QUANG PH HP TH NGUYN T - AAS

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M t sn phm :
Hng : AURORA INSTRUMENTS - Canada
Model : AI 1200
Dng phn tch cc kim loi c mt trong mu ca mi trng nc nh : nc
thi , nc ngp mn , nc sinh hot , phn tch kim loi trong mi trng t ,
trong m phm ,...
c im :
- Phn mm cho php ci t khe ph 0,2 , 0,6 v 1,2nm
- Cch t 1200 vch/mm
- Khong bc sng : 185 n 900nm
- C th iu chnh bc sng thng qua phn mm.
- Khong qut bc sng t 185 n 900nm , cho php chn la khong qut vi
chc nng Zoom.
- Hiu chnh ng nn chnh xc nh phng php t o chiu .
- n Deuterium p ng nhanh 1ms cho php hiu chnh chnh xc.
- T ng iu chnh tri
- Ngun sng : thp n vi 5 n c iu chnh t ng.
- n cathode rng cng cao.
Ph kin :
B PHN NGUYN T HO
H THNG NGN LA
- S dng c cho u t Acetylene v Nitrous Oxide
- Phn mm iu chnh kh cho php thay i t ng gia cc h thng ngn la
khc nhau.
- Bung t c ph Teflon tr vi acid v cc dung mi hu c.
- u t Titanium chng n mn cho c hn hp khng kh/acetylene v nitrous
oxide/acetylene.
- Yu cu v kh :
1. Kh kh , khng du v bi , p lc 50 - 80psi , Lu lng 10 - 12 lit/pht
2. Acetylene , tinh khit 99%, p lc 8 - 10psi , Lu lng 0,5 - 8 lit/pht
3. Nitrous oxide , tinh khit 99,5%, p lc 50 - 80psi, Lu lng 10 - 12 lit/pht
- Phn mm cho php kim sot lu lng kh.
- H thng an ton :

Kho an ton cho u t

Sensor bt / tt h thng ngn la.
T ng tt khi c s c v ngun in
H thng by cht lng v tm chn ngn la bo v khi s pht x ca tia
UV.
- Ph kin chun b mu cho h thng ngn la gm :
+ ng mao dn , tp polyurethane (di 100ft , ng knh 1/4 inch)
+ ng polyurethane dn kh Nitrous oxide (di 100ft , ng knh 5/32 inch)
+ Vng O-ring cho bung phun v u t
H THNG HO HI HYDRIDE
- H thng ho hi mu bng hi Hydrua
- Cho php xc nh cc nguyn t nh Arsen, Bimut, Antimony, thic, thu
ngn, ... v cc kim loi to hydride dng vt vi k thut to hydrid v ho hi
ngui.
- u d hp thu m bo n nh nhit trong khong t nhit phng n
1000oC
- H thng bm nhu ng c kh nng iu khin tc bm.
Ph tng cho b ho hi hydride:
- 01 ng FEP teflon , ng knh trong 0,86"
- 01 ng tygon , ng knh trong 1/8"
- 01 ng tygon , ng knh trong 1/16"
- 01 ng dn cho bm nhu ng.
B IU NHIT CHO H THNG HO HI
- B iu nhit u d thch anh dng cho b ho hi mu thay th cho b nng
nhit bng ngn la.
- iu khin nhit chnh xc , n nh nhit cao , gim nhiu , nng cao
nhy.
- Nhit iu khin : t nhit phng n 1000oC
- Bc nhy : 1oC
H THNG L GRAPHITE
- H thng l Graphite ca h thng quang ph hp thu nguyn t gip khc phc
cc vn nh hiu qu nguyn t ho km , qu trnh phn tch chm v
background cao.
- Nguyn t ho cc nguyn t iu kin ng nhit.
- Khong nhit ci t : 0 n 3000oC
- Tc gia nhit : 3800K/s
- Chng trnh nhit cho php ci t 30 thng s nhit .
Bc ci t thi gian 0,1s .
Thi gian gi c th chn la trong khong t 0s n 99s vi bc 0,1s
Ph tng cho h thng l Graphite:
- 10 ng Graphite (loi hp thu)
- 02 np bo v RF Feedthru
- 02 Quartz window

- B vng O-ring
- 04 spacer block v hp tip (96 ci , 10l n 250l)
- Tm chn bng thu tinh: cho php quan st l trong qu trnh lm vic.
- B cung cp kh Argon cho h thng l : dng lm kh mang cho l
Yu cu gm : van kh Argon v bnh kh Argon
THP N LT-0001
- Cho php gn 05 n trn cng 01 thp
- Mi bng n u c ngun in cung cp c lp
- n c chn hon ton t ng .
PHN MM IU KHIN SF-8000
- Aurora cung cp phn mm iu khin AISPEC 8.0
- Phn mm cho php iu khin hot ng ca h thng quang hc , ngn la , l
nung , b ho hi , autosampler , thu thp d liu .
PHN MM IU KHIN CHNG TRNH KH PG-0002
- Phn mm cho php iu khin lu lng kh .
- T ng thay i loi kh cho ph hp vi u t .
PHN MM BT / TT CH 2 CHM TIA DB-0002
- Dng iu khin bt / tt s dng ch 02 chm tia hay 01 chm tia.
IU CHNH NN N D2
- Module in t iu khin in p ca n .
- Cho php iu chnh nn n D2 vi thi gian tham chiu gia 2 ln o l 1ms
B BM MU T NG (AUTOSAMPLER)
- Tng thch vi cc b phn nguyn t ho ngn la , l nung hay b ho hi
- Chuyn ng a nng theo trc XYZ .
Ph tng cho b bm mu t ng :
+ B kit bao gm : cc ng mu 2ml (1000 ci) , cc ng mu 0,5ml (1000 ci)
v 02 ng ly mu .
N CATHODE RNG
- B n Cathode rng cho h thng gm : (10 n)
n Cathode rng Cd , n Cathode rng Mn , n Cathode rng Si , n Cathode
rng Cu , n Cathode rng Hg , n Cathode rng Pb , n Cathode rng Al , n
Cathode rng Fe , n Cathode rng As , n Cathode rng Zn .
Ph kin yu cu cho n Cathode rng :
+ Dung dch chun cho n Cathode (cung cp : Merck)
U T N2O
- Dng phn tch kim loi nh Al v Si
Yu cu km theo : Van kh N2O v bnh kh N2O
H THNG CUNG CP KH CHO H THNG
H thng yu cu gm :
- Bm nn kh khng du
- Van kh C2H2
- Bnh kh C2H2 : yu cu kh dng cho phn tch , tinh khit 99,8%

* Mt s thit b yu cu thm cho H thng phn tch quang ph hp thu nguyn

t :
1/ H thng ht kh thi :
- Lp t ti ni t thit b , c tc dng ht kh thi t thit b a ra ngoi .
2/ L nung :
- Dng tro ho mu phn tch
- Nhit ti a : khong 1100oC
3/ L ph mu vi sng :
- Phn hu mu nhanh chng , phc v cho qu trnh chun b mu phn tch .
(Tham kho thit b ph mu vi sng ca hng Aurora).
Quang ph hp th nguyn t AAS
( Manufacturer )
Call for Pricing

Xem hnh y

My quang ph hp th nguyn t nh lng trc tip cc nguyn t kim loi

trong cc loi mu: than, khong sn, sng, du m...vi hm lng chnh xc n
ppm.
My mi 100%, sn xut nm 2009.
Hot ng iu kin nhit i: nhit 150C- 350C; m: 20%-80%
Ngun in 220-240V/50-60Hz
t tiu chun M, Chu u.
Phng php ph hp thu nguyn t
Phng php ph hp thu nguyn t o s suy gim cng bc x ti mt
bc sng c trng b hp thu bi mt m hi nguyn t t do.
Cng hp thu t l vi mt hi n nguyn t, t l vi nng
c s dng trong phn tch nh lng.
S LC PHNG PHP PH HP THU NGUYN T
(AAS - Atomic Absorption Spectrometric)
1. Nguyn t:
Vt cht c cu thnh bi nhng nguyn t ha hc. V d: nc (H2O)

c cu thnh t nguyn t Hydro (H) v oxy (O); thanh st c cu

thnh bi cc nguyn t st (Fe).

Hnh 1: Cu to nguyn t
Theo thuyt Dalton, nguyn t ha hc li bao gm nhng nguyn t ca cng 1
loi nguyn t . V th c th xem nguyn t l phn t nh nht cn gi c
tnh cht ca mt nguyn t. V d: nguyn t Fe c cu to bi nhng nguyn
t Fe.
Cu to nguyn t gm 01 ht nhn v cc electron (in t). Cc in t sp xp
v phn b trn cc lp qu o t trong ra ngoi. Cc in t qu o ngoi
cng gi l in t ha tr.
2. S hp thu ca nguyn t:
Trong iu kin bnh thng, cc in t chuyn ng trn cc qu o ng vi
mc nng lng thp nht E0.

Hnh 2 : Qu trnh hp thu v pht x

Trang thi ny gi l trng thi c bn bn vng (nguyn t khng pht hoc thu
nng lng)
Khi cc nguyn t dng hi v c cung cp mt nng lng ph hp di
dng bc x th cc in t ha tr ca nguyn t ny s hp thu nng lng
v nhy ln mc nng lng cao hn. Lc ny ta ni nguyn t ang trang thi
kch thch En.
Mi loi nguyn t s hp thu ti a v chn lc mt nng lng bc x c
trng (bc x cng hng) ty theo cu to ha hc ca nguyn t .
3. Phng php ph hp thu nguyn t:
L phng php da trn nguyn l hp thu ca hi nguyn t. Ngi ta cho chiu
vo m hi nguyn t mt nng lng bc x c trng ca ring nguyn t .
Sau o cng cn li ca bc x c trng ny sau khi b m hi
nguyn t hp th, s tnh ra c nng nguyn t c trong mu em phn tch.
4. My quang ph hp thu nguyn t (AAS: Atomic Absorption
Spectrometer)
Bao gm cc b phn c bn sau:
- Ngun pht tia bc x cng hng ca nguyn t cn phn tch: thng l n
cathod rng HCL (Hollow Cathode Lamp) hoc n phng in khng cc EDL
(Electronic Discharge Lamp)
- H thng nguyn t ha mu phn tch, c hai loi k thut nguyn t ha mu:
+ K thut nguyn t ha bng ngn la, s dng kh C2H2 v khng kh nn
hoc oxit nit (N2O), gi l Flame AAS.
+ K thut nguyn t ha khng ngn la, s dng l in, gi l ETA-AAS
(Electro -Thermal-Atomization AAS)
- B n sc c nhim v thu nhn, phn ly v ghi tnh hiu bc x c trng sau
khi c hp thu

Hnh 3 : S h thng my hp thu nguyn t AAS

- H in t/ my tnh iu khin v x l s liu
My AAS c th phn tch cc ch tiu trong mu c nng t ppb - ppm. Mu
phi c v c ha thnh dung dch ri phun vo h thng nguyn t ha mu
ca my AAS. Khi cn phn tch nguyn t no th ta gn n cathode lm ca
nguyn t . Mt dy dung dch chun ca nguyn t cn o bit chnh xc
nng c o song song. T cc s liu o c ta s tnh c nng ca
nguyn t cn o c trong dung dch mu em phn tch.
u im ca my AAS :

chnh xc ca my AAS cao: RSD < 2%

lp li rt tt: RSD < 1%
nhy: rt nhy, o dc hm lng ti ppb (microgam/ kg)
Chi ph u t thp so vi my ICP-OES
Phn tch c rt nhiu nguyn t v thi gian phn tch nhanh

Hnh 4 : H thng my hp thu nguyn t AAS ca hng Varian

Ngun: Phng CNTN
MY QUANG PH HP TH NGUYN T (AAS)

1. Tn thit b: My Quang ph hp th nguyn t (AAS)

2. K m hiu: AAS 6800
3. Hng sn xut: Shimazdu Nht Bn
4. nh chp ton cnh thit b

M t thit b: My quang ph hp th nguyn t (AAS) 6800 do hng Shimazdu

- Nht Bn ch to l loi thit b chuyn s dng phn tch hm lng cc kim
loi nng trong mi trng khng kh, t, nc, phn bn v cc sn phm nng
nghip. Thit b s dng h iu hnh Windows XP iu khin gip ngi vn
hnh d dng s dng vi cc giao din thn thin.
5. Cc thng s k thut ch yu
My chnh phn ngn la (khong bc sng t 190 900 nm) v l graphit (
nguyn t ha mu khng ngn la); T ng iu chnh khe o khi thay i cc
nguyn t o; iu khin qua u cm bin tt c cc thng s p sut, ngn la
; c th lm ti 20 php o lp li v t ng loi tr cc kt qu sai so vi
chun % hng s dao ng; t ng chnh nn; t ng tnh h s pha long; c
th gn 8 n trn mt turet; c ti liu hng dn o cho tng nguyn t
(cookbooks); c l graphit vi ch hydro ha mu bng HVG hoc MVU cho
cc nguyn t d bay hi; c h thng bm mu t ng.
6. Nguyn l hot ng
C s l thuyt ca php o AAS l s hp th nng lng (bc x n sc) ca
nguyn t t do trng thi hi (kh) khi chiu chm tia bc x qua m hi ca
nguyn t y trong mi trng hp th. V vy mun thc hin c php o ph
hp th nguyn t cn phi c cc qu trnh sau:

+ Chn cc iu kin v mt loi thit b ph hp chuyn mu phn tch

t trng thi ban u (rn hay dung dch) thnh trng thi hi ca cc nguyn t t
do. l qu trnh nguyn t ho mu. Nhng thit b thc hin qu trnh ny
gi l h thng nguyn t ho mu.
+ Chiu chm tia sng pht x ca nguyn t cn phn tch qua m hi
nguyn t va iu ch c trn. Cc nguyn t ca nguyn t cn xc nh
trong m hi s hp th nhng tia bc x nht nh v to ra ph hp th ca n.
y, mt phn cng ca chm sng b mt loi nguyn t hp th v ph
thuc vo nng ca nguyn t trong mi trng hp th. Ngun cung cp chm
tia sng pht x ca nguyn t cn xc nh gi l ngun bc x n sc.
+ AAS 6800 c th nguyn t ha mu bng ngn la hoc khng ngn la
(s dng l graphit) c nhy rt cao c khi gp hng trm n hng nghn ln
php o trong ngn la nn c th xc nh c cc nguyn t vt vi nng
rt nh.

7. Cc thng s ca mu m thit b c th o c:
Hm lng cc kim loi nng nh (Cu, Pb, Zn, Cd, Hg, As, B, Cr, Al, Fe, Ni, )
cc kim loi kim v kim th (Ca, Mg, K, Na ) c trong cc thnh phn mi
trng t, nc, khng kh, phn bn v sn phm nng nghip.

8. Cc kt qu chnh:

9. Yu cu c bn i vi cc mu o: Hu ht tt c cc mu th rn (s c
ph hy bng l vi sng), lng, kh (c hp th trong dung dch ri o bng
my)
10. Lnh vc p dng v gii hn ca thit b: p dng cho cc nghin cu v
cht lng mi trng, gim st mi trng, kim nh cht lng phn bn v
sn phm nng nghip.
11. a im lp t thit b: Phng th nghim phn tch mi trng Khoa
Mi trng Trng i hc Khoa hc T nhin. Phng 102 nh T2, 334 Nguyn
Tri, Thanh Xun, H Ni.
12. Nm a vo s dng: 2008
13. Cn b qun l vn hnh: NCV. Nguyn Xun Hun. Mobile: 0983665756
CQ: 043.8584995
a ch : 02 Nguyn Vn Th, akao, qun 1, TP H Ch Minh

in thoi : 08.38295087 - Fax : 0838293087

Email : casehcm@case.vn