LVN

VN BN K THUT O LNG VIT NAM

LVN 275 : 2014

PHNG TIN O C CA NC
QUY TRNH KIM NH
Turbidity meters Verification procedure

H NI 2014

LVN 275 : 2014

Li ni u:
LVN 275 : 2014 do Ban k thut o lng TC 17 Phng tin o Ho l bin
son. Vin o lng Vit Nam ngh, Tng cc Tiu chun o lng Cht
lng ban hnh.

VN BN K THUT O LNG VIT NAM

LVN 275 : 2014

Phng tin o c ca nc - Quy trnh kim nh

Turbidity meters Verification procedure

1 Phm vi p dng
Vn bn k thut ny quy nh quy trnh kim nh ban u, kim nh nh k v
kim nh sau sa cha phng tin o c ca nc c phm vi o (0 4000)
NTU v sai s ln nht cho php 5 % gi tr c .

2 Gii thch t ng
Cc t ng trong vn bn ny c hiu nh sau:
2.1 c: gy ra bi s hin din ca cht ha tan v huyn ph nh t st,
bn, cht v c, sinh vt ph du, cc vi sinh vt khc, axt hu c, cht mu trong
cht lng.
2.2 Dung dch chun c u g i
dung dch chun c chng nhn: l
loi cht chun c ch ng nhn th lng c c xc nh.
2.3 Dung dch ng: l dung dch c dng thit lp gi tr c < 0,1 NTU ca
my o c v thng l dung mi tinh khit nh nc kh ion.
2.4 n v o:
NTU: n v o c khuch tn Nephelometric Turbidity Units).
FNU: n v o c Formazin khuch tn Formazin Nephelometric Units .
FTU: n v o c Formazin (Formazin Turbidity Units).
FAU: n v pha long Formazin Formazin Attenuation Units .
1 NTU = 1 FNU = 1 FTU = 1 FAU.

3 Cc php kim nh
Phi ln lt tin hnh cc php kim tra ghi trong bng 1.

LVN 275 : 2014

Bng 1

TT

Tn php kim nh

Ch kim nh

Theo iu
mc ca
quy trnh

Ban u

nh k

Sau sa
cha

Kim tra bn ngoi.

7.1

Kim tra k thut.

7.2

Kim tra o lng.

7.3

3.1 - Kim tra im 0.

7.3.2

3.2 - Kim tra sai s.

7.3.3

3.3 - Kim tra lp li.

7.3.4

4 Phng tin kim nh

Phng tin kim nh c ghi trong bng 2.
Bng 2

TT

Tn phng tin
kim nh

c trng k thut o lng c bn

p dng
cho iu
mc ca
quy trnh

(1)

(2)

(3)

(4)

Chun o lng
- i tr danh nh: 20, 200, 400, 800,
Dung dch chun 2000, 4000 NTU;
c c ch ng
- khng m bo o khng ln hn
nhn.
sai s cho php ca PT.

7.3.3; 7.3.4.

Phng tin o khc

2.1 Dung dch tr ng.

2.2 Bnh nh m c

- Nc ct 2 ln hoc nc siu sch theo

tiu chun TCVN 4851 : 1989 hoc ISO
3696 : 1987.
- Dung tch: 50, 100, 200, 250, 500, 1000
mL.

7.3.2

7.3

- chnh xc: 0,06 0,4 ml.

2.3 Pipet
4

- Dung tch: 1, 2, 3, 5, 10, 20, 25 ml;

- chnh xc: 0,007 0,03 ml.

7.3

LVN 275 : 2014

(1)

(2)

(3)

(4)

- Nhit : 0 50 oC;
Phng tin o
i tr chia: 1 oC.
2.4 nhit v m
- m khng kh: 25 95 %RH;
mi trng
i tr chia: 1 %RH.

Phng tin ph

3.1 Nc ct.

3.2 Bnh xt tia.

3.3

iy l c.

5 iu kin kim nh
Khi tin hnh kim nh, phi m bo cc iu kin mi trng sau y:
- Nhit : 25 5 oC;
- m khng kh:

80 %RH khng ng sng .

6 Chun b kim nh
Trc khi tin hnh kim nh phi thc hin cc cng vic chun b sau y:
- Ch n cc im kim nh tng ng vi cc dung dch chun c gi tr danh nh
nh bng 3.
Bng 3
Gi tr danh nh cc dung dch chun
(NTU)

TT

Phm vi o
(NTU)

(0 500)

20; 200; 400.

(0 1000)

200; 400, 800.

(0 4000)

400; 800; 2000.

7 Tin hnh kim nh

7.1 Kim tra bn ngoi
Phi kim tra bn ngoi theo cc yu cu sau y:
Kim tra bng m t xc nh s ph hp ca phng tin o c ca nc (sau
y g i l PT vi cc yu cu quy nh trong ti liu k thut v hnh dng, kch
thc, hin th, ngun in s dng, nhn hiu v ph kin km theo.
5

LVN 275 : 2014

7.2 Kim tra k thut
Phi kim tra k thut theo cc yu cu sau y :
Kim tra trng thi hot ng bnh thng v c cu chnh ca PT theo ti liu k
thut.
7.3 Kim tra o lng
PT c kim tra o lng theo trnh t ni dung, phng php v yu cu sau y:
7.3.1 Phng php kim nh phng tin o c l so snh kt qu o trc tip gi
tr c ca dung dch chun bng PT v gi tr c c ch ng nhn ca dung
dch chun .
7.3.2 Kim tra im 0
- Dng PT o ti thiu 03 ln lin tip dung dch tr ng.
kim nh ph lc 1.

hi kt qu vo bin bn

- Sai s cho php: 3 % gi tr ln nht ca thang o.

7.3.3 Kim tra sai s
- Ti m i im kim nh, u o ca PT phi c trng ti thiu 03 ln bng
dung dch chun tng ng.
- Ti m i im kim nh, o 03 ln lin tip bng PT.
bin bn ph lc 1.

hi kt qu o c vo

- Sai s c tnh theo cng th c sau:

C Cch
100
Cch

T ong :

- Sai s tng i, %;

C -

i tr c ca PT, NTU;

Cch -

i tr c c ch ng nhn ca dung dch chun, NTU.

- Sai s khng c ln hn sai s cho php ca PT.

7.3.4 Kim tra lp li.
- Ch n 01 dung dch chun c nh trong mc 6 tin hnh kim tra lp
li.
- Dng PT o ti thiu 05 ln lin tip xc nh nng dung dch chun
ch n. hi kt qu vo bin bn kim nh ph lc 1.
- lp li c tnh theo lch chun s trong cng th c sau:

LVN 275 : 2014

Y
n

i 1

n 1

T ong :
n - s ln o;
Yi - gi tr o th i;
Y - gi tr o trung bnh.
- lch chun s khng c ln hn 1/3 sai s cho php ca PT.

8 X l chung
8.1 Phng tin o c sau khi kim nh nu t cc yu cu quy nh theo quy
trnh kim nh ny c nim phong c cu chnh v cp ch ng ch kim nh tem
kim nh, du kim nh, giy ch ng nhn kim nh ... theo quy nh.
8.2 Phng tin o c sau khi kim nh nu khng t mt trong cc yu cu quy
nh ca quy trnh kim nh ny th khng cp ch ng ch kim nh mi v xa du
kim nh c nu c .
8.3 Chu k kim nh ca phng tin o c: 12 thng.

Ph lc 1
Tn c quan kim nh
..

BIN BN KIM NH
S:
Tn phng tin o: .
Kiu: .S:..
C s sn sut: ..Nm sn xut:
c trng k thut:...
..
C s s dng:...
Phng php thc hin:.
Chun, thit b chnh c s dng:..
iu kin mi trng:...
Ngi thc hin: Ngy thc hin:.........
a im thc hin:...
KT QU
1. Kim tra bn ngoi:

Khng t

2. Kim tra k thut:

Khng t

3. Kim tra o lng:

- Kim tra im 0
STT

Kt qu o

Gi tr chun

Sai s

(...........)

(...........)

(...........)

Sai s cho
php
(...........)

1
2
3
Kt lun:

- Kim tra sai s:

TT

Dung dch
chun

Kt qu o

(............)

(............)

Sai s

Sai s
cho php

Kt lun

- Kim tra lp li:

Gi tr chun: . . . . . . . . . .
TT

Kt qu o
(.............)

lch chun

lch chun cho php

1
2
3
4
5
Kt lun:

4 Kt lun: .............................................................................................................
.............................................................................................................
Ngi sot li

Kim nh vin

TI LIU THAM KHO

LU T O L

NG nm 2011.

LVN 113 : 2003

Yu cu v ni dung v cch trnh by vn bn k thut o lng Vit Nam.

TCVN 6165 : 2009 (ISO/IEC GUIDE 99 : 2007)

T vng quc t v o lng h c khi nim, thut ng chung v c bn VIM .

JIS K 0801 : 1986

Continuous Turbidimeter.

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