Ulangan

1
2
3
4
5
6

Berat smpel
(mg)
500
500
500
500
500
500

Pengenceran

Absorbansi

50
50
50
50
50
50

0,302
0,342
0,325
0,375
0,356
0,320
= 0,336667

Kadar CuSo4
(mg/tablet)
1,30
1,10
1,20
0,90
1,00
1,20

SD = 0,02641

RSD

100 %

100%

= 7,84455%

KV

=
= 0,0784455

AKURASI (perhitungan % recovery)

Ulangan
Berat
Pengenceran
ke
Sampel
1a
500 mg
50
1b
500 mg + 50
Cu
standar 1
ppm 1 ml
2a
500 mg
50
2b
500 mg + 50
Cu
standar 1
ppm 1 ml
3a
500 mg
50
3b
500 mg + 50
Cu
standar 1
ppm 1 ml

Serapan

Recovery

0,363
0,359

sebenarnya
0,843
0,865

0,354
0,349

0,891
0,918

356,4%
240%

0,344
0,341

0,945
0,961

378%
255,926%

337,2%
220,37%

Perhitungan sebenarnya
Y = -0,187 + 0,5207
a) 0,363 = -0,187 + 0,5207
0,187 = 0,5207 0,363
=
= 0,843
b) 0,359 = -0,187 + 0,5207
0,187 = 0,5207 0,359
=
= 0,865
c) 0,354 = 0,187 + 0,5207
0,187 = 0,5207 0,354
=
= -,891
d) 0,349 = -0,187 + 0,5207
0,187 = 0,5207 0,349
=
= 0,918
e) 0,344 = -0,187 + 0,5207
0,187 = 0,5207 0,344
=
= 0,945
f) 0,341 = -0,187 + 0,5204
0,187 = 0,5207 0,349
=
= 0,961

Perhitungan % recovery

a. % recovery =

100%

100%

= 337,2%
b. % recovery =

100%

= 220,37%
c. % recovery =
= 356,4%
d. % recovery =

100 %

= 240%
e. % recovery =
= 378%
f. % recovery =
=255,526%

100%