Materials & Streams Report April 14, 2011

for Syafiq - Tutorial one

1. OVERALL PROCESS DATA

Annual Operating Time 7,912.90 h
Annual Throughput 0.00 kg MP
Batch Throughput 0.00 kg MP
Recipe Batch Time 11.91 h
Recipe Cycle Time 10.52 h
Number of Batches per Year 752.00
MP = Main Product = Unknown

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2.1 STARTING MATERIAL REQUIREMENTS
Amount
Gross
Needed Molar Mass
Mass
Section Starting Material Active Product (kg Yield Yield
Yield
Sin/kg (%) (%)
(%)
MP)
Main Section (none) (none) Unknown Unknown Unknown Unknown

Sin = Section Starting Material, Aout = Section Active Product

2.2 BULK RAW MATERIALS (ENTIRE PROCESS)

Raw Material kg/yr kg/batch kg/kg MP
Heptane 676,800 900.000
A 37,600 50.000
B 30,080 40.000
TOTAL 744,480 990.000

2.3 BULK RAW MATERIALS (PER SECTION)

SECTIONS IN: Main Branch

Main Section
Raw Material kg/yr kg/batch kg/kg MP
Heptane 676,800 900.000
A 37,600 50.000
B 30,080 40.000
TOTAL 744,480 990.000

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2.4 BULK RAW MATERIALS (PER MATERIAL)
Heptane
Procedure % Total kg/yr kg/batch kg/kg MP
Main Section (Main Branch)
P-1 88.89 601,600 800.000
P-2 11.11 75,200 100.000
TOTAL 100.00 676,800 900.000

A
Procedure % Total kg/yr kg/batch kg/kg MP
Main Section (Main Branch)
P-1 100.00 37,600 50.000
TOTAL 100.00 37,600 50.000

B
Procedure % Total kg/yr kg/batch kg/kg MP
Main Section (Main Branch)
P-1 100.00 30,080 40.000
TOTAL 100.00 30,080 40.000

2.5 BULK RAW MATERIALS (kg/batch): SECTION TOTALS

Raw Material Main Section
Heptane 900.000
A 50.000
B 40.000
TOTAL 990.000

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2.6 BULK RAW MATERIALS (kg/yr): SECTION TOTALS
Raw Material Main Section
Heptane 676,800
A 37,600
B 30,080
TOTAL 744,480

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3. STREAM DETAILS
Stream Name Heptane A B Emission
Source INPUT INPUT INPUT P-1
Destination P-1 P-1 P-1 OUTPUT
Stream Properties
Activity (U/ml) 0.00 0.00 0.00 0.00
Temperature (°C) 25.00 25.00 25.00 20.00
Pressure (bar) 1.01 1.01 1.01 1.01
Density (g/L) 681.57 994.70 994.70 1.40
Component Flowrates (kg/batch)
A 0.000 50.000 0.000 0.000
B 0.000 0.000 40.000 0.000
Heptane 800.000 0.000 0.000 0.227
Nitrogen 0.000 0.000 0.000 1.030
Oxygen 0.000 0.000 0.000 0.313
TOTAL (kg/batch) 800.000 50.000 40.000 1.570
TOTAL (L/batch) 1,173.768 50.266 40.213 1,119.531

Stream Name Rxt out Wash in C B + Heptane

Source P-1 INPUT P-2 P-2
Destination P-2 P-2 OUTPUT OUTPUT
Stream Properties
Activity (U/ml) 0.00 0.00 0.00 0.00
Temperature (°C) 50.00 25.00 43.12 50.00
Pressure (bar) 1.01 1.01 1.01 1.01
Density (g/L) 683.21 681.57 845.21 670.30
Component Flowrates (kg/batch)
A 2.500 0.000 0.019 2.415
B 32.083 0.000 0.244 30.993
C 55.417 0.000 52.646 2.771
Heptane 799.773 100.000 28.479 772.600
TOTAL (kg/batch) 889.773 100.000 81.388 808.779
TOTAL (L/batch) 1,302.348 146.721 96.293 1,206.595

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Stream Name Wash out
Source P-2
Destination OUTPUT
Stream Properties
Activity (U/ml) 0.00
Temperature (°C) 36.19
Pressure (bar) 1.01
Density (g/L) 674.08
Component Flowrates (kg/batch)
A 0.066
B 0.846
Heptane 98.694
TOTAL (kg/batch) 99.606
TOTAL (L/batch) 147.765

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4. OVERALL COMPONENT BALANCE (kg/Batch)
COMPONENT INITIAL INPUT OUTPUT FINAL
A 0.000 50.000 2.500 0.000
B 0.000 40.000 32.083 0.000
C 0.000 0.000 55.417 0.000
Heptane 0.000 900.000 900.000 0.000
Nitrogen 1.473 0.000 1.030 0.443
Oxygen 0.447 0.000 0.313 0.135
TOTAL 1.921 990.000 991.343 0.578

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5. EQUIPMENT CONTENTS
V-101
Procedure Operation Time (in h) Volume (in L)
P-1 START 0.000 0.000
P-1 CHARGE-1 (Charge) 0.279 1,173.434
P-1 CHARGE-2 (Charge) 0.404 1,223.700
P-1 CHARGE-3 (Charge) 0.521 1,263.913
P-1 REACT-1 (Batch Stoich. Reaction) 6.521 1,302.348
P-1 TRANSFER-OUT-1 (Transfer Out) 10.521 0.000

PFF-101
Procedure Operation Time (in h) Volume (in L)
P-2 START 6.521 0.000
AFTER AUTO-INIT 6.521 1,302.348
P-2 FILTER-1 (Cloth Filtration) 10.521 95.753
P-2 CAKE-WASH-1 (Cake Wash) 11.521 96.293
P-2 TRANSFER-OUT-1 (Transfer Out) 11.906 0.000

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