HPSB-PHENOL-2nd

4-4-BIS-4-HYDROXYPHENYL-THIO-BIPHENYL-HPSB
PREPARATION OF HPSB-PHENOL-2nd
• CHECK VESSEL EMPTY, BOTTOM VALVE CLOSED & WORKING PROPERLY.
• BATCH OPERATION :
• CHARGE 3000 LITER RAW WATER IN REACTOR.
• CHARGE 490 KG HPSB-PHENOL-1st IN REACTOR.
• HEAT : 65°C ± 2°C (JACKET STEAM HEATING).
• CHARGE 1000 LITER RAW WATER & MAINTAIN 70°C TEMP.
• CHARGE 90 KG SODA ASH.
• ADJUST PH 8.0 ± 0.2
• CHARGE 336 KG SODA ASH AS FAST AS POSSIBLE.
• CHARGE 300 KG SODIUM HYDROSULPHITE (Na2S2O4)IN 3 HOURS & MAINTAIN
TEMPRATURE 65°C -70°C.
• FILTER:
• PRESS SETTING
• START & FINISH FILTER.
• WASH WITH HOT WATER (36000 LITER WATER + STEAM) AT 70°C-
80°C.
• CHECK PH 6.0-7.0
• WASTE WATER TO ETP.
• UNLOAD.
FLOWSHEET OF HPSB-PHEN0L-2nd
APPLICATION
• USE IN THE PREPARATION OF POLYCARBONATES,
POLYESTERS,POLYSULFONES AND POLYETHERS.
• IT IS USEFUL IN THE PREPARATION OF FILMS,FIBERS AND MOLDED
PARTS.
 PREPARATION OF LEVOCOL
• CHECK VESSEL EMPTY, BOTTOM VALVE CLOSED & WORKING PROPERLY.
• BATCH OPERATION : DISSOLUTION & MIXING.
• CHARGE 2250 LITER RAW WATER IN REACTOR-1.
• CHARGE 600 KG SODIUM CHLORATE (NaClO₃) IN REACTOR-1.
• HANDLE NaClO₃ VERY CAREFULLY BEACAUSE IT IS STRONG OXIDIZER , ANY
SPILLAGE OR RESIDUAL SOLUTION MAY CAUSE FIRE.
• STIRR IT FOR ½ HOUR.
• TAKE SAMPLE FROM REACTOR-1 AND CHECK PH(7.0-8.0).
• TRANSFER THE SOLUTION OF REACTOR-1 INTO SECOND REACTOR.
• CHARGE 150 KG POLY ETHYLENE GLYCOL (PEG) IN REACTOR-2.
• STIRR FOR ½ HOUR.
• CHECK SAMPLE.
• TRANSFER THE SOLUTION OF REACTOR-2 INTO LEVOCOL TANK.
• FILL THE CARBOYS FROM THE LEVOCOL TANK.
FLOWSHEET OF LEVOCOL