APPENDIKS

Siklus 1

Sebelum Distilasi

( M pikno+ sampel )−( M pikno kosong )

ρ sampel =
V pikno

52.81 gr−33.05 gr
=
24.31ml

= 0.812834 gr/ml
Setelah Distilasi

( massa gelas ukur +isi ) −( massa gelas ukurkosong )

ρ minyak =
V minyak
64.24 gr−62.414 gr
=
2 ml

= 0.913 gr/ml
M minyak = ( massa gelasukur +isi )−( massa gelasukurkosong )

= 64.24 gr – 62.414 gr

= 1.826 gr
( M pikno+ etanol )− ( M piknokosong )
ρ etanol =
V pikno
52.56 gr −33.05 gr
=
24.31 ml

= 0.80255 gr/ml

ρ etanol( gram/ml)
B =
V etanol( ml)
0,80255(gram/ml)
=
140 (ml)
= 0,005733 gram

%Volume = 990,08X2 – 1314,3X

= 990,08 (1,3332) – 1314,3(1,333)
 = 7,300361
%Volume
Y1 =
100
7,300361
=
100
= 0,0700361

Y1 x B = 0,0700361 x 0,005733 gram

= 0,000418 gram

A rendemen = Massa Kemiri Awal x 55%

= 1500 gram x 0,55
= 825 gram

X = (Y1 x B) / (-1500)
= 0,55 gram

( B x Y 1)
Effiseiensi stage =
Massakemiri awal x X

( 0,0700361 x 0,005733 ) gram

=
1500 gr am x 0,55 gram

= 5,0726 x 10-7

y 1 total x 2000 x ρ final

Yield total =
1500
0,206519 x 2000 x 0.882764 gram/ml
=
1500
= 0,243077

B x Y 1 Total
Yield Overall =
Massa Kemiri Awal x X
0,005733 gram x 0,206519
=
1500 x 0,55
= 1,435 x 10-6