts (1%) of kerosene was added as
viscosity modifier. To the boiling bitumen, natural rubber latex as specially preserved field
latex (about 2-4% by weight of bitumen) was added, stirred well and kept for about 2
hours for homogenization.
Benefits of NRMB:
• Increase in useful service life
• Improved resistance to cracking at low
temperature
• Better resistance to fatting up or
bleeding of bitumen under hot condition
• Improved skid resistance
• Increased fuel economy
• Better grip and cornering
• Low repairs and maintenance cost
(about 33% savings)
Requirements of PMB/CRMB/NRMB as per IS:15462-2004
❖ CRMB:
Characteristics CRMB 50 CRMB 55 CRMB 60
Viscosity, 1500C, Poise 1-3 2-6 3-9
Flash Point, min, OC , 220 220 220
Softening Point, min , 0C 40 45 47
Penetration, 0.1mm, at 250C <70 <60 <50
Elastic Recovery of half thread at 15 0C, min 50 50 50
❖ NRMB:
Characteristics NRMB 120 NRMB 70 NRMB 40
Viscosity, 1500C, Poise 1-3 2-6 3-9
Flash Point, min, OC , 220 220 220
Softening Point, min , 0C 45 50 55
Penetration, 0.1mm, at 250C 90-150 50-90 30-50
Elastic Recovery of half thread at 15 0C, min 50 40 30
Highest Daily Mean Air Temperature, C (IRC: 111)
Lowest Daily Mean Air Less than 20 C 20 to 30 C More than 30 C
Temperature, C
More than – 10 C PMB/NRMB 120 PMG/NRMB 70/ PMB/ NRMB 40/
CRMB 50 CRMB 55 CRMB 60
– 10 C or lower PMB/ NRMB 120/ PMG/ NRMB 120/ PMB/ NRMB 70/
CRMB 50 CRMB 50 CRMB 55
Asphalt Concrete Requirements
• Sufficient workability
Significance and Use
1. aggregate evaluation
2. asphalt cement evaluation
3. specimen preparation
4. Marshall stability and flow measurement
5. density and voids analysis
6. design asphalt content determination
Equipment and Materials
1. Remove premade hot mix asphalt from oven at 150 degrees Celsius.
2. Take a 1200 g sample.
3. Place the hot mix asphalt in the 101.6 mm mold with release paper on both
sides.
Procedure
4. Compact the hot mix asphalt 75 times on each side using the mechanical
compaction hammer.
5. Remove the sample from the mold with the specimen extruder.
Procedure
6. Immerse the specimen in a 60⁰C (140⁰F) water bath for 30~40 minutes.
7. Remove the specimen from the water bath, dry lightly and place it in the
breaking head.
8. Set up a strip chart to collect the data from the breaking head.
9. Load the specimen at a rate of 50.8 mm/min (2 in./min).
10. Once the maximum load is reached, record it along with the Marshall flow
deformation.
Procedure
where:
𝑚 G = specific gravity
𝑣 𝑚 m = mass of the material
𝐺 = 𝑜𝑟
𝜌 𝑣×𝜌 v = volume of the material
ρ = density of water
If any two of the three are quantities, G, m, or v, are known through testing, the
third can be easily calculated.
Volumetric Properties of Asphalt Mixture
Several different specific gravity types are determined in the volumetric analysis of
an asphalt mixture. Each specific gravity uses a particular mass (binder and/or
aggregate) and a particular volume (air, binder or aggregate or some combination).
Some specific gravity values use an aggregate volume that also includes the water-
permeable voids, while others include only the portion of the water-permeable voids
not filled with absorbed asphalt. (Because liquid water is always at a lower viscosity
than asphalt binder, the asphalt can never penetrate the aggregate voids as much as
water.)
The voids created by the aggregate The percentage of the VMA filled
structure of a compacted asphalt mixture, with effective (nonabsorbed)
expressed as a percentage of the total mix asphalt binder.
volume. VMA represents the volume of air
voids and effective (nonabsorbed) asphalt
binder
Mixture Volumetric Properties of Asphalt Mixture
❖ Percent Aggregate (Ps):
The total percentage of aggregate in the
asphalt mixture, expressed as a percentage
of the total mix mass.
The Gse is then used to calculate Gmm at each of the other binder contents. This step is
not necessary if the designer has performed Gmm testing at each trial binder
percentage
Aggregate Volumetric Properties of Asphalt Mixture
❖ Determining Gmm at other binder content
Note: AASHTO M 323, “Superpave Volumetric Mix Design,” sets the design air
voids at 4.0 percent, some agencies have lowered the target to 3.5 percent or even
3.0 percent in an effort to force more binder into the mix. A reasonable rule of
thumb says that for each 1.0 percent decrease in the air void content for a given
aggregate structure, the design binder content increases 0.3 to 0.4 percent
Volumetric Properties of Asphalt Mixture
❖ Percent air voids in compacted mixture (Pa):
Traditionally, test results and calculations are tabulated and graphed to help
determine the factors that must be used in choosing the optimum asphalt content.
Plots of results including asphalt content versus air voids, VMA, VFA, unit weight,
Marshall stability, and Marshall flow
Design Asphalt Content Determination
❖ Selection of optimum asphalt/bitumen content (OAC or OBC):
Design Asphalt Content Determination
❖ Selection of optimum asphalt/bitumen content (OAC or OBC):
National Asphalt Paving Association (NAPA), use the asphalt cement content at 4%
air voids as the design value, and then check that the other factors meet the criteria.
If the Marshall stability, Marshall flow, VMA, or VFA fall outside the allowable range,
the mix must be redesigned using an adjusted aggregate gradation or new material
sources
• When traffic loads are applied on the pavement surface, tension is developed at
the bottom of the asphalt concrete layer.
• Therefore, it is important to evaluate the tensile strength of asphalt concrete for
the design of the layer thickness.
• The indirect tensile strength test is also used for determining moisture
susceptibility
Characterization of Asphalt Concrete
❖ Indirect Tensile Strength (ITS) test procedure:
Principle: The flexural beam fatigue test is conducted by applying a repeated flexural
strain to an asphalt beam specimen in four-point flexural loading at 10 Hz and a fixed
temperature (usually 20°C) until the specimen stiffness (En) decreases to 50 percent of
the initial stiffness (Ei). By this point, micro-cracks in the specimen are expected to
have formed
Characterization of Asphalt Concrete
❖ Modulus (Stiffness) Test:
The greatest difference among the compaction procedures is the manner in which the
compaction effort is applied.
In the Marshall procedure, a slide hammer weighing 4.45 kg is dropped from a height of
0.46 m to create an impact compaction force (ASTM D1559).
For the gyratory compaction, the mixture in the mold is placed in the compaction
machine at an angle to the applied force. As the force is applied the mold is gyrated,
creating a shearing action in the mixture. Gyratory compaction devices have been
available for a long time, but their use was limited due to the lack of a mix-design
procedure based on this type of compaction. However, the Superpave mix design method
(FHWA, 1995) uses a gyratory compactor; thus, this compaction method is now common.
Purpose
• To prepare HMA specimen at desired density under actual pavement climate
and actual loading condition (traffic) or as needed for laboratory testing
Mechanical Marshall
Compaction hammer
Significance and Use
• Performance Based
• To prepare HMA specimen at desired density under actual pavement climate and
actual loading condition (traffic) or as needed for laboratory testing
angle
Mixing Compaction
temperature temperature
°F 283 - 292 261 - 270
°C 139 - 144 127 - 132
Significance and Use
• To prepare HMA specimen at desired density under actual pavement climate
and actual loading condition (traffic) or as needed for laboratory testing.
ram pressure
600 kPa
150 mm (6 in.)
diameter mold
http://www.youtube.com/watch?v=PbmgcdkNPxA
Significance and Use
- Field coring
http://www.youtube.com/watch?v=hNscKsLLQbI (7 : 25)
Significance and Use
Economic justification: comes from the utilization of the bitumen already existing in
the pavement, which reduces the requirement of expensive virgin bitumen
Recycling of Asphalt Concrete
❖ RAP Evaluation:
• Properties of both asphalt binder and aggregates in the RAP.
• Below figure is based on assumption that RAP may come from single project and
used for single project.
• However, it is a common practice to collect RAP from several projects into a single
stockpile
Recycling of Asphalt Concrete
❖ RAP Evaluation:
• Highly variable stockpile and quality control during production and
construction will be difficult at best.
• To reduce the problem with variability, the contractor should develop
“production” stockpiles by blending, crushing, and sorting into stockpiles of
different sizes.
• The properties of the aggregate in each pile are evaluated following the
procedures for virgin material. Evaluation of the binder in the RAP depends on
the target RAP content of the mix:
Involves
• Design (how pavement should be designed using reclaimed materials with the given
properties)
• Technology (the methods to reclaim and reprocess, equipment, knowhow and
quality)
Recycling of Asphalt Concrete
❖ Variability in terms of Aggregate Gradation and Binder Content:
• Lot of variability depending upon the location they come from (i.e., the project site
and/or stockpile)
• Layers they are drawn from (surfacing, bituminous base, or the granular bases)
• Method used for reclaiming (milling, ripping, breaking)
Recycling of Asphalt Concrete
❖ Overview of Reclamation and Recycling:
• Requires consideration and provision of all processes:
• Reclamation (milling, ripping, breaking)
• Handling the reclaimed materials (in-place or off site)
• Processing of reclaimed materials (to achieve the design gradation including by
adding fresh aggregates and to produce the new mix with the graded aggregate
by including by adding fresh binder) during construction.
• Construction
Different Aspects of Recycling
❖ Reclamation (hot and cold processes)
❖ Hot in-place recycling (HIR)
❖ Cold in-place recycling (CIR)
❖ Hot in-plant recycling (HIP)
❖ Cold in-plant recycling (CIP)
Hot process reclamation is applicable only in HIR, while Cold Process reclamation can
apply to all other recycling processes. In Hot Process reclamation, the existing
pavement is heated by radiation and then milled or scarified while the hot bituminous
surface is soft due to heating. The reclaimed material is invariably used in-place. In
Cold Process reclamation, the pavement material is reclaimed by Cold Milling, breaking
or ripping. In cold milling the pavement surface is milled to the required depth, the
reclaimed material is discharged into a tipper truck and stockpiled at some designated
site.
Different Aspects of Recycling
❖ Hot in-place Recycling (HIR):
In HIR, a train of equipment is used with capabilities to perform different functions such as infrared
heating of the pavement surface to soften it, milling the softened hot pavement surface, transferring
the milled materials into Pug mill mixer of the Recycling equipment through a belt conveyor, adding
fresh mix/binder/rejuvenator as per requirements of design into the pug mill, discharging the
remixed materials into integrated paving screeds for paving the re-mixed output, rolling and
compaction of the paved material.
• This process involves production and laying of hot mix materials but not with virgin
aggregates and binder but with a combination of reclaimed stockpiled aggregates
already coated with binder and additional virgin aggregate and fresh binder to meet
the requirements of the design.
• Usually, some rejuvenator is used to soften the old hardened binder in the reclaimed
aggregates. Heating the reclaimed binder coated aggregates may release
unacceptable fumes while feeding them cold directly into the pug mill may reduce
the mixing temperature.
• The hot mix production process, therefore, has to be suitably modified. In all other
respects, hot in-plant recycling is just like normal hot mix construction.
• Not more than 50% of the reclaimed material is used, though a widely accepted
percentage is only 30 and the thickness in which it can be laid is typically 100 mm.
Different Aspects of Recycling
❖ Cold in-place Recycling (CIR):
• In this process, milling and mixing are simultaneous processes accomplished by a single
equipment or a train of equipment capable of milling and conveying the milled material to be
fed to a pug mill, with parallel supply line for feeding fresh aggregates also, and separate
feeding lines to the pug mill for bitumen emulsion, and rejuvenator.
• Where foam bitumen is to be used, there has to be separate feeding line for hot bitumen and
water to produce the foam bitumen and then feed into the pug mill.
• The mixed material is discharged into the paver hopper closely following the recycling
equipment or train of equipment, then paved and compacted. This type of recycling is
considered suitable for depth upto 150 mm and the use of reclaimed material is also of the
same order (typically 30 to 50%) as in HIP.
Different Aspects of Recycling
❖ Cold in-place Recycling (CIR):
• The process involves production of the mix in a plant using either emulsion or foam bitumen
and laying and compaction in the usual manner.
• A rejuvenator is to be added in the mixing process to soften the hard binder in the reclaimed
material.
• The application range in terms of depth of recycling and use of reclaimed materials is typically
the same as for cold in-place recycling.
• Serviceability of the pavement (High severity: IRC 82: roughness and rut depth)
• The extent of surface defects (confined to surface course or lower layers)
• Structural strength (if residual life of pavement can take wheel load for next 5 yrs)
Recycling of Asphalt Concrete
❖ Recycling Options:
Recycling of Asphalt Concrete
❖ Limitations as to Depth of Recycling
• HIR: 50 mm
• HIP: 100 mm
• CIR: 75 mm
• CIP: 100 mm
In HIR or CIR 100 percent of the reclaimed materials can be used. In HIP and CIP not
more than 30 per cent of the reclaimed material should be used.
Reclamation
❖ Reclamation involves three processes viz milling, demolition, and full depth reclamation
In places where recycling is to be done in place (HIR, CIR), reclamation and recycling
are combined processes.
❖ Milling:
Milling is the control removal of an existing pavement to a desired depth, using
specially designed equipment having replaceable tungsten carbide cutting teeth
mounted on a rotor drum driven by the power supplied by the milling machine. It is the
most common way of reclaiming the bituminous pavement material. It is mostly used
following a cold process, and hence commonly known as cold milling, though milling is
done following hot process also in HIR.
Reclamation
❖ Pavement Demolition
• In Full depth reclamation (FDR) all the reclaimed materials of the pavement, with or
without fresh materials, is stabilized in-situ with suitable stabilizers to produce the
base course of the pavement to be overlaid by bituminous course(s). If economically
feasible, it is preferable to reclaim the bituminous layer and other granular or bound
layers separately to retrieve as much useful and high value bituminous materials as
possible.
• Full Depth Reclamation (FDR) is basically a cold mix recycling process in which
different types of additives such as foam bitumen, bituminous emulsions and
chemical agents such as cement, fly ash, and lime, including commercially available
cementitious stabilizers are added, mostly in-situ, and compacted to obtain an
improved base. The four main steps in this process are pulverization, introduction of
additive, mixing, compaction, and application of a surface or a wearing course. If the
in-place material is not sufficient to provide the desired depth of the treated base,
new materials may be imported and included in the processing. New aggregates can
also be added to the in-place material to obtain a particular gradation of material.
Reclamation
❖ Full Depth Reclamation (FDR)